BS en 14718-2014
BS en 14718-2014
BS en 14718-2014
National foreword
This British Standard is the UK implementation of EN
14718:2014. It supersedes BS EN 14718:2006 which is
withdrawn.
At the time of publication, this standard is not currently included
in the (UK) product testing to be used for materials in contact with
drinking water as all the methodology in BS 6920, together with
the pass/fail criteria, has not been replaced by EN standards. To
ensure the correct methodology is being used, refer to the
National Approval schemes for the UK before undertaking any
testing. Further information can be obtained for UK approvals
from the Drinking Water Inspectorate and the Water Regulations
Advisory Scheme.
The UK participation in its preparation was entrusted to Technical
Committee EH/6, Effects of materials on water quality.
A list of organizations represented on this committee can be
obtained on request to its secretary.
This publication does not purport to include all the necessary
provisions of a contract. Users are responsible for its correct
application.
© The British Standards Institution 2015.
Published by BSI Standards Limited 2015
ISBN 978 0 580 85701 0
ICS 13.060.20; 23.040.20; 67.250
Compliance with a British Standard cannot confer immunity from
legal obligations.
This British Standard was published under the authority of
theStandards Policy and Strategy Committee on 31 January 2015.
Amendments/corrigenda issued since publication
Date Text affected
EUROPEAN STANDARD EN 14718
NORME EUROPÉENNE
EUROPÄISCHE NORM December 2014
English Version
Influence des matériaux organiques sur l'eau destinée à la Einfluss organischer Materialien auf Wasser für den
consommation humaine - Détermination de la demande en menschlichen Gebrauch - Bestimmung der Chlorzehrung -
chlore - Méthode d'essai Prüfverfahren
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same
status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United
Kingdom.
© 2014 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 14718:2014 E
worldwide for CEN national Members.
BS EN 14718:2014
EN 14718:2014 (E)
Contents Page
Foreword ..............................................................................................................................................................4
1 Scope ......................................................................................................................................................5
2 Normative references ............................................................................................................................5
3 Terms and definitions ...........................................................................................................................5
4 Principle ..................................................................................................................................................6
5 Reagents .................................................................................................................................................6
5.1 Sodium hypochlorite solution ..............................................................................................................6
5.2 Test water ...............................................................................................................................................6
5.3 Rinsing water .........................................................................................................................................6
5.4 Cleaning liquids for apparatus .............................................................................................................6
6 Apparatus for chlorine demand assessment ......................................................................................7
6.1 Materials .................................................................................................................................................7
6.2 Test vessels............................................................................................................................................7
6.3 Equipment ..............................................................................................................................................7
7 Procedural constraints ..........................................................................................................................7
8 Samples of products and test pieces ..................................................................................................7
8.1 Factory made products .........................................................................................................................7
8.1.1 General ....................................................................................................................................................7
8.1.2 Samples and test pieces of factory made products ...........................................................................8
8.2 Site applied products ............................................................................................................................8
8.2.1 General ....................................................................................................................................................8
8.2.2 Samples and test pieces of site applied products .............................................................................9
8.3 Surface-area-to-volume ratio (S/V) .......................................................................................................9
9 Preparation of test water and apparatus .......................................................................................... 10
9.1 Test water ............................................................................................................................................ 10
9.2 Preparation of apparatus ................................................................................................................... 10
9.3 Cleaning of the glassware ................................................................................................................. 10
9.4 Cleaning of stainless steel ................................................................................................................. 10
10 Test procedure .................................................................................................................................... 10
10.1 General ................................................................................................................................................. 10
10.2 Flushing ............................................................................................................................................... 10
10.3 Stagnation ........................................................................................................................................... 11
10.4 Pre-washing......................................................................................................................................... 11
10.4.1 General ................................................................................................................................................. 11
10.4.2 Flushing ............................................................................................................................................... 11
10.4.3 Rinsing ................................................................................................................................................. 11
10.5 Determination of chlorine demand ................................................................................................... 11
10.5.1 General ................................................................................................................................................. 11
10.5.2 Contact water ...................................................................................................................................... 11
10.5.3 Blank waters ........................................................................................................................................ 11
10.6 Determination of free chlorine........................................................................................................... 11
11 Expression of results ......................................................................................................................... 12
11.1 Description of the calculation ........................................................................................................... 12
11.2 Validation of the test results.............................................................................................................. 12
11.2.1 General ................................................................................................................................................. 12
11.2.2 Validation of duplicate samples ........................................................................................................ 12
11.2.3 Validation of blank tests .................................................................................................................... 12
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EN 14718:2014 (E)
Foreword
This document (EN 14718:2014) has been prepared by Technical Committee CEN/TC 164 “Water supply”,
the secretariat of which is held by AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by June 2015, and conflicting national standards shall be withdrawn at
the latest by June 2015.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
This document has been prepared under a mandate given to CEN by the European Commission and the
European Free Trade Association.
