Afton Chemical Specification Manual 2008
Afton Chemical Specification Manual 2008
Afton Chemical Specification Manual 2008
Specification
Handbook
• Viscosity
• Crankcase
• Driveline
• Industrial
• Off-highway
• Engine Tests
• Rig Tests
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Viscosity
Viscosity
Contents Viscosity
01/08 Viscosity - 1
SAE J300 Viscosity Grades for Engine Oils - December 1999
SAE Low Temperature (°C) Low Temperature (°C) Kinematic Kinematic High-Shear
Viscosity Cranking Viscosity(1), Pumping Viscosity(2), cP Max. Viscosity(3) (cSt) Viscosity(3) (cSt) Viscosity(4) (cP) at 150°C
Grade cP Max. with No Yield Stress at 100°C Min. at 100°C Max. and 106 s-1 Min.
0W 6200 at -35 60 000 at -40 3.8 - -
5W 6600 at -30 60 000 at -35 3.8 - -
10W 7000 at -25 60 000 at -30 4.1 - -
15W 7000 at -20 60 000 at -25 5.6 - -
20W 9500 at -15 60 000 at -20 5.6 - -
25W 13000 at -10 60 000 at -15 9.3 - -
20 - - 5.6 < 9.3 2.6
30 - - 9.3 < 12.5 2.9
2.9 (0W-40, 5W-40,
40 - - 12.5 < 16.3
and 10W-40 grades)
3.7 (15W-40, 20W-40,
40 - - 12.5 < 16.3
25W-40, 40 grades)
50 - - 16.3 < 21.9 3.7
60 - - 21.9 < 26.1 3.7
All values are critical specifications as defined by ASTM D 3244.
1 cP=1 mPa.s; 1 cSt=1 mm2s-1
Notes:
(1)ASTM D 5293.
(2)ASTM D 4684. Note that the presence of any yield stress detectable by this method constitutes a failure regardless of viscosity.
(3)ASTM D 445.
(4)ASTM D 4683, CEC L-36-A-90 (ASTM D 4741), or ASTM D 5481.
01/08 - Viscosity - 2
ISO Viscosity Grade Conversions
ISO Mid-point Kinematic Viscosity Limits ASTM, Saybolt Saybolt Viscosity SUS
Viscosity Kinematic cSt at 40°C (104°F) Viscosity Number 100°F (37.8°C)
Grade Viscosity Min. Max. Min. Max.
2 2.2 1.98 2.42 32 34.0 35.5
3 3.2 2.88 3.52 36 36.5 38.2
5 4.6 4.14 5.06 40 39.9 42.7
7 6.8 6.12 7.48 50 45.7 50.3
10 10 9.00 11.0 60 55.5 62.8
15 15 13.5 16.5 75 72 83
22 22 19.8 24.2 105 96 115
32 32 28.8 35.2 150 135 164
46 46 41.4 50.6 215 191 234
68 68 61.2 74.8 315 280 345
100 100 90.0 110 465 410 500
150 150 135 165 700 615 750
220 220 198 242 1000 900 1110
320 320 288 352 1500 1310 1600
460 460 414 506 2150 1880 2300
680 680 612 748 3150 2800 3400
1000 1000 900 1100 4650 4100 5000
1500 1500 1350 1650 7000 6100 7500
01/08 - Viscosity - 3
Viscosity Ranges for AGMA Lubricant Numbers
01/08 - Viscosity - 4
SAE J306 Automotive Gear Viscosity Classification Axle and Manual Transmission Lubricant Viscosity Classification
MIL-PRF-2105E Specification
75W 80W-90 85W-140
Viscosity at 100°C min,mm2/s 4.1 13.5 24.0
max, mm2/s - 18.5 32.5
Viscosity of 150,000 mPa.s,
-40 -26 -12
max temp °C
Channel Point, min, °C -45 -35 -20
Flash Point, min, °C 150 165 180
01/08 - Viscosity - 5
Comparison of Viscosity Classifications Approximate Equivalents
2000 10000
70 8000 300 1500
60
6000 1000 250
1000 50 5000
200 8A
800 4000
40 680
600 3000 8
500 460 140
30 2000
400 7
320
300 1500 6
20 100
90 220 50 90
200 1000 5
800 80 150 40
70 4
600 100 85W
100 500 30
80 10 60 3
9 400 68
55 80W
60 8 300 2
50 7 50 46 20
40 200 1
6 45 32
30 10W 75W
5 150
22
20 4 100 40 5W
80 15
70 10
10 60 Viscosities can be related horizontally only.
