1-2 Extrusion
1-2 Extrusion
1-2 Extrusion
agglomeration technologies
BY GALEN J. ROKEY AND BRIAN PLATTNER
REVIEWED AND EDITED BY ADAM FAHRENHOLZ, CHARLES STARK, AND CASSANDRA JONES
Because preconditioning is recognized as being preconditioners being used in the extrusion cooking
important to producing premium products and industry today are double (DC) preconditioners,
operating an efficient extrusion cooking process, it differential diameter/differential speed (DDC)
is important that the basic principles of the preconditioners, and high intensity (HIP)
preconditioning process are well understood. The preconditioners (see Figure 2-2). The single-shafted
three objectives accomplished during the preconditioner, as found in most traditional
preconditioning process are: hydration of raw pelleting systems was also utilized to a large extent
material particles; heating of raw material particles; in the past in extrustion, but the double-shafted
and mixing of materials added to the preconditioner conditioners represent today’s technology.
in separate streams. This is accomplished in a
preconditioner by holding the materials in a moist,
warm environment for sufficient time and with Figure 2-2. Types of atmospheric
sufficient mixing. This process results in the raw preconditioners.
material particles being plasticized by the steam and
water in the environment. In practice, the objective
is to completely plasticize the raw material particles
in order to eliminate any dry core as illustrated in
Figure 2-1.
conveying. The two shafts of a double Table 2-2. Coefficient of Variation for Moisture
preconditioner usually counter-rotate such that Content in Different Preconditioner Designs
material is continuously interchanged between the Preconditioner Design CV (%)
two intermeshing chambers. HIP 2.65
DDC 4.96
The most recent technology in the industry are the DC (Double Cylinder) 6.66
DDC and HIP preconditioners, which have the best SC (Single Cylinder) 9.36
mixing characteristics combined with the longest
average retention times. Retention times of up to 2- The more uniform moisture distribution not only
4 minutes for throughputs comparable to those used improves extrusion stability for recipes that become
in double and single preconditioners can be sticky when hydrated, but contributes to more
expected. As with a double preconditioner, the two consistent destruction of biological contaminates
shafts of a differential diameter/differential speed (salmonella) using thermal critical control points.
preconditioner usually counter-rotate such that As in traditional pelleting, preconditioners are
material is continuously interchanged between the usually installed above the extruder barrel so that
two intermeshing chambers. The HIP gives an the preconditioned material falls directly into the
added layer of control as each shaft has an inlet of the extruder as depicted in Figure 2-3. In
independent drive. This allows the direction of shaft addition, there are other important installation
rotation and speed of the shaft to be varied allowing recommendations for proper functioning of the
direct operator control of the residence time and preconditioning hardware and process.
mixing intensity (see Table 2-1).
Figure 2-3. Preconditioner installed above an
Table 2-1. Effect of Speed on Residence Time extruder.
Side A Side B
Retention Time
Speed Speed (minutes)
(rpm) (rpm)
100 500 1.00
250 125 1.47
800 50 2.40
water throughout the raw materials, spray nozzles Figure 2-4. Introducing materials to the
are used. Other water-based additives such as preconditioner.
molasses, digests and fresh meats can be added in
conjunction with the water or at any point in the
preconditioning process. It is recommended to add
these slurries as close to the inlet of the
preconditioner as possible to allow for optimal
hydration of the dry materials and uniform
incorporation of all the added streams. Adding these
streams near the discharge of the preconditioner
often causes clumping of the material and does not
allow enough time for the complete incorporation
into the dry mash.
process. This is especially true for those processes mixing efficiency of the preconditioner, as shown in
in which slurries such as fresh meat are added. If Figure 2-7. In certain instances, operators often
effective mixing is not present, individual particles reduce the preconditioner shaft speed in an effort to
may tend to agglomerate, and thus increase the increase the degree of fill, and therefore gain
effective particle size. This increases the resistance retention time for their process. However in doing
to energy and moisture transfer into the raw this, one should also be aware that decreasing the
material particles. The particles end up with a preconditioner shaft speed can significantly
wetted surface and a dry center which leading to an decrease the mixing efficiency.
inferior product and an increase in extruder wear. In
cases where slurries are added and poorly mixed in
the preconditioner, clumps of wet product will be Results of proper preconditioning
evident at the discharge and can plug the inlet of the When the three essential objectives (hydration,
extruder. heating and mixing) of preconditioning prior to
extrusion are adequately satisfied, several results
Figure 2-7. Mixing efficiency for a should be expected. First, in the area of machine
preconditioner. life, preconditioning will increase the life of wear
components in the extruder barrel by several times.
Second, in the area of extruder capacity,
preconditioning has proven to increase the
throughput of the extrusion system. Third, in the
area of product quality, preconditioning assists in
altering product textures and functionality. Finally,
adding preconditioning to the extrusion process
enhances product flavor.
The raw material particles should be thoroughly increased starch gelatinization, and that the first 120
hydrated and heated to eliminate the dry core seconds of retention time are the most important.
present in the center of raw material particles prior Increasing the amount of total steam injection also
to entering the extruder barrel. This leads to more increased starch gelatinization, but at sufficient
efficient cooking of starch and protein. This results retention time, additional steam injection above
in more complete starch gelatinization and protein 10% had little additional effect on starch
denaturation. Theoretical principles of heat and gelatinization.
mass transfer indicate that hydration usually takes
2-8 times longer than does heat penetration.