In this second edition, along with editorial corrections, an error in Formula (2) in 11.2.3 has been corrected.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece,
Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.
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EN 14718:2014 (E)
1 Scope
This European Standard specifies a method for determining the chlorine demand of organic materials
intended for use in contact with drinking water.
This European Standard is applicable to factory made and site applied products used for the distribution,
transport and storage of drinking water.
This European Standard does not cover the use of high levels of chlorine to disinfect products when they are
put into service.
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated references,
the latest edition of the referenced document (including any amendments) applies.
EN ISO 7393-2:2000, Water quality - Determination of free chlorine and total chlorine - Part 2: Colorimetric
method using N, N-diethyl-1, 4-phenylenediamine, for routine control purposes (ISO 7393-2:1985)
For the purposes of this document, the following terms and definitions apply.
3.1
chlorine demand
ability of a material in contact with chlorinated water to remove/reduce the concentration of free chlorine in the
water compared with a reference sample
3.2
test water
water used for testing purposes prepared with a free-chlorine content as described in 5.2
3.3
rinsing water
test water without added chlorine
3.4
contact water
test water (see 3.2) which has been in contact with a test piece under specified conditions
3.5
blank water
test water (see 3.2) which has been kept at the same specified conditions (e.g. temperature, contact time,
contact with any sealing material) as contact water but without contact with the test piece
3.6
flushing water
tap water
3.7
product
manufactured item, in its finished form
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3.8
sample
one or more units, or a specified quantity of a product, selected from a batch or lot
3.9
test piece
sample or portion of it which is tested to obtain a single test result
3.10
factory made product
product made in a factory under controlled conditions as part of the manufacturing process
3.11
site applied product
manufactured item for application on-site and subsequent contact with water
Note 1 to entry: In this context, the product is the final prepared surface that comes into contact with water.
4 Principle
Test pieces are then completely filled with or immersed in test water. This filling or immersion procedure is
carried out three times on the same test pieces under specified conditions. After each contact period the
contact water is immediately analysed to determine the residual content of free chlorine. Blank tests without
test pieces are undertaken with the same test water to obtain blank water results.
NOTE If the reduction in the free-chlorine concentration of the test water in contact with the test material is
particularly high, the test will have to be repeated using fresh test samples and a reduced S/V test ratio (see 8.3).
The chlorine demand of the material is based on the difference between the free chlorine content of the
contact water (see 3.4) and of the blank water (see 3.5).
5 Reagents
Sodium hypochlorite solution, with a concentration of about 0,1 % by mass of free chlorine determined in
accordance with EN ISO 7393-2, to be prepared from a commercial solution of sodium hypochlorite (NaOCl).
As this sodium hypochlorite solution is unstable, it shall be prepared on the day of use.
Test water shall have a conductivity of < 2 mS/m and a total organic carbon content (TOC) of < 0,2 mg/l C
(e.g. prepared by reverse osmosis, deionization or distillation, followed by activated carbon filtration) and the
addition of sodium hypochlorite solution (see 5.1) to (1,0 ± 0,1) mg/l of free chlorine. The test water shall be
stable in the absence of light, such that the depletion of free chlorine shall not exceed 0,1 mg/l during the
contact period i.e. (72 ± 2) h at (23 ± 2) °C, when stored without contact with a test piece.
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— biodegradable detergent;
6.1 Materials
Vessels, containers, connectors and stoppers, shall be made of materials which do not consume free chlorine
under the conditions of the test (see Annex A).
Test vessels shall be designed for filling without headspace (ullage). They shall be reserved for chlorine
demand testing only and cleaned separately from other items.