8 7
6 50 Viscosities based on 95 VI single grade oils.
5 ISO grades are specified at 40°C.
5
4 40 AGMA grades are specified at 100°F.
3
3 SAE 75W, 80W, 85W, and 5W & 10W specified at low temperature.
35
2 Equivalent viscosities for 100° & 210°F are shown.
2
32
01/08 - Viscosity - 6
Viscosity Equivalents at Same Temperature Approximate Equivalents
Kinematic Saybolt Redwood Engler Saybolt Redwood Kinematic Saybolt Redwood Engler Saybolt Redwood
(Centistokes) Universal No.1 (Degrees) Furol No.2 (Centistokes) Universal No.1 (Degrees) Furol No.2
(Seconds) (Seconds) (Seconds) (Seconds) (Seconds) (Seconds) (Seconds) (Seconds)
1.8 32 30.8 1.14 - - 96.8 450 397 12.8 47.0 -
2.7 35 32.2 1.18 - - 102.2 475 419 13.5 49 -
4.2 40 36.2 1.32 - - 107.6 500 441 14.2 51 -
5.8 45 40.6 1.46 - - 118.4 550 485 15.6 56 -
7.4 50 44.9 1.60 - - 129.2 600 529 17.0 61 -
8.9 55 49.1 1.75 - - 140.3 650 573 18.5 66 -
10.3 60 53.5 1.88 - - 151 700 617 19.8 71 -
11.7 65 57.9 2.02 - - 162 750 661 21.3 76 -
13.0 70 62.3 2.15 - - 173 800 705 22.7 81 -
14.3 75 67.6 2.31 - - 183 850 749 24.2 86 -
15.6 80 71.0 2.42 - - 194 900 793 25.6 91 -
16.8 85 75.1 2.55 - - 205 950 837 27.0 96 -
18.1 90 79.6 2.68 - - 215 1,000 882 28.4 100 -
19.2 95 84.2 2.81 - - 259 1,200 1,058 34.1 121 104
20.4 100 88.4 2.95 - - 302 1,400 1,234 39.8 141 122
22.8 110 97.1 3.21 - - 345 1,600 1,411 45.5 160 138
25.0 120 105.9 3.49 - - 388 1,800 1,587 51 180 153
27.4 130 114.8 3.77 - - 432 2,000 1,763 57 200 170
29.6 140 123.6 4.04 - - 541 2,500 2,204 71 250 215
31.8 150 132.4 4.32 - - 650 3,000 2,646 85 300 255
34.0 160 141.1 4.59 - - 758 3,500 3,087 99 350 300
36.0 170 150.0 4.88 - - 866 4,000 3,526 114 400 345
38.4 180 158.8 5.15 - - 974 4,500 3,967 128 450 390
40.6 190 167.5 5.44 - - 1,082 5,000 4,408 142 500 435
42.8 200 176.4 5.72 23.0 - 1,190 5,500 4,849 156 550 475
47.2 220 194.0 6.28 25.3 - 1,300 6,000 5,290 170 600 515
51.8 240 212 6.85 27.0 - 1,405 6,500 5,730 185 650 580
55.9 260 229 7.38 28.7 - 1,515 7,000 6,171 199 700 600
60.2 280 247 7.95 30.5 - 1,625 7,500 6,612 213 750 645
64.5 300 265 8.51 32.5 - 1,730 8,000 7,053 227 800 690
69.9 325 287 9.24 35.0 - 1,840 8,500 7,494 242 850 730
75.3 350 309 9.95 37.2 - 1,950 9,000 7,934 256 900 770
80.7 375 331 10.70 39.5 - 2,055 9,500 8,375 270 950 815
86.1 400 353 11.40 42.0 - 2,165 10,000 8,816 284 1,000 855
91.5 425 375 12.10 44.2 -
01/08 - Viscosity - 7
Two Components Viscosity Blending (cSt)
Component A
0% 10% 20% 30% 40% 50% 60% 70% 80% 90% 100%
