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ISSN 1392 - 1207. MECHANIKA. 2011. 17(3): 264-270

Performance optimization of aluminium (U) type vibration based electromechanical Coriolis mass flow sensor using response surface methodology
Pravin P. Patil*, Satish C. Sharma**, Roshan Mishra***
*Department of Mechanical Engineering, Graphic Era University, Dehradun, Uttarakhand, India, E-mail: pravinppatil2004@gmail.com **Department of Mechanical and Industrial Engineering, Indian Institute of Technology Roorkee, Roorkee, Dist. Haridwar, Uttarakhand-247667, India, E-mail: sshmedme@iitr.ernet.in ***BHEL, Hydrabad, India, E-mail: roshangreat1@gmail.com

1. Introduction The electromechanical Coriolis mass flow sensor has a tube through which a fluid to be measured flows is supported at one end or both ends thereof , and vibration is applied to a portion of the tube around the supporting point in a direction vertical to the flowing direction of the tube. The Coriolis mass flow sensor utilizes the fact that the Coriolis forces applied is referred to the flow tube when vibration is thus applied thereto are proportional to a mass flow rate [1]. Successful operating performance of mass flow sensor depends on the selection of suitable design variables and conditions [2]. Therefore it is important to determine the operating design parameters at which the response reaches its optimum. The optimum could be either a maximum or a minimum of a function of the design parameters. One of the methodologies for obtaining the optimum results is response surface methodology (RSM). Performance optimization requires many tests. However, the total number of experiments required can be reduced depending on the experimental design technique. It is essential that an experimental design methodology is very economical for extracting the maximum amount of complex information while saving significant experimental time, material used for analyses and personnel costs [3]. This methodology is actually a combination of statistical and mathematical techniques and it was primarily proposed by Box and Wilson [4] to optimize operating conditions in the chemical industry. RSM has been further developed and improved during the past decades with applications in many scientific realms. Myers et al [5, 6] present reviews of RSM in its basic development period and a comparison of different RS metamodels with different applications is given by Rutherford et al [7]. A comprehensive description of RSM theory can be found in [3]. Apart from chemistry and other realms of industry, RSM has also been introduced into the reliability analysis and model validation of mechanical and civil structures [8, 9]. This methodology has been widely employed in many applications such as design optimization, response prediction and model validation. But so far the literature related to its application in Coriolis mass flow sensing is scarce. Thus, the primary objectives of this study was therefore to use RSM in conjunction with central composite design, which requires fewer tests than a full factorial design to establish the functional relationships between three operating variables namely sensor location, drive

frequency and mass flow rate, and phase shift for optimum performance of Coriolis mass flow sensor. These relationships can then be used to determine the optimal operating parameters. In the following sections, the application of RSM and CCD to modeling and optimization of the influence of three operating design variables on the performance of Coriolis mass flow sensor is discussed. 2. Response surface methodology (RSM) RSM is a collection of statistical and mathematical methods that are useful for modeling and analyzing engineering problems. In this technique, the main objective is to optimize the response surface that is influenced by various process parameters. RSM also quantifies the relationship between the controllable input parameters and the obtained response surfaces [3]. The design procedure for RSM is as follows: 1. Performing a series of experiments for adequate and reliable measurement of the response of interest. 2. Developing a mathematical model of the second-order response surface with the best fit. 3. Determining the optimal set of experimental parameters that produce a maximum or minimum value of response. 4. Representing the direct and interactive effects of process parameters through two and three-dimensional (3D) plots. If all variables are assumed to be measurable, the response surface can be expressed as follows
y = f ( x1 , x2 ,..., xi )

(1)

where y is the answer of the system, and xi the variables of action called factors. The goal is to optimize the response variable y . An important assumption is that the independent variables are continuous and controllable by experiments with negligible errors. The task then is to find a suitable approximation for the true functional relationship between independent variables and the response surface [3]. 3. Central composite design (CCD) As mentioned above, the first requirement for RSM involves the design of experiments to achieve adequate and reliable measurement of the response of interest. To meet this requirement, an appropriate experimental