6.3 Equipment
Equipment, capable of maintaining the test temperature of (23 ± 2) °C, for the duration of the test.
7 Procedural constraints
Unlike migration tests, the chlorine demand test starts with a fixed concentration of free chlorine and a realistic
surface area to volume (S/V ) ratio according to Tables 1 and 2.
At the end of each contact period there shall be a minimum concentration of free chlorine (see 11.2.3).
NOTE To ensure the results are reliable it is necessary to limit the reduction of free chlorine by fixing a minimum
concentration for free chlorine after the contact period. This is achieved by adapting the best surface area to volume (S/V)
ratio.
8.1.1 General
8.1.1.1 Sampling of products shall be performed in accordance with the relevant product standard,
system standard or the national regulations, where applicable.
8.1.1.2 Care shall be taken that the transport conditions shall not influence the test results.
8.1.1.3 If it is necessary to store samples before testing, they shall be protected from contamination. If
the manufacturer provides written storage instructions they shall be followed. The samples shall be stored in
their original form as delivered.
Where appropriate, storage containers shall be cleaned using the same procedures used for the test
containers.
8.1.1.4 For a product where only part of its surface will come into contact with drinking water, the test
piece(s) shall be prepared so that only this part of its surface is exposed to the test water (see 5.2).
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8.1.1.5 If the preparation procedure for a test piece of a particular type of product has not been covered
in this standard, deviation from this procedure is permissible under the following conditions:
a) product and the test piece shall be produced in the same manner;
b) preparation of the test pieces before testing shall conform to the procedures, which are performed in
practice before the system is put into operation, e.g. curing and cleaning procedures.
8.1.1.6 Ensure that the surface of the test piece(s), which are intended to come into contact with the test
water shall be free from adhesive tapes, labels, ink or pencil marks.
8.1.1.7 The minimum age of the test pieces shall conform to the relevant product standard, system
standard or, if not given in such a standard, a manufacturer recommendation that the product is ready for use.
8.1.2.1 Pipes
For each test, take a specimen of sufficient length from a pipe to give sufficient volume (V) of test water for
analysis purposes.
If no difference in the material composition and the production process exists in the range of diameters
produced, testing the smallest diameter, where appropriate and with regard to the quantity of test water and
the necessary quantity of free chlorine, is sufficient.
8.1.2.2.1 For each test take one or more test pieces of the product and immerse them in a volume of the
test water sufficient to provide enough water for the chlorine demand assessment procedure.
Where it is not possible to reach the analytical limits given for the chlorine demand assessment, the procedure
as described in 8.3 shall be applied, taking into account the calculated S/V ratio.
The test pieces shall have a sufficiently low S/V-ratio to conform the procedural constraints (see Clause 7).
8.1.2.2.2 If the outside and the inside surfaces of the product (including pipes) have a different material
composition, the product may be tested in the form of a more convenient test piece, prepared under the same
manufacturing and processing conditions as used for the product.
8.2.1 General
Test samples shall be prepared by a test laboratory, or under the supervision of a laboratory by the
manufacturer or contractor, in accordance with the manufacturer’s written instructions. Deviation from these
instructions shall only occur with the prior agreement of the test laboratory and manufacturer or contractor.
The test laboratory shall keep a detailed written record of sample production and curing conditions.
If specialized equipment is required for site application of a material, the test samples shall be prepared by a
competent contractor under realistic site conditions, e.g. onto wet surfaces.
Start the test procedure as soon as the curing period specified by the manufacturer is completed.
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8.2.2.1 Preparation
The term site applied materials covers coatings, linings, paints, composite products and sealants.
8.2.2.2.2 Linings
For self-adhesive linings, apply the samples to the test panel(s) of the substrate for which it is intended.
For non-adhesive linings, test a sheet prepared in accordance with the manufacturer’s instructions.
Test pieces shall be prepared such that only the surface intended to come into contact with drinking water is
exposed to the test water.
NOTE If it is necessary to seal cut the edges of test pieces, it is better to use a sealant that is inert under the
specified test conditions.
8.2.2.2.4 Sealants
Apply the product to test plates of the substrate for which it is intended.
where:
S is the surface area of the test piece in contact with the test water, in square decimetres;
V is the volume of test water in contact with the test piece, in litres.