4000 4000
3000 3000
2000 2000
1500 1500
1000 1000
800 800
600 600
500 500
400 400
300 300
200 200
150 150
100 100
90 90
80 80
70 70
60 60
Viscosity Centistrokes
Viscosity Centistrokes
50 50
40 40
30 30
20 20
15 15
10 10
9.0 9.0
8.0 8.0
7.0 7.0
6.0 6.0
5.0 5.0
4.0 4.0
3.0 3.0
2.0 2.0
100% 90% 80% 70% 60% 50% 40% 30% 20% 10% 0%
Component B
01/08 - Viscosity - 8
Base Stocks Viscosities Approximate Equivalents
Neutrals
40°C 100°C
cSt SUS cSt SUS
70N 13.3 70.8 3.0 37.0
80N 15.6 80.3 3.35 37.3
90N 18.0 89.0 3.4 37.5
100N 21.5 104.0 4.0 39.0
140N 30.7 144.0 4.5 41.0
150N 31.6 148.0 4.9 42.4
160N 33.7 158.0 5.2 43.3
170N 34.0 159.0 5.4 44.0
180N 38.5 181.0 5.7 44.9
200N 44.5 204.0 6.2 46.0
250N 56.1 257.0 6.5 47.0
300N 61.3 285.0 7.0 49.0
315N 70.0 315.0 7.9 52.0
330N 70.9 328.0 8.4 53.7
350N 76.0 358.0 8.8 55.0
400N 86.0 398.6 9.8 58.0
450N 98.0 454.0 10.5 61.0
500N 107.0 496.0 11.0 64.0
600N 130.4 604.0 12.1 66.0
650N 141.0 665.0 13.8 71.0
700N 151.0 668.0 14.0 73.0
Brights
40°C 100°C
cSt SUS cSt SUS
135 Brt 413.2 1875.0 28.6 135.0
145 Brt 523.3 2425.0 30.9 145.0
150 Brt 568.0 2632.0 33.0 155.0
160 Brt 600.0 2800.0 35.2 166.0
175 Brt 616.0 2855.0 36.0 169.7
185 Brt 654.7 3034.0 37.6 177.0
225 Brt 1030.0 4800.0 49.3 229.0
01/08 - Viscosity - 9
Conversion Factors
1 yd = 0.9144 m
1 m = 1.0936 yd
1 ft = 0.3048 m
1 m = 3.28 ft
1 in = 2.54 cm
1 cm = 0.3937 in
1 mile = 1.6093 km
1 km = 0.6214 mile
1 sq yd = 0.8361 sq m
1 sq m = 1.1960 sq yd
1 sq in = 6.452 sq cm
1 sq cm = 0.155 sq in
1 cu in = 16.3872 cc
1 cc = 0.0610 cu in
1 cu ft = 0.02832 cu m
1 cu m = 35.314 cu ft
1 cu yd = 0.7646 cu m
1 cu m = 1.3079 cu yd
1 oz = 28.3495 g
1 g = 0.03527 oz
1 lb = 453.59 g
1 kg = 2.20462 lbs
01/08 Viscosity - 10
Crankcase
Crankcase
Contents Crankcase
01/08 Crankcase - 1
Contents Crankcase
Volkswagen
VW 501.01/505.00
VW 505.00
VW 502.00/505.00
VW 502.00/505.01
VW 504.00/507.00
01/08 Crankcase - 2
API Service Classification
“S” Service
01/08 Crankcase - 3
API Service Classification
“S” Service
Oils developed for this service provide improved control of engine deposits,
oil oxidation and engine wear relative to oils developed for previous
categories. These oils also provide protection against rust and corrosion. Oils
meeting API Service Category SG may be used where API Service Categories
SF, SF/CC, SE or SE/CC are recommended.
• The IID gasoline engine test has been correlated with vehicles used
in short-trip service prior to 1978, particularly with regard to rusting.