265 design technique has to be employed. The experimental design techniques commonly used for process analysis and modeling are the full factorial, partial factorial and central composite designs. A full factorial design requires at least three levels per variable to estimate the coefficients of the quadratic terms in the response model [4]. A partial factorial design requires fewer experiments than the full factorial design. However, the former is particularly useful if certain variables are already known to show no interaction [10]. An effective alternative to factorial design is central composite design (CCD), originally developed by Box and Wilson [4] and improved upon by Box and Hunter [11]. CCD gives almost as much information as a three-level factorial, requires many fewer tests than the full factorial design and has been shown to be sufficient to describe the majority of steady-state process responses. Hence in this study, it was decided to use CCD to design the experiments. The number of tests required for CCD includes the standard 2k factorial with its origin at the center, 2k points fixed axially at a distance, say , from the center to generate the quadratic terms, and replicate tests at the center; where k is the number of variables. The axial points are chosen such that they allow rotatability [11], which ensures that the variance of the model prediction is constant at all points equidistant from the design center. Replicates of the test at the center are very important as they provide an independent estimate of the experimental error. For three variables, the recommended number of tests at the center is six [11]. Hence the total number of tests required for the three independent variables is 23+ (23) + 6 = 20. Once the desired ranges of values of the variables are defined, they are coded to lie at 1 for the factorial points, 0 for the center points and for the axial points [11]. The codes are calculated as functions of the range of interest of each factor as shown in Table 1. When the response data are obtained from the test work, a regression analysis is carried out to determine the coefficients of the response model (b1, b2, , bn), their standard errors and significance. In addition to the constant (b0) and error () terms, the response model incorporates [10]: linear terms in each of the variables ( x1 , x2 , ..., xn ) ; squared

The solution of Eq. (3) can be obtained by the matrix approach [3]
b = ( X X ) 1 X Y

(4)

where X is the transpose of the matrix X and ( X X ) 1 is the inverse of the matrix X X . The coefficients, i.e. the main effect ( bi ) and twofactor interactions ( bi j ) can be estimated from the experimental results by computer simulation programming applying the method of least squares using the mathematical software package design expert [12].
4. Experimental design

CCD was used to design the experiments to the reason mentioned above. In order to obtain the required data, the range of values of each of the three variables was defined as follows: sensor location of 60 - 120 mm, drive frequency of 62 - 64 Hz, and mass flow rate of 0.1 0.3 kg/s. Applying the relationships in Table 1, the values of the codes were calculated as shown in Table 2. These were then used to determine the actual levels of the variables for each of the 20 experiments (Table 3). Table 1 Relationship between coded and actual values of a variable [3]
Code 1 0 +1 + Actual value of variable xmin [(xmax+xmin)/2][(xmax xmin) /2] (xmax+xmin)/2 [(xmax+xmin) / 2]+[(xmax xmin)/2] xmin

5. Experimental setup and procedure

terms

x12 , x2 2 , ..., xn 2 ;

in

each

of

the

variables

first order interaction terms for each paired combination ( x1 , x2 , x1 x3 , ..., xn i xn ) .

Trials were conducted in an indigenously deve loped setup based on the Coriolis technology for vibration based aluminium U tube CMFS. A brief description of the set-up and the Coriolis action is presented as follows. The Experimental set up used in the present study has been designed on Pro Engineer Wildfire modelling software and later manufactured at the Instrumentation laboratory of Mechanical and Industrial Engineering Department, IIT, Roorkee. Table 2 Independent variables and their levels for CCD
Design parameter Mass flow rate Sensor location (SL) Drive frequency (DF) Symbol unit Kg/s mm Hz -1 Low 0.1 60 62 0 center 0.2 90 63 +1 high 0.3 120 64

Thus for the three variables under consideration, the response model is y = (bo + ) + bi xi + bi xi 2 + bi j xi x j
i =1 i =1 i =1 j = i +1 3 3 3 3

(2)

X1 X2 X3

The b coefficients are obtained by the least squares method. In general Eq. (2) can be written in matrix form

Y = bX +

(3)

where Y is defined to be a matrix of measured values and X to be a matrix of independent variables. The matrices b and consist of coefficients and errors, respectively.