Pathogen and toxin destruction
A measure of the effectiveness of a preconditioning An additional area in which preconditioning is
process is to examine its effect on key constituents becoming important, is in producing pathogen-free
of the recipe being preconditioned. One key feed. Research has proven that proper conditioning
constituent is the level of starch gelatinization as of the feed prior to final processing can eliminate
measured by the susceptibility of the starch to pathogens such as E. coli, Salmonella and Listeria.
enzymatic conversion to glucose (Mason and If the discharge temperature of the mash exiting the
Rokey, 1992). It has been well documented that conditioning cylinder reaches 72ºC, Salmonella can
starch gelatinization requires three basic elements: be destroyed (Fung and Hoffman, 1993). This work
Elevated temperature, moisture content and time. is further supported by the data in Figure 2-9.
Because the amount of gelatinized starch has a These curves, if extrapolated, indicate that all three
proportional relationship with the amount of heat pathogens would be destroyed if a temperature of at
exposure, it can be used as an indicator of the final least 80ºC is reached.
pellet quality.
Figure 2-9. Thermal death curves for E. Coli,
Figure 2-8. Effect of steam addition and total Salmonella and Listeria.
retention time on cook.
Extrusion
The extrusion process can generally be divided into
two basic categories: Cooking extrusion and A guideline to follow in grinding recipes prior to
forming extrusion. Both processes affect the feed as extrusion is to select a hammermill screen with
the name indicates. Cooking extrusion elevates feed holes being one-third the size of the extruder’s final
temperature to a level that often results in an die orifice. Adhering to this guideline will ensure
expanded product (final feed bulk density less than that all recipe particles will easily pass through the
the bulk density of the starting raw materials). extruder die orifice without danger of plugging or
Feed Pelleting Reference Guide Section 1: Introduction
Chapter 2: Extrusion and Other Technologies
partially plugging the orifice. A sifting device is pellet mills is usually drastically reduced if the fat
often inserted into the process flow between the levels in the recipe exceed 5%, while extruded
grinder and the extruder to remove all foreign products have been processed with internal fat
material and particles that are larger than the die levels as high as 25%.
orifice. It is critical in the extrusion process to avoid
plugging of die orifices, as product is actively The pelleting process depends largely on starch and
flowing through all orifices simultaneously. In a other binding agents to give durability to the final
pellet mill, active product flow occurs only where product. Mild operating parameters in the pelleting
the rolls are forcing or “pressing” the recipe through process yield low levels of starch gelatinization.
the die ring. Several openings can plug in a pellet Gelatinization increases the binding properties of
mill die and little capacity is lost. The total die open the recipe starch. The extrusion process gelatinizes
area in an extrusion application is typically much more of the starch present and thus binding is
less than the pellet mill process and any reduction in increased. This often reduces the level of starch
die open area directly impacts throughput and required in an extruded feed compared to the levels
product quality. required in pelleted feeds for product binding and
structural strength. Extrusion provides flexibility in
The grinding step for an extruder follows the formulating for product characteristics such as
guidelines discussed above, and usually precedes a pellet quality. An increasing number of requests
sifting operation to remove foreign material and come from various industries to process material
large particles. A magnet is usually installed prior to currently classified as waste streams. The intent in
the grinding step in all feed mill process flows to many scenarios is to utilize these materials as a feed
remove tramp metal. It is recommended to also or feed ingredient.
include a magnet just prior to the extrusion or
pelleting process to prevent accidental metal from
the grinding operation from damaging the Hardware components
equipment components. An extrusion system includes a live bin/feeder,
preconditioner, extrusion cooker and die/knife
A major difference in process flows occurs after the assembly as shown in Figure 2-12.
extrusion or pelleting steps. Extruded products
usually contain more moisture than pelleted Figure 2-12. Extrusion system.
products. This moisture must be removed in a
drying step if moisture is greater than 12-15% by
weight of the extruded product. The higher moisture
levels required for most extrusion processes can
lend versatility to the process and expand the feed
manufacturers’ product possibilities. Ingredient
flexibility is an important tool for feed millers in
that it allows the opportunity to take advantage of a
wide variety of ingredient sources. The more
positive conveyance features of an extrusion system
permit the use of wet, sticky ingredients. The high-
temperature/short-time extrusion cooking process is
able to accommodate a wide range of raw materials Each component is designed to accomplish a
that might otherwise be discarded as unqualified specific function in the process of cooking and
material. Pellet mills are limited to 15-18% process forming feed products. The operating conditions
moisture to avoid plugging of the roll and die can be adjusted to vary the characteristics of the
components. Wet byproducts and other high- finished product.
moisture ingredients can be utilized in the extrusion
process at levels up to 60%. The functionality of
Feed Pelleting Reference Guide Section 1: Introduction
Chapter 2: Extrusion and Other Technologies
The live bin/feeder provides a means of uniformly cooking extruded feeds. This additional energy
metering the raw materials into the preconditioner input results in capacity increases, more tolerance
and subsequently into the extruder. This flow of raw for high-fat levels in the formulations and reduced
material must be uninterrupted and the rate requirements for large drive motors. Moisture
controlled. The live bin/feeder controls the product addition in the form of water or steam and a
rate or throughput of the entire system. Variable- properly-configured extruder barrel could result in a
speed augers or screw conveyors can be used to final pressure of the extrudate prior to the extruder
volumetrically meter ingredients into the system. die of 34-37 atmospheres, a temperature of 125-
These same devices can be designed and 150°C and a moisture content of 23-28%.The three
manufactured to act as loss-in-weight (gravimetric) types of extruders most common in the feed
feed systems by mounting the bin/feeder assembly industry are the single-screw, co-rotating twin-
on load cells and continuously monitoring its screw and conical co-rotating twin-screw extruders.
weight. Preconditioning hardware, an important and
necessary step in extrusion of feeds, is discussed in Figure 2-13. Effect of screw speed on specific
depth earlier in this chapter. mechanical energy.