• The IIIE gasoline engine test has been correlated with vehicles used
in high-temperature service prior to 1988, particularly with regard to oil
thickening and valve train wear.
• The VE gasoline engine test has been correlated with vehicles used in
stop-and-go service prior to 1988, particularly with regard to sludge and
valve train wear.
• The L-38 gasoline engine test requirement provides a measurement
of copper-lead bearing weight loss and piston varnish under high
temperature operating conditions.
• The 1-H2 diesel engine test requirement provides a measurement
of high-temperature deposits.
01/08 Crankcase - 4
API Service Classification
“S” Service
Engine oils that meet API Service Category SJ designation may be used where
API Service Category SH and earlier Categories have been recommended.
Engine oils that meet the API Service Category SJ designation have been tested
in accordance with the CMA Code, may use the API Base Oil Interchangeability
Guidelines and the API Guidelines for SAE Viscosity-Grade Engine Testing.
Engine oils that meet these requirements may display API Service
Category SJ in the upper portion of the API Service Symbol.
Engine oils that meet API Service Category SL designation may be used where
API Service Category SJ and earlier Categories have been recommended.
Engine oils that meet the API Service Category SL designation have been tested
in accordance with the ACC Code and may use the API Base Oil
Interchangeability Guidelines and the API Guidelines for SAE Viscosity-Grade
Engine Testing.
First licence date was July 1, 2001, engine oils that meet these requirements
may display API Service Category SL in the upper portion of the API Service
Symbol.
SM For all automotive engines currently in use. Introduced in 2004, SM oils are
designed to provide improved oxidation resistance, improved deposit protection,
better wear protection, and better low-temperature performance over the life of
the oil. Some SM oils may also meet the latest ILSAC specification and/or
quality as Energy Conserving.
The first license date for API SM was November 30th 2004. Engine oil that meet
these requirements may display API Service Category SM in the upper portion
of the API Service Symbol.
01/08 Crankcase - 5
API Gasoline Engine Performance Criteria
01/08 - Crankcase - 6
API Gasoline Engine Performance Criteria
Test Primary Performance Criteria
SE Sequence IIC or IID IIC IID
Avg. Engine Rust Rating, min. 8.4 8.5
Lifter Sticking None None
Sequence IIIC or IIID IIIC IIID
Viscosity Increase at 100°F.
400 -
and 40 test hrs, %. max.
Viscosity Increase at 40°C.
- 375
and 40 test hrs, %. max.
Avg. Piston Skirt Varnish Rating, min. 9.3 9.1
Ring Land Face Varnish Rating, min. 6.0 4.0
Avg. Sludge Rating, min. 9.2 9.2
Ring Sticking None None
Lifter Sticking None None
Cam & Lifter Scuffing None None
Cam & Lifter Wear, in. average 0.0010 0.0040
Cam & Lifter Wear, in. max. 0.0020 0.0100
Sequence VC or VD VC VD
Avg. Engine Sludge Rating, min. 8.7 9.2
Avg. Piston Skirt Varnish Rating, min. 7.9 6.4
Avg. Engine Varnish Rating, min. 8.0 6.3
Oil Ring Clogging, %. max. 5 10
Oil Screen Plugging, %. max. 5 10
Compression Ring Sticking None None
Cam Wear, in. average - 0.0020*
Cam Wear, in. max. - 0.0040*
CRC L-38 Bearing Weight Loss, mg. max. 40
SF Sequence IID Avg. Engine Rust Rating, min. 8.5
Lifter Sticking None
Sequence IIID Viscosity Increase at 40°C. and
375
64 test hrs, %. max.
Avg. Piston Skirt Varnish Rating, min. 9.2
Ring Land Face Varnish Rating, min. 4.8
Avg. Sludge Rating, min. 9.2
Ring Sticking None
Lifter Sticking None
Cam & Lifter Scuffing None
Cam & Lifter Wear, in. average 0.0040
Cam & Lifter Wear, in. max. 0.0080
Sequence VD Avg. Engine Sludge Rating, min. 9.4
Avg. Piston Skirt Varnish Rating, min. 6.7
Avg. Engine Varnish Rating, min. 6.6
Oil Ring Clogging, %. max. 10
Oil Screen Plugging, %. max. 7.5
Compression Ring Sticking None
Cam Wear, in. average 0.0010
Cam Wear, in. max. 0.0025
CRC L-38 Bearing Weight Loss, mg. max. 40
Note:
* Suggested performance - not pass/fail limit.