The surface area to volume ratio for pipes is determined by the pipe diameter. For other products Tables 1
and 2 give suitable values for the initial tests.
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EN 14718:2014 (E)
If the concentration of free chlorine in the test water is reduced to less than 0,4 mg Cl2/l after (72 ± 2) h of
contact with the test material, repeat the test using fresh test pieces with an S/V-ratio of one half of that
previously used.
The vessels and other items necessary for the test shall conform to the requirements of Annex A. If this
cannot be achieved then clean the apparatus as described in 9.3.
9.3.1 Clean the glassware to be used, using detergent (see 5.4). Rinse the glassware with rinsing water
(see 5.3) and then clean the inner surface (see 9.3.2).
9.3.2 Clean the inner surface of the glassware with hydrochloric acid (see 5.4) and rinse with rinsing water
(see 5.3).
9.3.3 If further cleaning of the inner surface is necessary, repeat the cleaning using hydrogen peroxide (see
5.4) followed by rinsing with rinsing water (see 5.3).
Perform cleaning as described in 9.3.1 and 9.3.2, using nitric acid (see 5.4) in place of hydrochloric acid.
10 Test procedure
10.1 General
Perform the procedure in the following sequence: flushing, stagnation, pre-washing, exposure to the test water
and finally calculation of the chlorine depletion of the blank water and of the contact water to determine
chlorine demand.
10.2 Flushing
10.2.1 For products that can be flushed such as pipes flush the test piece with flushing water (see 3.6) for
(60 ± 10) min.
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10.2.2 Place test pieces which cannot be flushed like pipes in an appropriate vessel (e.g. a bucket) having a
water through flow from the bottom upwards for (60 ± 10) min.
NOTE For practical reasons, an alternative arrangement described in Annex B may be used when the flow of water
required for large diameter products exceeds the available water supply.
10.3 Stagnation
10.3.1 Fill or immerse the test pieces (from 10.2) using rinsing water (see 5.3) and allow to stand at
(23 ± 2) °C for (24 ± 1) h.
10.3.2 After this period discard the water and carry out pre-washing in accordance with 10.4.
10.4 Pre-washing
10.4.1 General
Pre-washing shall be carried out in two stages, flushing (see 10.2) and rinsing (see 10.4.3).
10.4.2 Flushing
10.4.3 Rinsing
Rinse the test piece(s) three times with rinsing water (see 5.3).
10.5.1 General
The procedure establishing the suitability of the apparatus and the test water is described in Annex A.
Prepare a sufficient quantity of test water (see 5.2) and determine free chlorine concentration (CI) immediately
prior to filling or immersing the test pieces (see 10.5.2).
Fill or immerse the test pieces without headspace using test water and allow them to stand in the absence of
light for (72 ± 2) h at (23 ± 2) °C. At the end of this period, collect the contact waters (see 3.4) and immediately
measure the free chlorine concentration (CT) (see 10.6).
Take the necessary steps to ensure that there is no significant loss of free chlorine during the filling of test
pipes or test vessels.
Repeat 10.5.1 and 10.5.2 two more times with the same test pieces.
Carry out duplicate blank tests at the same time as 10.5.2. Determine the free chlorine concentration (CB) of
the blank waters (see 3.5) immediately after each test period (see 10.6).
Determination of free chlorine shall be carried out in accordance with EN ISO 7393-2.
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11 Expression of results
For each of the three contact periods, the following values are recorded:
Calculate the following average values CT and CB for each contact period.
Calculate the free-chlorine depletion Cd from (CB – CT) for each contact period.
Calculate the free-chlorine demand CD, for each contact period, using the following formula:
Cd × V
CD = (1)
S×3
Where
Cd is expressed in mg Cl2;
S is the surface area of the test piece in contact with the test water, in square decimetres;
V is the volume of test water in contact with the test piece, in litres;
CD is expressed in mg Cl2/dm² x day.
Record the chlorine demand (CD) for each of the 3 contact periods [CD1, CD2, CD3].
11.2.1 General
If any of the following conditions are not met the test is invalid. Any repeat testing shall be undertaken using
fresh samples.
The difference between the duplicate test results from the third 72 h test period shall not exceed 0,2 mg Cl2/l.