The actual photograph of the experimental setup has been shown in Fig. 1, which consists of the several functional elements such as: Hydraulic bench for providing regulated water supply to the flowmeter. Test bench for

266 supporting the tubes of the Coriolis mass flow sensor. Excitation system for providing mechanical excitation to the Coriolis mass flow sensor, consists of an electrodynamics shaker, control unit, accelerometer and vibration sensor. Virtual instrumentation comprising of noncontact optical sensors, and a signal conditioning unit as shown in Fig. 1. A Coriolis mass flow sensor measures mass flow directly, which is based on the conservation of angular momentum, as it applies to the Coriolis acceleration of a given fluid. cause both arms to vibrate in phase. Mass flowing into the tube starts to receive vibrational energy from the tube walls as it enters the first bend. In this process, the tube loses the same amount of energy. The result is that the phase of the vibrational cycle lags at sensor location of one limbs, the reverse will happen at the location of another limbs. The liquid is vibrating as it enters the bend, but transfers this energy to the pipe. The result is that the mass flow advances the vibrational phase at the sensor location of another limb. When combined, these two changes in vibrational phase produce a twisting of the flow tube. The amplitude of this twist is directly proportional to the mass flow rate and is nearly independent of the temperature, density, or viscosity of the liquid involved. The details of the experimental procedure used to conduct the present study have been described in Fig. 3 as shown below. The hydraulic unit for providing regulated
Constant voltage transformer Test bench

Fig. 1 Actual photographic view of experimental setup. Various design components as follows: 1 - hydraulic bench, 2 - electromagnetic flowmeter, 3 - vibration control unit, 4 - vibration driver,5 - U tube, 6 - test bench, 7 - laser sensors, 8 - sensor holding stand, 9 foundation, 10 - data acquisition box, 11 - inlet pipe, 12 - outlet pipe, 13 - sensor locations In principle, as shown in Fig. 2, a Coriolis mass flow sensor consists of a tube with a fixed inlet and outlet, which is vibrated about the axis, formed by the inlet and outlet ends. The tube used in this study is Aluminium U shaped vibrating tube, and is made to vibrate using an electrodynamics vibration shaker attached at point as shown in figure. Optical analog displacement sensors are mounted as indicated in figure and is labeled as SL on two limbs of tube to measure displacement signals from the vibrating tube. This means that liquid flow is measured by transferring vibrational energy from the meter tubing to the flowing liquid and back to the meter. To appreciate this princepple, imagine a vibrating tube shown in Fig. 2. If no liquid is flowing, the excitation in the middle of the tube will

Fluid in Hydraulic unit

Fluid out

Electromagnetic flow meter

Volume flow rate * Density = mass flow rate

Tube SL1 Vibration control unit Vibration meter amplitude

Optical displacement sensors signals

SL2

V1 (t) Signal conditioner V2 (t)

Vibration exciter

Accelerometer

Virtual instrumentation

Measured PHASE SHIFt

Fig. 3 Flow diagram showing experimental procedure water supply to the mass flow sensor. The hydraulic unit derives its power from the constant voltage transformer (CVT) to maintain constant flow rate. The U-tube is made to vibrate using an electronic shaker. An accelerometer is attached to the shaker which measures the velocity, amplitude and acceleration of the vibration induced by the electronic shaker. The accelerometer gives the feedback to the vibration meter which is observed for maintaining the constant amplitude. A pair of optical displacement sensors has been placed on the mechanical positioning attachment facing the two limbs of the U-tube. The output terminals of the sensors have been connected to the input of the NIDAQ through a signal conditioner. The processing of the signals is processed in Labview to extract phase shift from the two acquired signals using FFT. Accuracy and repeatability for each experiment was achieved with the same input conditions until stabilized output was achieved.
6. Model development and results

Fig. 2 Vibrating aluminium U type tube: 1 - test bench, 2 - vibration driver, 3 - laser sensors, 4 - vibration driver rod, 5 - U tube, 6 - inlet pipe, 7 - outlet pipe, 8 - sensor locations

Results from the experiments are summarized in Table 3. Considering the effects of main factors and the

267 interactions between two factors, Eq. (2) takes the form
y = 0 + 1 x1 + 2 x2 + 3 x3 + 11 x12 + 22 x22 + +33 x32 + 12 x1 x2 + 13 x1 x3 + 23 x2 x3

Table 4 Experimental and predicted values of phase shift (5)