Specific product characteristics or processing The C2TX’s conical design allows for positive
requirements where twin-screw extrusion systems compression in the barrel and reduces possibility of
have found applications are as follows: back feeding. Positive compression yields an
• Ultra-high fat feeds (above 17% internal fat). efficient manner of imparting mechanical energy
• Products which have high levels of fresh meat or into the extrudate. The conical design of the C2TX
other high moisture slurries (above 35%). causes the material to be kneaded and sheared along
• Uniform shape/size product (portioned foods). the screw profile. In traditional twin-screw
• Ultra-small products (0.6 to 2.0 mm diameter extruders, the melt is kneaded and sheared by shear
Feed Pelleting Reference Guide Section 1: Introduction
Chapter 2: Extrusion and Other Technologies
locks, mixing lobes or cut-flight screw elements. Other design advancements in die configurations
The “profile kneading” present in the C2TX design have resulted in “rapid change multiple dies,” where
eliminates the need for such special screws and dies can be changed without stopping the extrusion
locks to provide the appropriate cooking. Therefore, system. This design reduces set-up time by up to
the extruder shafts and screws can be machined 50%, resulting in smaller lot sizes, easier
from a single piece of steel. The result is a lower scheduling, reduced inventory, increased plant
manufacturing cost of the screws and reduced efficiency and increased profitability (Rokey and
maintenance and downtime, since a screw profile Aberle, 2001). A face cutter is used in conjunction
change is not needed for each different product. The with the die, which involves cutting knives
C2TX design provides the possibility for a feed revolving in a plane parallel to the face of the die.
manufacturer to more economically process those The relative speed of the knives and the linear speed
feeds requiring twin-screw extrusion attributes. of the extrudate result in the desired product length.
The blades of the knife run in very close proximity
to the die face, and in the case of spring-loaded
Die/knife design blades, may actually ride on the surface of the die.
The extrusion chamber is capped with a final die Knife blade metallurgy, design, positioning relative
which serves two major functions. The die provides to die face, speed and extrudate abrasiveness
restriction to product flow, causing the extruder to determine their life.
develop the required pressure and shear. The final
die also shapes the extrudate as the product exits the Many feed extrusion applications require changing
extruder. Die design and its effect on expansion, or re-sharpening blades every six to eight hours.
uniformity and appearance of the final product are This is especially critical with intricate shapes. Dull
often overlooked. The amount of expansion desired blades distort the product shape and increase the
in the final product can be controlled by formula number of “tails” or appendages on the product
manipulation and open area in the die. Unexpanded, which later are broken off in drying and handling,
but fully-cooked feeds generally require 550 to 600 resulting in fines. Final product characteristics can
square millimeters of open area per metric tonne of be controlled by the extruder or die configuration
throughput. Highly-expanded feeds require 200 to selected for processing feeds. However, feed millers
250 square millimeters of open area per metric prefer not to lose production time by having to
tonne throughput. change the extruder configuration to modify
specific product characteristics such as final product
Final dies may be as simple as single plates with a bulk density. There are other hardware tools that
pre-determined number of sized round openings, or can be used to control product bulk density. Four
they may consist of two or more plate elements. The tools that are available to the industry include the
first plate element of a two-piece die serves to following:
increase the resistance to flow and to aid in • Vented extruder barrel with or without vacuum
imparting shear to the extrudate. The second die assist;
plate in a two-piece die is used to size and shape the • Separate cooking and forming extruders where the
extrudate by forcing it to flow through a number of product is vented between the two units;
orifices. Very high shear rates are experienced by • Restriction device at the discharge end of the
the extrudate as it flows in a radial direction extruder; and
between the two die plates. Typical products made • Pressure chamber at the extruder die.
on two-piece dies are light-density snacks or treats
for pets and are not applicable to most feed
products. Spacers may be added between the Vented extruder barrel
extruder barrel and the final die plate to even out the
flow from the extruder screw to the final die plate The extruder barrel is normally closed to the
and give additional retention time for cooking. atmosphere and the extrudate is subjected to an
environment of increasing pressures until it exits the
Feed Pelleting Reference Guide Section 1: Introduction
Chapter 2: Extrusion and Other Technologies
die orifice. The high process pressures (0 to 40 bar) Figure 2-18. Vented extruder barrel with
result in significant expansion ratios and product vacuum assist.
densities low enough to produce feeds such as
floating aquafeeds. Expansion can be further
enhanced by injection of steam into the extruder
barrel, which increases thermal energy inputs. Feeds
with high bulk densities are preferred for several
reasons such as:
• Reduced transportation costs;
• Aquatic feeds that are sinking in fresh and sea
water; and
• Increased product bin capacity within a feed mill.