For the average of the blanks and for each contact period (10.5.1) the decrease of free chlorine shall not
exceed 0,1 mg Cl2/l when calculated using the following formula :
(CB A +CB B )
CI - ≤ 0,1 mg CI2 / I (2)
2
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EN 14718:2014 (E)
If the concentration of free chlorine of the contact waters (CT) after any of the third 72 h test periods is less
than 0,4 mg Cl2/l, the test shall be repeated using a reduced surface area to volume test ratio (see 8.3).
12 Test report
— levels of free-chlorine concentration in tap water; if > 0,2 mg/l corrective measures should be taken.;
— reference to this standard and to the referring standard or national regulation, if applicable;
— surface area of the test piece exposed to the test liquid (S) in square decimetres calculated from the
actual dimensions of the test pieces;
— any factors which may have affected the results, such as any incidents or any operating details not
specified in this standard;
c) Test results
The test results shall include the calculated chlorine demand data for the three periods (CD1, CD2 and CD3 -
see 11.1).
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Annex A
(normative)
The apparatus used for testing shall conform with the requirement that free-chlorine depletion shall not exceed
0,1 mg/l for each contact period. If new glassware or related items are introduced then this requirement shall
be satisfied by pre-testing (blank test procedure).
After the test procedure has been undertaken for the first time it is recommended that the test vessels are kept
permanently filled with test water between tests to avoid deterioration of the surface with regard to the chlorine
depletion.
After the third test exposure, the vessel shall be refilled completely with test water and stored under test
conditions (room temperature, not exposed to light) until the next test starts in the following week (typically
Thursday through Tuesday). During these five days, chlorine depletion shall not exceed 0,15 mg Cl2/l,
otherwise the results show the need to clean the vessel.
To obtain the depletion rates of the blanks (see 5.2) and the figures mentioned above for between tests, test
water shall conform with 5.2. This shall be verified each time the tests are undertaken.
If the tests are not carried out continuously, or if the test vessels are not kept continuously filled with
chlorinated water, each test shall be preceded by a controlled filling and evaluation of the actual chlorine
depletion of the test vessels as described above.
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Annex B
(informative)
Arrangement for flushing large diameters pipes
An alternative arrangement for flushing large diameter pipes is shown in Figures B.1 and B.2.
This arrangement is designed to produce the required flow rate over the surface of the test piece while using
the minimum quantity of water.
The device is a cylinder made of inert material (see 6.1) with a diameter less than that of the internal diameter
of the test piece.
It is essential for the diameter of the cylinder be at least 10 mm less than that of the internal diameter of the
test piece. This will leave a gap of at least 5 mm between the wall of the cylinder and the test piece. If the gap
is any smaller than this, there will possibly be too much resistance to the waterflow.
The wash water is delivered from a mains tap via a valve and flow meter through a pipe to a space at the
bottom of the cylinder. The cylinder is supported on the base plate by three or four short legs. The space into
which the pipe delivers the water should allow for equal flow of wash water over the whole inside of the test
piece. The space has an air vent which is opened at the start of the washing period in order to let out the air
which would otherwise be trapped in the distribution space. Most of the volume of the cylinder is empty space
which can be filled with e.g. water or sand in order to stabilize the setup.
Towards the top of the cylinder there is an adjustable ring with three or four screws to adjust the height of the
ring for different lengths of test pieces. There are also three or four screws which can be tightened into the
outside of the test pieces in order to ensure that the cylinder is centred within the test piece, thus ensuring
equal flows of wash water over the whole inside surface of the test piece. The position of the ring is adjusted
to allow a free flow of water over the top edge of the test piece. A vertical gap of about 10 mm should be
sufficient.
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EN 14718:2014 (E)
Key
1 air vent 5 flow meter 9 test piece
2 gap > 5 mm 6 plug 10 seal
3 valve 7 height adjusting screw 11 base plate
4 wash water 8 centering screw
Figure B.1 - Example of an arrangement for flushing large diameter pipes, side view
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EN 14718:2014 (E)
Key
1 air vent 5 wash water
2 main cylinder 6 test piece
3 centering screw 7 water inlet
4 adjustable ring
Figure B.2 - Example of an arrangement for flushing large diameter pipes, top view
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