Actual level of variables Drive Mass freflow Sensor location quency rate mm Hz kg/s 120 62 0.1 60 64 0.1 90 63 0.2 90 64 0.2 120 64 0.3 120 62 0.3 90 63 0.2 60 63 0.2 60 62 0.3 90 63 0.2 90 63 0.2 90 62 0.2 120 63 0.2 90 63 0.3 90 63 0.2 60 62 0.1 120 64 0.1 90 63 0.2 90 63 0.1 60 64 0.3 Observed value of Predicted phase value of shift phase shift degrees 1.542886 1.509698 1.238847 1.291726 4.01569 4.192984 2.420494 2.514256 2.920386 2.923913 2.449727 2.263899 4.618508 4.192984 2.85711 3.123008 1.848543 1.766002 4.42002 4.192984 4.16356 4.192984 1.449934 1.887966 4.34051 4.606408 4.911829 4.800876 3.90024 4.192984 0.835637 0.699161 1.609594 1.559185 4.152364 4.192984 3.893454 3.585092 3.068856 2.969095

The coefficients, i.e. the main effect (i) and twofactor interactions (ij) were estimated from the experimental results using a computer simulation applying the method of least squares in design expert simulation software. From the experimental results in Table 3 and Eq. (4), the second-order response functions representing phase shift can be expressed as a function of the three operating parameters of CMFS, namely the sensor location, drive frequency, mass flow rate. Table 3 Central composite design consisting of experiments for the study of three experimental factors in coded and actual levels with experimental results
Test run Coded level of variables X1 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 1 -1 0 0 1 1 0 -1 -1 0 0 0 1 0 0 -1 1 0 0 -1 X2 -1 1 0 1 1 -1 0 0 -1 0 0 -1 0 0 0 -1 1 0 0 1 X3 -1 -1 0 0 1 1 0 0 1 0 0 0 0 1 0 -1 -1 0 -1 1 Actual level of variables Sensor Drive frelocaquency tion mm Hz 120 62 60 64 90 63 90 64 120 64 120 62 90 63 60 63 60 62 90 63 90 63 90 62 120 63 90 63 90 63 60 62 120 64 90 63 90 63 60 64 Observed phase shift degrees 1.542886 1.238847 4.01569 2.420494 2.920386 2.449727 4.618508 2.85711 1.848543 4.42002 4.16356 1.449934 4.34051 4.911829 3.90024 0.835637 1.609594 4.152364 3.893454 3.068856

Test run 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20

Mass flow rate kg/s 0.1 0.1 0.2 0.2 0.3 0.3 0.2 0.2 0.3 0.2 0.2 0.2 0.2 0.3 0.2 0.1 0.1 0.2 0.1 0.3

Fig. 4 Relation between experimental and predicted phase shift values using Eq. 6 6.1. Effect of variables on phase shift In order to gain a better understanding of the results, the predicted models are presented in Fig. 5 through 7 as the 3D response surface plots. Fig. 5 shows the effect of the sensor location and the Drive frequency at the high level of mass flow rate. As can be seen, a higher phase shift can be achieved maintaining a optimum level of drive frequency and sensor location. Fig. 6 shows the effect of the mass flow rate and sensor location at the center level of Drive frequency. The general form of three-dimensional relationship is similar to the previous figure, i.e. a higher phase shift is obtained with optimum level of sensor location but maximum level of mass flow rate. Fig. 7 shows the effect of the mass flow rate and the drive frequency at the center level of sensor location. It can be seen that a higher phase shift can be obtained with

The relationship between response (phase shift) and operating parameters were obtained for coded unit as follows: In coded variables
Phase shift = 4.19 + 0.74 X 1 + 0.31X 2 + 0.61X 3 0.33 X 12 1.99 X 2 2 0.14 X 1 X 2 0.078 X 1 X 3 + +0.15 X 2 X 3 0.55 X 1 X 2
2

(6)

The response factors at any regime in the interval of our experimental design can be calculated from Eq. (6). The predicted values for phase shift with observed values are given in Table 4. The observed values and predicted values of phase shift obtained using model Eq. (6) is presented in Fig. 4 as can be seen, there is a good agreement between predicted values and the observed data points (R2 value of 0.97 for phase shift).