Where higher product densities are required for
certain feeds, the extruder barrel can be configured
to include a vent which releases process pressure Separate cooking and forming extruders
and reduces product temperature through
evaporative cooling (see Figure 2-17). Another hardware tool utilized by the feed
manufacturers to control product bulk density is a
dual extrusion process (see Figure 2-19). In this
Figure 2-17. Extruder with vented barrel.
process, the first extruder is used in solo for the
production of expanded feeds, or it can be used as a
cooking extruder for the two-stage cooking/forming
process. The second, forming extruder (product
densification unit, or PDU) is used only when
processing very dense feeds, such as fast-sinking
aquafeeds.
wide range of feed densities from highly-expanded Table 2-4. Controlling feed density with the
feeds with one extruder, or very dense feeds with BPV.
the cooking extruder and PDU. Final Product
Oil
Back pressure valve Back Uncoated After
Pressure Extruder Product Vacuum
Final product characteristics such as density can be
Valve, Speed Density, Infusion,
controlled by extruder die restriction. One device
% Closed Index g/L %
commonly used by feed manufacturers is termed a
45 1.0 654 16.2
“back pressure valve” (BPV) which is used to adjust
55 1.0 628 19.5
die restriction while the extrusion system is in
65 1.0 530 23.8
operation. By changing the restriction at the
65 1.3 504 28.4
discharge of the extruder during operation, the
70 1.2 420 37.8
product density can be varied by up to 25% without
70 1.3 392 40.5
changing the screw configuration or the final die.
The BPV mounts on the end of the extruder prior to
The extrusion process for feeds is reported to be
the final die assembly (see Figure 2-20).
more stable with a BPV, and
preconditioning/extrusion process temperature
Figure 2-20. Back Pressure Valve requirements are lower, resulting in improved
nutrient retention. The BPV eliminates the need for
altering extruder configurations between different
product families. An integral part of the BPV is a
bypass feature to divert product from the die/knife
assembly and product conveyor for service and
start-up/shutdown procedures, which improves
sanitation in this area.
cooked feed of sufficient bulk density to sink The combined impact of a pressure chamber and a
rapidly and still absorb the required oil during the BPV is illustrated in Figure 2-22. The BPV can be
coating step. used as an independent tool to alter product density
and other critical properties, or can be used in
Table 2-5. Effect of increasing pressure in conjunction with a pressure chamber to further alter
die/knife chamber. product density over a wide range. The hardware
Over- Expected tool of choice to manage product bulk density
Pressure in Increase depends on the process application. Each tool has
Chamber, Boiling Point in Product advantages and disadvantages, and these must be
Bar of Water, °C Density, % evaluated in light of the process requirements. For
0 100 0 example, for very small diameter pellets (<3mm)
0.5 112 10.0 that contain high levels of starch, such as a high-
1.0 121 18.3 carbohydrate shrimp feed, the processing system of
1.5 128 25.0 choice may be the combination of a cooking
2.0 134 28.3 extruder followed by a forming extruder (PDU).
The level of product density increase expected from Figure 2-22. Effect of chamber pressure and
over-pressure in the EDMS depends on several BPV closure on bulk density of 8 mm feed
factors. For example, as the feed pellet size pellets.
(diameter and mass) decreases, a given pressure in
the chamber results in a lower density increase, as
illustrated in Figure 2-21.
Process parameters 24% soybean meal and 16% wheat was extruded at
Extrusion and similar agglomeration techniques six internal fat levels. The internal fat level was
have been utilized to process various feedstuffs for adjusted by continuously injecting fish oil into the
many years. Extrusion cooking is universally preconditioning phase of a single-screw extrusion
recognized as a high-temperature/short-time system at 0%, 0.9%, 1.8%, 3.6%, 7.2% and 14.4%.
process. The higher temperatures employed during As the added internal fat level during extrusion
the extrusion process present an interesting increased, the bulk density of the final product
challenge in the assessment of nutrient retention. increased significantly (see Figure 2-23).
During extrusion, the recipe and its constituents are
subjected to a succession of almost instantaneous As internal fat levels increase, durability decreases.
treatments or unit operations. There is a remarkable decrease in durability when
the total fat level of the extrudate exceeds 12%. Fat
These variables include moisture and temperature added in the extruder has a lubricating effect and
profiles, extruder configuration, extruder speed and reduces mechanical heat dissipation and starch
preconditioning of the material prior to extrusion. gelatinization. Fat also weakens the product matrix
The critical process parameters could be and thus reduces the pellet strength. However,
summarized into four areas—specific mechanical extrusion processes have been used to produce
energy, specific thermal energy, retention time and feeds of up to 22% internal fat, while pelleting
product moisture. processes are limited to 4-5% fat. Energy
management is essential in controlling bulk density
The following process parameters are utilized to of feeds. As energy inputs increase during
control product characteristics such as bulk density: extrusion, the bulk density decreases. Figure 2-24
• Internal and/or external fat levels; indicates the correlation between specific
• Specific mechanical and thermal energy inputs; mechanical energy inputs and the final bulk density
and of the extruded product.
• Extrusion moisture.
Figure 2-24. Effect of specific mechanical energy
Figure 2-23. Effect of internal fat on product on extrudate bulk density.
density.
product will begin to increase in density. Ultra-high Large electrical motors are used to drive expanders,
moisture levels decrease the viscosity of the and up to12 kWh per metric tonne of product is
material in the extruder barrel and make it more required for the expander process alone. Reported
difficult to expand the product. The improvements to pellet quality by coupling an
moisture/density curve (see Figure 2-25) is specific expander to a pellet mill have been inconsistent.
for each product. This may be due to recipe characteristics such as
high internal fat levels, but much of this is due to
Figure 2-25. Effect of extrusion moisture on the low moisture levels employed during
product bulk density. processing. Extruders and expanders have general
similarities in design and function, but they are not
the same. Even within the extruder family, there are
many not-so-subtle differences that have a major
impact on the characteristics of the end product.