01/08 - Crankcase - 7
API Gasoline Engine Performance Criteria
01/08 - Crankcase - 8
API Gasoline Engine Performance Criteria
01/08 - Crankcase - 9
API Gasoline Engine Performance Criteria
01/08 - Crankcase - 10
API Gasoline Engine Performance Criteria
01/08 - Crankcase - 11
API Gasoline Engine Performance Criteria
(1) To be measured at 5˚C greater than that specified by SAE J300 for the viscosity grade of the oil.
(2) For all viscosity grades: If CF-4, CG-4, CH-4 and/or CI-4 categories precede the “S” category and there is no API
Certification Mark, the limits for phosphorus, sulfur, and the TEOST MHT do not apply. Note that these oils have been
formulated primarily for diesel engines and may not provide all of the performance requirements consistent with vehicle
manufacturers’ recommendations for gasoline-fueled engines.
(3) This is a non-critical specification as described in ASTM D3244.
(4) To be evaluated from -5˚C to temperature at which 40,000 cP is attained or -40˚C, or 2 Celsius degrees below the
appropriate MRV TP-1 temperature (defined by SAE J300), whichever occurs first.
01/08 - Crankcase - 12
ILSAC Specifications: GF-1
Test Limits
Viscosity
As defined by SAE J300
Requirements
Engine Test Sequence IID, Sequence IIIE, API SG Limits apply. Tested
Requirements Sequence VE, CRC L-38 according to CMA Code of Practice
Bench Test 6 -1
HTHS Viscosity at 150°C. and 10 s 2.9 min. (for all viscosity grades)
Requirements
Volatility
Sim. dis. (ASTM D2887)
or Evaporative Loss (CEC L-40-T-87)
SAE 0W and 5W multigrades 20% max. at 371°C.
25% max. 1 hr. at 250°C.
All other SAE viscosity grades 17% max. at 371°C.
20% max. 1 hr. at 250°C.
GM EOFT Filterability 50% max. flow reduction
Foaming (Tendency/Stability)
ASTM D892 (Option A)
Sequence I, max. 10/0
Sequence II, max. 50/0
Sequence III, max. 10/0
Sequence IV, max. Report & Report
Flash Point
ASTM D92 or 185°C. min.
ASTM D93 200°C. min.
Shear Stability
L-38 10 hour stripped viscosity Must stay-in-grade
Homogeneity and Miscibility
Federal test method 791B, method 3470 Shall remain homogeneous and
when mixed with SAE reference oils,
shall remain miscible
Additional Sequence VI, EFEI 2.7% min.
Requirements Catalyst Compatibility
Phosphorus Content, %. wt. 0.12% max.
SAE J 300 Low Temperature Viscosity, mPa.s
Cranking 3500 max. at -20°C.
Pumping 30000 max. at -25°C.
01/08 - Crankcase - 13
ILSAC Specifications: GF-2
ILSAC GF-2 is applicable to SAE viscosity grades 0W-X, 5W-X and 10W-X grades only. Oils can be
licensed with the API Engine Oil Licensing and Certification System (EOLCS) from 15 October 1996.
The Sequence VI fuel economy engine test from ILSAC GF-1 is replaced with the Sequence VI-A.
Three categories of fuel economy improvement are possible with ILSAC GF-2.
ILSAC GF-2 oils have a phosphorus limitation of 0.10% maximum compared with 0.12%
maximum for GF-1.
Test Limits
Viscosity
0W-X, 5W-X, 10W-X As defined by SAE J 300
Requirements
Engine Test Sequence IID, Sequence IIIE, API SG Limits apply. Tested
Requirements Sequence VE, CRC L-38 according to CMA Code of Practice
Bench Test CEC L-40-A-93/L-40-T-87 (Noack), % 22 max.