268
64.00

3.37941

5.14372
63.50

4.29929 3.45486

B : D riv e frequenc y

Predicti 4.93
4.50477
63.00

P hase shift

2.61043 1.766

3.94209

62.50

64.00 120.00 63.50

3.37941
63.00

105.00 90.00 62.50 62.00 60.00 75.00

2.25404
62.00 60.00 75.00

2.81672

B: Drive frequency
105.00 120.00

A: Sensor location

90.00

A: Sensor location

Fig. 5 Response surface predicting phase shift from the model equation: effect of the sensor location and the drive frequency at the high level of mass flow rate Phase shift 0.30
5.14484 4.47164
0.25

3.79844

C: Mass flow rate

Phase shift

4.50477

3.12524 2.45204

0.20

3.94209

3.37941

0.15

0.30 120.00
2.81672

0.25 105.00 0.20 90.00 0.15 0.10 60.00 75.00

0.10 60.00 75.00 90.00 105.00 120.00

C: Mass flow rate

A: Sensor location

A: Sensor location

Fig. 6 Response surface predicting phase shift from the model equation: effect of the mass flow rate and sensor location at the center level of drive frequency
0.30

4.9284 4.06943
0.25

3.21047

C: Mass flow rate

Phase shift

4.50477 2.81672
0.20

2.35151 1.49255

3.37941

3.37941

2.25404

2.81672

0.15

0.30

3.94209
0.25 63.50

64.00

2.25404
0.10 62.00 62.50 63.00 63.50 64.00

0.20

63.00 0.15 0.10 62.00 62.50

C: Mass flow rate

B: Drive frequency

B: Drive frequency

Fig. 7 Response surface predicting phase shift from the model equation: effect of the mass flow rate and the drive frequency at the center level of sensor location

269 minimum level of mass flow rate but center level of drive frequency. It is clear from the 3D response surface plots that drive frequency; sensor location and mass flow rate have a significant effect on phase shift. A centre level of sensor location is determined as optimum to achieve maximum phase shift, whereas a maximum level of mass flow rate is determined to achieve maximum phase shift.
7. Conclusions

The application of response surface methodology (RSM) in conjunction with central composite design (CCD) to modeling and optimizing the performance of a Coriolis mass flow sensor was discussed. CCD was used to design an experimental program for modeling the effects of sensor location, drive frequency and mass flow rate on the performance of CMFS. The range of variables of CMFS used in the design were SL 60-120 mm, DF of 6264 Hz and mass flow rate of 0.1-0.3 kg/s. A total of 20 tests including center points were conducted. A mathematical model equation was derived for phase shift by using the experimental data and the mathematical software package design expert. A predicted value from the model equations was found to be in good agreement with observed values (R2 value of 0.97 for phase shift). In order to gain a better understanding of the three variables for optimal CMFS performance, the model was presented as 3D response surface graphs. The model allow confident performance prediction by interpolation over the range of data in the database, it was used to construct response surface graphs (Figs. 5-7) to describe the effect of the variables on the performance of a CMFS. The results show that the all the three variables have a significant effect on phase shift. This study demonstrates that RSM and CCD can be successfully applied to modeling and optimizing CMFS and that it is the economical way of obtaining the maximum amount of information in a short period of time and with the least number of experiments.
Acknowledgement