Extruders can be broadly classified as dry or moist
and as single- or twin-screw.
Table 2-6. Variations in complexity and conveying of products from the extruder to the
capacity of extruder types. dryer inlet reduces product moisture content 1-2%.
Extruder Type Output Versatility Pneumatic systems help separate sticky products
Single-screw that tend to clump with belt conveyors and improve
Low Low sanitation around the extruder die.
(dry extrusion)
Single-screw The two types of dryers used for most feed products
High Moderate are conveyor and vertical style dryers (Plattner,
(moist extrusion)
Twin-screw 2001).
High High
(moist extrusion)
Final product applications
Post-extrusion processing Many of the advantages claimed for agglomerated
or pelleted feeds are really due to the form in which
For most “dry” feeds, the final moisture content
the feed is presented to the animal, and the fact that
needs to be less than 12% to prevent mold and
the feed has been subjected to a heat treatment. The
bacterial growth. Final products with moistures
relatively dry treatment employed during pelleting
above 12% are sometimes referred to as semi-moist
followed by a pressing step yields a final pellet
products. This group of products may have moisture
matrix that may deteriorate during transportation
levels greater than 30% and represent a category of
and handling. The process flexibility and the
products that cannot be processed on pellet mills.
processors’ philosophy toward total quality
When considering a soft-moist product, one needs
management are the greatest factors in pellet
to determine the water activity of the product.
quality.
Water activity is the critical factor in determining
the lower limit of available water for microbial
Low-moisture or dry extrusion has been utilized in
growth. In general, if the water activity of a product
the feed industry for many years. Although
is less than 0.65, no microbial growth can occur.
applications have usually been limited to extrusion
of dietary ingredients such as full-fat soy, extrusions
of complete diets without a pellet mill have been
Drying and cooling employed. Extrusion has been used to process the
The primary purpose of drying is to reduce the level following feeds:
of moisture in an extrusion cooked product. Many • Full-fat soybeans and other high-oil ingredients;
extruded products exit the extruder die at moisture • Piglet feed and calf starters;
levels above 18%, which necessitates product • Hygienic feeds for poultry;
drying for shelf stability. In some cases, the drying • Protein bypass feeds for ruminants;
process can involve additional heat treatment of the • Aquatic feeds;
product. One example of this is the drying at • Petfoods; and
elevated temperatures to impart a “baked” or • Feeds containing high levels of wet byproducts.
“toasted” flavor and appearance to the product. As
mentioned earlier, many feeds are best processed at
Full-fat soy
extrusion moistures between 23-28%. Some of the
moisture is lost due to flash evaporation as the Full-fat soybeans are thermally processed to destroy
superheated product exits the die and expands. anti-nutritional factors and to increase oil
Further moisture will be lost through evaporative availability, while preserving the nutritional quality
cooling, as the product cools during conveying or of the protein. The major anti-nutritional factor of
when a cooling step is employed. Pellet coolers will concern in raw soybeans is a trypsin inhibitor.
generally result only in a reduction in moisture Trypsin inhibitor is a protease that is harmful to
levels of about 3% and further reductions in most animals and humans, and nutritionists have
moisture levels require a drying step. Pneumatic documented this effect conclusively. This protease
enzyme can be inactivated by heat treatment. A
Feed Pelleting Reference Guide Section 1: Introduction
Chapter 2: Extrusion and Other Technologies
reduction of at least 85% of the trypsin inhibitor been the subject of many studies. However, reports
units is considered necessary by feed technologists indicate moist extrusion of high-fat dairy feeds
to avoid nutritional problems (Schumacher). Pellet increased palatability and milk production by over
mills are unable to process full-fat soya due to the 2.0 kg per day when compared to the same diets
high levels of fat (18-20%) indigenous to soybeans. being pelleted (Castaldo, 1995). Extruded feed
Expanders are capable of destroying 70% of the processing costs were higher, but still netted a 2:1
trypsin inhibitor by processing at 120ºC. In return on the added feed cost. Several patents exist
comparison, moist extrusion destroys up to 95% of for extrusion processing of feedstuffs to increase the
the trypsin inhibitor through heat treatment. Higher protected or bypass protein contents. Soybean meal
moisture during heat processing results in more is extruded in combination with rapeseed meal or
efficient destruction of the trypsin inhibitor and cottonseed meal under specific process parameters
urease activity (McNaugton and Reece, 1980). to yield a protein supplement. The moist heat
Additionally, full-fat soybeans can be moist treatment denatures protein, which escapes large-
extruded to destroy over 95% of the trypsin scale degradation in the rumen and thus serves as a
inhibitor without damaging lysine (Mustakas, et al., protein source for digestion in the abomasum
1964). Evidence indicates that “dry” heat (ruminant stomach).
processing is not as successful as extrusion in
enhancing subsequent nutritional value of raw full- Complete diets
fat soybeans. It may be concluded that any
processing treatment involving moisture tends to Complete diets for livestock, such as piglet feeds,
have a beneficial effect. Thus steam (moist) calf starters and grower and finishing diets for
extrusion tends to result in higher subsequent poultry and swine have been successfully extruded.
nutritive value than dry extrusion and dry roasting Moist, extruded swine finishing diets were
(Wiseman, 1990). compared to mash diets in a Texas A&M University
study. The studies indicated a 13% improvement in
feed efficiency with the moist extruded diet
Pasteurization and Salmonella control (Herbster, 1991). The extruded diets did not
The feed industry is acutely aware of the increase the incidence of ulcers or hyperkeratotic
possibilities of food-borne illnesses related to activity in slaughtered animals. Moist extrusion and
microbial contamination—which can occur at any similar agglomeration technologies have been used
point along the food chain. This is an especially to produce aquatic feeds for many years. Feeds for
important consideration for animal foods/feeds shrimp and other aquatic species are among the
entering the home, such as petfoods. As early as most expensive feeds on the market today. These
1965, widespread testing indicated that moist diets usually contain high-quality ingredients that
extrusion was much more effective than pelleting in are highly digestible and of a high nutrient density.