Requirements Phosphorus, % m. 0.10 max.
Flash Point (ASTM D92), °C. 200 min.
Foaming (Tendency/Stability)
Sequence I, max. 10/0
Sequence II, max. 50/0
Sequence III, max. 10/0
High temp. (ASTM 1392), max. 200/50
Homogeneity/Miscibility Pass
GM EOFT Filterability
Flow reduction, % 50 max.
GM EOFT Modified
0.6/1.0% water Rate & Report
2.0/3.0% water Rate & Report
High Temp. Deposits (TEOST)
Deposit wt. mg. 60 max.
Gelation Index 12.0 max.
Additional Sequence VI-A Fuel Economy
Requirements SAE 0W-20, 5W-20 1.4% min.
Other SAE 0W-X, 5W-X 1.1% min.
SAE 10W-X 0.5% min.
01/08 - Crankcase - 14
ILSAC Specifications: GF-3
ILSAC GF-3 is applicable to SAE viscosity grades 0W-X, 5W-X and 10W-X grades only. Oils can be
licensed with the API Engine Oil Licensing and Certification System (EOLCS) from 15 October 1996.
The Sequence VI-A fuel economy engine test from ILSAC GF-2 is replaced with the Sequence VI-B.
Three categories of fuel economy improvement are possible with ILSAC GF-3.
ILSAC GF-3 oils maintain a phosphorus limitation of 0.10% maximum established in ILSAC GF-2
to maintain acceptable catalyst protection.
Test Limits
Viscosity
0W-X, 5W-X, 10W-X As defined by SAE J 300
Requirements
Engine Test Sequence IIIF, Sequence IVA, API SL Limits apply. Tested
Requirements Sequence VG, Sequence VIII, BRT according to ACC Code of Practice
Bench Test Evaporation Loss (ASTM D5800) 15% max. 1hr. at 250ºC.
Requirements Simulated Distillation (ASTM D6417) 10% max. at 371ºC.
Phosphorus, % m. 0.10 max.
Foaming (Tendency/Stability)
Sequence I, max. 10/0
Sequence II, max. 50/0
Sequence III, max. 10/0
High temp. (ASTM 1392), max. 100/0
Homogeneity/Miscibility Pass
GM EOFT Filterability
Flow reduction, % 50 max.
GM EOFT Modified (EOWTT) (*)
0.6/1.0% water 50 max.
2.0/3.0% water 50 max.
High Temp. deposits (TEOST-MHT-4)
Deposit wt. mg. 45 max.
Gelation Index 12.0 max.
Additional Sequence VI-B Fuel Economy FE1 (16hr) FE2 (96hr) Sum FE1/FE2
Requirements SAE 0W-20, 5W-20 2.0 min 1.7 min. -
Other SAE 0W-30, 5W-30 1.6 min. 1.3 min. 3.0 min.
SAE 10W-30 & all other viscosity grades 0.9 min. 0.6 min. 1.6 min.
Notes:
(*) Test formulation with highest additive (DI/VI) concentration.
Read across results to all other base oil/viscosity grade formulations using same
or lower concentration of identical additive (DI/VI) combination.
Each different DI/VI combination must be tested.
01/08 - Crankcase - 15
ILSAC Specifications: GF-4
ILSAC GF-4 is applicable to SAE viscosity grades 0W-X, 5W-X and 10W-X grades only. Oils can be
licensed with the API Engine Oil Licensing and Certification System (EOLCS) from 14 January 2004.
Three categories of fuel economy improvement are possible with ILSAC GF-4.
ILSAC GF-4 oils have a phosphorus limitation of 0.08% maximum compared with 0.10% maximum for GF-3
and a sulphur limit depedent on the viscosity grade, to maintain acceptable catalyst protection.
Test Limits
Viscosity
0W-X, 5W-X, 10W-X As defined by SAE J 300
Requirements
Engine Test Sequence IIIG
Requirements Kinematic Viscosity Increase @ 40ºC, % 150 max.
Average Weighted Piston Deposits, merits 3.5 min.
Hot Stuck Rings none
Average Cam plus Lifter Wear, μm 60 max.