sponse surface methodology, 1966-1988 Technometrics 31: 137-158. 6. Myers, R.H. 1999. Response surface methodology: current status and future directions (with discussion), J. Qual. Technol. 31: 30-44. 7. Rutherford, B. M.; Swiler, L. P.; Paez, T.L.; Urbina, A. 2006. Response surface (meat-model) methods and applications, Proc. 24th Int. Modal Analysis Conf. (St. Louis, MO): 184-197. 8. Lee, S.H.; Kwak, B.M. 2006. Response surface augmented moment method for efficient reliability analysis, Struct. Saf. 28: 261-272. 9. Gavin, H.P.; Yau, S.C. 2008. High-order limit state functions in the response surface method for structural reliability analysis, Struct. Saf. 30: 162-179. 10. Box, G.E.P.; Hunter, W.G. 1961. The 2kp fractional factorial designs part I and II, Journal of Technometrics 3: 311-458. 11. Box, G.E.P.; Hunter, J.S. 1957. Multi-factor experimental design for exploring response surfaces, Annals of Mathematical Statistics 28: 195-241. 12. Design Expert Software, Version 6, Users Guide, Technical manual, Stat-Ease Inc., Minneapolis, MN, 2004. Pravin P. Patil, Satish C. Sharma, Roshan Mishra ALIUMININIO TIPO VAMZDIO SVYRAVIMAMS OPTIMIZUOTI NAUDOJAMO ELEKTROMECHANINIO KORIOLIO SRAUTO MASS JUTIKLIO CHARAKTERISTIK TYRIMAS TAIKANT PAVIRIAUS REAKCIJOS METODOLOGIJ Rezium Darbe diskutuojama apie paviriaus reakcijos metodikos taikym modeliuojant ir optimizuojant kai kuri projektavimo kintamj tak Koriolio srauto mass jutiklio charakteristikoms. Trys projektavimo kintamieji: jutiklio padtis, suadinimo danis ir tekjimo greitis buvo keiiami atliekant bandymus pagal CCD (Central Composite Design) metodik. Projekte buvo naudojamos tokios kintamj kitimo ribos: jutiklio padtis 60-120 mm, suadinimo danis 62-64 Hz ir mass tekjimo greitis 0.10.3 kg/s. Naudojant laboratorijoje sukurt rang buvo atlikta 20 bandym. Mass srauto jutiklio charakteristikoms optimizuoti naudojant kompiuterin imitavimo program Expert Dx6, buvo sudarytos matematinio modelio lygtys. ios lygtys tai reakcij antros eils funkcijos, rodanios fazi poslink, priklausomai nuo trij projektavimo parametr. Prognozuojami rezultatai gerai sutapo su eksperimentiniais (R2 vert fazs poslinkiui yra 0.97). Norint geriau paaikinti trij kintamj tak optimalioms charakteristikoms, buvo parodyti 3D paviriaus pokyio modeli paveikslai. is tyrimas parod, kad paviriaus reakcijos metodologij ir CCD galima efektyviai naudoti modeliuojant Koriolio srauto mass jutiklio charakteristikas ir tai yra ekonomikas bdas, per trump laik minimaliu bandym skaiiumi teikiantis ypa daug informacijos.

The authors would like to thank the Department of Science and Technology (DST) Government of India for providing the necessary funding to carry out this research work.
References

1. Sharma, Satish C.; Patil, Pravin P.; Vasudev, Major Ashish; Jain, S.C. 2010. Performance evaluation of an indigenously designed copper (U) tube Coriolis mass flow sensors, Measurement 43(9): 1165-1172. 2. Anklin, Martin: Drahm, Wolfgang; Rieder, Alfred. 2006. Coriolis mass flowmeters: Overview of the current state of the art and latest research, Flow Measurement and Instrumentation 17: 317-323. 3. Montgomery, D.C. 2009. Design and Analysis of Experiments; 7th edition. Hoboken, NJ: Wiley. 4. Box, G.E.P.; Wilson, K.B. 1951. On the experimental attainment of optimum conditions, J. R. Stat. Soc. Ser. B 13: 1-45. 5. Myers, R.H.; Khuri, A.I.; Carter, W.H. 1989. Re-

270 Pravin P. Patil, Satish C. Sharma, Roshan Mishra PERFORMANCE OPTIMIZATION OF ALUMINIUM (U) TYPE VIBRATION BASED ELECTROMECHANICAL CORIOLIS MASS FLOW SENSOR USING RESPONSE SURFACE METHODOLOGY Summary In this study, the application of response surface methodology (RSM) for modelling and optimization of the influence of some design variables on the performance of a Coriolis mass flow sensor is discussed. Three design variables, namely sensor location, drive frequency, and mass flow rate were changed during the experimental tests based on Central composite design (CCD). The range of values of the variables used in the design were a sensor location of 60-120 mm, drive frequency of 62-64 Hz and mass flow rate of 0.1-0.3 kg/s. A total of 20 tests were conducted using the experimental setup developed at laboratory. In order to optimize the performance of mass flow sensor, mathematical model equations were derived by computer simulation programming using design-Expert software (DX6). These equations that are second-order response functions representing phase shift were expressed as functions of three design parameters. Predicted values were found to be in good agreement with experimental values (R2 values of 0.97 for phase shift). In order to gain a better understanding of the three variables for optimal performance, the models were presented as 3D response surface graphs. This study has shown that the RSM and CCD could efficiently be applied for modeling the performance of Coriolis mass flow sensor and it is an economical way of obtaining the maximum amount of information in a short period of time and with the fewest number of experiments. . : , , D (Central Composite Design). : 60-120 , 62-64 0.1-0.3 /. 20 . xpert Dx6. . (R2 0.97). 3D . , D , . Received December 21, 2010 Accepted June 07, 2011 . , . , . U

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