Salmonella control (see Table 2-7). Moist extrusion using single- or twin-screw designs
are the most common method of processing aquatic
Table 2-7. Effect of extrusion and pelleting on feeds. Feeds are processed to various bulk densities
Salmonella destruction. depending on the species being cultured:
Extruded Pelleted • Floating (carp, tilapia, catfish);
Number of Samples 775 35 • Slow-sinking (trout, salmon yellowtail); and
Process Temperature, °C 95-120 60-85 • Sinking (shrimp, river crab, cod).
Process Moisture, % 25-35 11-19
Salmonella positive, % 0 60 Extrusion permits sinking and floating diets via
density control that is not possible with pellet mills.
Factors that affect product density include the
Ruminant feeds following:
Processing the concentrate portion of beef and dairy • Starch and soluble protein contents of the recipe;
rations through expanders and extruders has not • Thermal and mechanical energy inputs during
Feed Pelleting Reference Guide Section 1: Introduction
Chapter 2: Extrusion and Other Technologies
at the extruder die but, rather, to “form” a strand or must take place prior to extrusion, and the end
a shape that is similar in size and shape to the die product is expanded at the die. However, the
orifice. The intention is to gain as much cooking as ingredient characteristics are similar to those of
possible during extrusion. Generally, it is not semi-moist products and the final product, although
possible to expand the product a great deal due to expanded, is soft and pliable, much like real meat.
the higher levels of fats and oils associated with the
meat portion of the mix, but when the extruder Semi-moist and soft, expanded dog and cat foods
barrel is properly configured, it is possible to fully contain moderate levels of moisture (25-32% on a
cook the mass within the extrusion chamber. wet basis). Due to the elevated moisture contents,
semi-moist and soft, expanded petfoods are
Another major difference between semi-moist and stabilized and protected from spoilage without
dry-expanded petfood products involves extrusion refrigeration. Preservation systems are built into the
moistures and final processing to handle those formulation to adjust the final product water activity
moisture levels. Typical semi-moist products are (Aw) to a level (0.60 to 0.8) where the growth of
extruded in the range of 20-30% moisture. microorganisms is prevented or greatly reduced.
Preservatives are included in the ingredients to The Aw is lowered by humectants (sugars, syrups,
provide shelf stability, and since it is most desirable salts and polyhydric alcohols such as propylene
for the final product to be soft (similar to meat), the glycol). These petfoods are further stabilized by
moisture in the product is not removed following adjusting the pH to levels (4.0 to 5.5) that are too
extrusion or prior to storage. Bulk densities of both low to support many microorganisms. The recipes
the wet stages of semi-moist products as well as the also prevent mold growth by the inclusion of an
packaged final stages differ greatly from typical antimycotic agent such as potassium sorbate.
dry-expanded products. Wet densities of semi-moist
products will range from 480-560 grams per liter, Common ingredients in this category of petfoods
with final densities very much in the same range, include animal products, milk products, fats and
since moisture removal is not required. oils, soybean products, cereal grains and their
byproducts, marine products, minerals and vitamin
Soft expanded products supplements. Semi-moist petfoods are heavier in
bulk density and usually contain fresh animal
The third petfood product category is soft-expanded products while soft, dry products usually contain
products. This category represents an innovative dehydrated animal products and possess bulk
product type that is similar to semi-moist products. densities similar to dry-expanded petfoods.
Both products often contain a relatively high Formulations usually reflect dogs’ preference for
percentage of meat or meat byproducts and are sweetness and cats’ preference for acidic flavors.
typically higher in fats and oils than dry-expanded
products. Meat-type ingredients may be introduced Snacks and Treats
into the extruder by either of the means previously The final market category involves those products
mentioned under the semi-moist category. They often referred to as snacks or treats for pets. These
differ from semi-moist products in that they take on products usually take the shape and appearance of
the expanded appearance associated with dry- real bones; however, there are other snack-type
expanded products after they are extruded. products for pets that come in a biscuit or variety of
Alterations to equipment required to convert a dry- other shapes. In recent years, more and more
expanded petfood system to semi-moist production producers of those types of pet snacks, as well as
are also required in order to produce soft, expanded- would-be producers of those types of petfood
type products. products, are investigating the potential of extrusion
cooking. The primary reason for the interest is the
With soft, expanded-type products, the basic potential cost savings that may be realized from the
extrusion process is similar to that of dry, expanded short-time/high-temperature of the extrusion
products in that conditioning with steam and water cooking process, the high thermal efficiency of
Feed Pelleting Reference Guide Section 1: Introduction
Chapter 2: Extrusion and Other Technologies
extruders, the floor space saved by the process and performance is enhanced by this high-
reduced labor costs may make production of such temperature/short-time process.
products more profitable. A typical extrusion snack
petfood system would utilize the same basic
principles and equipment arrangements of a typical Raw material specifications
semi-moist extrusion system. In some instances, a Every feed production facility manufactures a broad
dry-expanded system can be applied to the range of products. These can include several
production of pet treats or snacks. The primary different diets for a single species (integrators) or
differences would include the final die and cutting several different diets for many species (commercial
apparatus designed for producing a relatively large mills). Broad product assortments require a vast
piece, such as a bone, biscuit or wafer. number of available ingredients to meet the
nutritional requirements of each specific diet. Since
the number of possible ingredient combinations is
Universal Pellet Cooker (UPC) endless, and selection is normally based on least-
cost formulations, demographics or nutritional
A patented UPC cooking system and process (see value, the formulations may change frequently.