Sequence IIIGA The D 4684 viscosity of the EOT
Evaluate the EOT oil from the ASTM sample must meet the requirements
Sequence IIIGA test with ASTM D 4684 of the original grade or the next
(MRV TP-1) higher grade.
(1)
Sequence VG
Average Engine Sludge, merits 7.8 min.
Average Rocker Cover Sludge, merits 8.0 min.
Average Engine Varnish, merits 8.9 min.
Average Piston Skirt Varnish, merits 7.5 min.
Oil Screen Sludge, % area 20 max.
Oil Screen Debris, % area Rate and report
Hot Stuck Compression Rings None
Cold Stuck Rings Rate and report
Oil Ring Clogging, % area Rate and report
Follower Pin Wear, cyl #8, avg, μm Rate and report (1)
Ring Gap Increase, cyl #1 & #8, avg, μm Rate and report (1)
Sequence IVA
Average Cam Wear
90 maximum
(7 position average), μm
Sequence VIII (2)
Bearing Weight Loss, mg 26 maximum
Sequence VIB
SAE 0W-20 and 5W-20 viscosity grades: 2.3% FEI 1 min. after 16 hrs. aging
2.0% FEI 2 min. after 96 hrs. aging
SAE 0W-30 and 5W-30 viscosity grades: 1.8% FEI 1 min. after 16 hrs. aging
1.5% FEI 2 min. after 96 hrs. aging
SAE 10W-30 and all other viscosity 1.1% FEI 1 min. after 16 hrs. aging
grades not listed above 0.8% FEI 2 min. after 96 hrs. aging
01/08 - Crankcase - 16
ILSAC Specifications: GF-4
Test GF-4 is applicable to SAE viscosity grades 0W-X, 5W-X and 10W-X grades
ILSAC Limits
only. Oils can be
Bench Test Evaporation Loss (ASTM D5800) 15% max. 1hr. at 250ºC
Requirements Simulated Distillation (ASTM D6417) 10% max. at 371ºC
Phosphorous, % mass 0.06 min. - 0.08 max.
Sulphur, % mass,
SAE 0W and 5W multigrades 0.5% max.
SAE 10W multigrades 0.7% max.
Shear Stability, Sequence VIII (ASTM D6709) Kinematic viscosity must remain
10 hr stripped KV @ 100ºC in original SAE viscosity
Ball Rust test (ASTM D6557)
Average Grey value 100 min.
Foaming (Tendency/Stability)
Sequence I, max. 10/0
Sequence II, max. 50/0
Sequence III, max. 10/0
High temp. (ASTM 1392), max. 100/0
Homogeneity/Miscibility Pass
GM EOFT Filterability
Flow reduction, % 50 max.
GM EOFT Modified (EOWTT) (3)
0.6/1.0% water 50 max.
2.0/3.0% water 50 max.
High Temp. deposits (TEOST-MHT-4)
Deposit wt. mg. 35 max.
Additional Sequence VI-B Fuel Economy FE1 (16hr) FE2 (96hr)
Requirements SAE 0W-20, 5W-20 2.3 min. 2.0 min.
SAE 0W-30, 5W-30 1.8 min. 1.5 min.
SAE 10W-30 & all other viscosity grades 1.1 min. 0.8 min.
Notes:
(1) ASTM Surveillance Panel will review statistics annually.
(2) All FEI 1 and FEI 2 values determined relative to ASTM Reference Oil BC.
(3) Test formulation with highest additive (DI/VI) concentration.
Read across results to all other base oil/viscosity grade formulations using same or lower concentration of identical
additive (DI/VI) combination.
Each different DI/VI combination must be tested.
01/08 - Crankcase - 17
API Commercial Classification
“C” Commercial
Oil meeting the performance requirements measure in the following diesel and
gasoline engine tests: The 1-G2 diesel engine test has been correlated with
indirect injection engines used in heavy-duty operation, particularly with regard
to piston and ring groove deposits. The L-38 gasoline engine test requirement
provides a measurement of copper-lead bearing weight loss and piston
varnish under high-temperature operating conditions.