Figure 2-26) is an extrusion-based pelleting system Therefore, proper attention must be taken to ensure
(Wenger, 1997; Wenger, 1999). It was designed high-quality pellets are consistently produced.
specifically for the production of livestock feeds; Ingredient grind (mean particle size) and
but because of its design, can also be used to make formulation play a major role in producing high-
other extruded products such as aquatic feeds and quality pellets. These factors similarly affect the
some petfoods. It appears to be more effective, UPC as they do other pelletizers.
efficient and versatile than the traditional pelleting
systems, such as the expander plus pelleting press Many researchers have studied the importance and
that are currently used. The UPC also allows the effect of particle size reduction on animal
processor to utilize many raw materials that do not performance. They have tried to determine the
process well in a conventional pellet mill, such as “optimum” particle size to achieve maximum
those which contain high fiber or high levels of growth rates. The optimum size varies for each
sugar. species, age group and selection of ingredients.
Researchers have found that the common thread in
Figure 2-26. Wenger Universal Pellet Cooker®. particle size reduction is that a smaller mean
particle size will improve animal performance due
to an increased surface area available for enzymatic
attack. However, there are limitations to how fine
one can grind feed before health of the animals
becomes a concern.
If the maximum particle size or foreign matter in dimensional structure when exposed to high
the feed is larger than the die opening, it is possible temperatures. This three-dimensional structure is
that the opening can be plugged or partially modified when the proteins are subjected to
blocked, resulting in a change of appearance of the mechanical and thermal energy. The re-association,
pellets. In cases of severe blockage, the pelleting die which aligns the protein molecules, occurs during
will need to be cleaned before normal operation can laminar flow and forms a rigid structure. However,
proceed. As a rule of thumb, when the desired pellet not all sources of protein are good binders. Those
diameter is 4 mm or less, the suggested maximum sources with low amounts of pre-processing, such
particle size should be one-third the diameter of the as some types of blood plasma meals, contain
opening. For larger diameter pellets, the grind size “functional” protein, which has a greater binding
should be less than one-half of the die opening size. ability than heavily processed sources such as meat
and bone meal. Functional proteins are those that
Table 2-8. Example particle size are not already denatured.
distribution. Three mm grind;
sorghum-based ration. Figure 2-27. Expander-pellet mill flow diagram.
US Sieve Weight, g Weight, %
12 0.03 0.02
16 1.64 1.20
20 27.21 19.88
25 43.29 31.64
30 40.33 29.47
40 17.09 12.49
Pan 7.25 5.30
Total 136.84 100.00
Starch possesses a unique ability to lose its Most sources of fiber strengthen pellets by
crystalline structure and becomes a viscous gel “melting.” The re-association of the lignin present
during processing. This allows it to disperse through in fiber gives binding power to the pellet. It takes
and around structures of other origins. This loss of much higher processing temperatures to melt lignin
crystallinity is known as gelatinization. Upon than it does to gelatinize starch or denature protein.
exiting the UPC and cooling, the starch returns to a Therefore, its influence is often only low to
crystalline state, resulting in a durable structure. moderate in binding ability; yet high-fiber diets will
Between 50-80% of the starch fraction in most diets typically form very durable pellets.
can be gelatinized during processing. Protein, like
starch, can also function as a binder. Protein
denaturation is the modification of a protein’s three-
Feed Pelleting Reference Guide Section 1: Introduction
Chapter 2: Extrusion and Other Technologies
crumbles are produced; and by reducing cutter This combination of temperature and retention time
speed, longer pellet lengths are produced. This will destroy many microbial populations.
flexibility eliminates the need for crumbling rolls to
produce a crumbled feed. The second opportunity to destroy microbes is in
the rotor and stator. The technological concept
behind the UPC differs somewhat from the
Cooling/drying currently-used methods of heat treatment processes.
Other methods depend on high-temperature/short-
Because heat and moisture are added during
time (HT/ST™) processing, meaning the feed
processing, extra equipment is required to lower the
spends a relatively short amount of time (i.e., 20-30
temperature, remove moisture, prevent mold growth
seconds in an extruder and 15-25 seconds in an
and prolong storage life. This is one of the most
expander) at conditions of high temperature and
significant differences between the UPC process
high pressure. However, the UPC utilizes high-
and a traditional pelleting process. The UPC
temperature/micro-time (HT/MT™) processing.
generally operates within the same moisture
This means that the feed spends a much shorter
constraints as other pelletizers. Exit moistures reach
amount of time under these conditions, usually 3-4
a maximum of 18%. This requires a cooler capable
seconds and still reaches temperatures of 115-
of driving off at least 3-6% moisture to achieve
150°C. This ability to cook feed quickly ensures
final moistures of 12% or less. The pellets must also
that heat-sensitive nutrients such as vitamins and
be cooled within 10°C of ambient temperature. In
amino acids are handled more delicately to prevent
situations where a conventional cooler will not
degradation. However, harmful microorganisms,
provide adequate moisture removal, a dryer will be
such as Salmonella, can be completely destroyed.
required. A more complete discussion of the drying
and cooling requirements appear later in this book.
Table 2-9. Nutrient retention and
microorganism destruction. Source: Wenger
Technical Center Test Data. (1996).
Process Impacts Vitamin Lysine, Mold
To this point, both thermal and mechanical energy A, % count,
have been loosely defined, but it is important to Sample IU/kg CFU/g
understand how these process variables affect the Raw Material 1 8,580 0.70 300,000
UPC process. Production of quality livestock feed Processed 12,320 0.71 < 10
depends on many processing variables. Sample 1 Lot 1
Pasteurization and production of durable pellets Processed 13,046 0.72 < 10
require the addition of steam and/or water in the Sample 1 Lot 2
preconditioner to increase product moisture from Raw Material 2 9,042 0.70 300,000
14-18% and a temperature of 70-90ºC. The shear Processed 14,278 0.71 < 10
provided by the rotor, stator and the pelleting die Sample 2 Lot 1
can elevate the product temperature to 110-150ºC Processed 14,190 0.72 < 10
depending on the die configuration and ingredient Sample 2 Lot 2
formulation. Raw Material 3 n/a 1.36 500,000
Processed n/a 1.41 40
Sample 3 Lot 1
Pasteurization
The UPC system offers two opportunities to Table 2-9 shows retention of various heat-sensitive
pasteurize pelleted feed products. The first stage is nutrients and destruction of microorganisms in feed
the DDC preconditioner. As previously mentioned, produced on the UPC. In each case, none of the
the DDC is capable of holding the feed for up to nutrients were degraded, but the detrimental
two minutes and can reach temperatures of 90-95ºC. microorganisms were destroyed. Table 2-14
indicates the results of expanding plus pelleting on
Feed Pelleting Reference Guide Section 1: Introduction
Chapter 2: Extrusion and Other Technologies
vitamin retention. This data show that the expander feed mix has a different Tg and Tm, each feed
does partially destroy some vitamins. formulation will process somewhat differently.
Figure 2-30. State diagram of the UPC process To help understand the Tg phenomena, consider the
(Strahm and Plattner, 2001; Strahm and feed mix as a mass of wax. At room temperature it
Plattner, 2000). is in a crystalline state and breaks when one tries to
bend it. As the wax is heated it becomes pliable.
The temperature at which the wax begins to show a
considerable amount of flexibility could be
considered as its Tg. Continuing to heat the wax will
eventually convert it into a fluid, so the temperature
at which it fluidizes can be considered its Tm.
Figure 2-31 shows photos of a pelleted feed made
using a conventional expander plus pellet mill
process and one from the UPC system, magnified
with a scanning electron microscope. Notice the
laminar structure that develops with the UPC
process. This structure provides superior strength
over the expander plus pelleted product.
Pellet Durability Figure 2-31. Scanning electron micrographs of
The ability for the UPC to produce an extremely pelleted feeds.
durable and dense pellet is illustrated in Figure 2-
30. This graph shows how the raw material
viscosity changes inside the preconditioner and
stator as energy and moisture are added. When
energy inputs are sufficient and the product
temperature moves above the glass transition
temperature (Tg), major components of the raw
material, such as protein and starch, transform from
a highly viscous, glassy state into a rubbery dough.
This change begins to occur in the preconditioner.
Figure 2-32. Effect of SME on trypsin barrel will plug die orifices. Production runs are
destruction (Wenger Technical Center Test often less than one hour due to plugging of the die
Data, 1996). orifices.
Ingredient preparation a die plate that forms and separates the dough into
The raw ingredients used in the process can be individual, continuous strands which have a
much different than the requirements for diameter of the desired product. The agglomerated
conventional extrusion. In typical extrusion, starch strands are then fed into the Sphere-izer for sizing
is required to bind the ingredients together in order and forming to the desired size. The Sphere-izer is a
to form a durable pellet, and contents of 15-20% spinning disc with a series of radially-symmetrical
must be present in the formulation. With the SAS grooves or corrugations. As the ropes drop onto the
process, low-starch formulations can be disc they are broken into small pieces, which
successfully used since the starch required for eventually turn into spheres as the pieces roll over
traditional extruded products does little to bind the the corrugations. Continuous drying of the small
product together because the temperature of the diameter starter feeds presents problems when
process is low, usually in the 40-50°C range. The considering the traditional horizontal continuous
particles are bound by using natural binders from bed dryers and vertical dryers. The small diameter
fishmeal, fish soluble, gluten and other organic products cannot be handled in a static bed or
ingredients. moving bed perforated tray dryer because of several
factors. The SAS products pack together so tightly
Preparation of the formulation mixture includes that they create a bed of product that does not allow
micro-pulverizing to a specified particle size range air to pass through. Therefore, the product will not
to prevent die plugging during processing. After dry completely. To eliminate this problem, a
grinding, the formulation is passed through a rotary vibrating bed/fluid bed dryer is utilized for drying
sieve to remove any particle larger than specified and cooling these products. The fluid bed dryer
for the finished product size. The same particle size forces air through perforations in the vibrating bed
rules apply for the SAS system as in a conventional with enough velocity to suspend the particles in the
extrusion system. The raw materials should have a airflow and keep the product moving and exposed
maximum particle size less than 1/3 of the die to the heated air stream. The cooling portion of this
opening. If this criterion is not met, it becomes very unit does the same only using ambient temperature
difficult to successfully produce a product for any air. A complete flow diagram for the SAS is shown
length of time. in Figure 2-34.