01/08 Crankcase - 18
API Commercial Classification
“C” Commercial
01/08 Crankcase - 19
API Commercial Classification
“C” Commercial
Oils meeting the performance requirements in the following diesel and gasoline
engine tests:
The T-6, T-7, NTC 400 and L-38 engines: See API CE Category above
for explanation.
The 1K diesel engine test, which has been correlated with direct injection
engines used in heavy-duty service prior to 1990, particularly with regard
to piston and ring groove deposits. It has been demonstrated that the 1K
test, in combination with test method D5968, the bench corrosion test, can
be substituted for the NTC-400 test as an acceptable means to demonstrate
performance against this category.
Test method D6483, the T-9 diesel engine test can be used as an alternate
for the T-6 test and its limits.
Test method D5967, the F8A version, and its limits can be used as an alternate
for the T-7 test and its limits.
01/08 Crankcase - 20
API Commercial Classification
“C” Commercial
These oils are especially effective to sustain engine durability even under
adverse applications that may stress wear control, high temperature stability,
and soot handling properties. In addition, optimum protection is provided
against non-ferrous corrosion, oxidative and insoluble thickening, foaming,
and viscosity loss due to shear. These oils also have the performance
capability to afford a more flexible approach to oil drain intervals in
accordance with the recommendations of the individual engine builders
for their specific engines.
CH-4 oils are superior in performance to those meeting API CF-4 and API CG-4
and can effectively lubricate engines calling for those API Service Categories.
Engine oils that meet the API Service Catergory CI-4 designation have been
tested in accordance with the ACC Code and may use the API Base Oil
Interchangeabilit Guidelines and the API Guidelines for SAE Viscocity-Grade
Engine Testing.
CI-4 oils are superior in performance to those meeting API CH-4, CG-4, and
CF-4 and may be used in engines calling for those API Service Catergories.
01/08 Crankcase - 21
API Commercial Classification
“C” Commercial
API Service Category CJ-4 describes oils for use in high-speed four-stroke
cycle diesel engines designed to meet 2007 model year on-highway exhaust
emission standards as well as for previous model years.
These oils are compounded for use in all applications with diesel fuels ranging
in sulfur content up to 500ppm (0.05% by weight). However, the use of these
oils with greater than 15ppm (0.0015% by weight) sulfur fuel may impact
aftertreatment system durability and/or oil drain interval.
Engine oils that meet the API Service Category CJ-4 designation have been
tested in accordance with the ACC Code and may use the API Base Oil
Interchangeability Guidelines and the API Guidelines for SAE Viscosity-Grade
Engine Testing.
API CJ-4 oils exceed the performance criteria of API CI-4 with CI-4 PLUS,
CI-4, CH-4, CG-4 and CF-4 and can effectively lubricate engines calling for
those API Service Categories. When using CJ-4 oil with higher than 15 ppm
sulfur fuel, consult the engine manufacturer for service interval.
The first licence date for API CJ-4 will be October 15, 2006.
Effective May 1, 2006, marketers may license products meeting API CJ-4
requirements as API CI-4 with CI-4 PLUS, CI-4, CH-4, CG-4, and CF-4.
01/08 Crankcase - 22
API Diesel Engine Performance Criteria
Test Primary Performance Criteria Limits
L-4 L-38
CA L-4 or L-38 Bearing Weight Loss, mg. max. 120-135 50
Piston Skirt Varnish Rating, min. 9.0 9.0
L-1 (0.35% min. Top Groove Filling, % vol. max. 25
sulphur fuel) Second Groove and below Essentially clean
CB L-4 or L-38 Same as CA
L-1 (0.95% min. Same as CA, except
30
sulphur fuel) Top Groove Filling, % vol. max.
CC L-38 Bearing Weight Loss, mg. max. 50
Piston Skirt Varnish Rating, min. 9.0
LTD Mod LTD
LTD or Modified LTD Piston Skirt Varnish Rating, min. 7.5 7.5
Total Engine Varnish Rating, min. - 42
Total Engine Sludge Rating, min. 35 42
Oil Ring Plugging, %. max. 25 10
Oil Screen Clogging, %. max. 25 10
IIC IID
IIC or IID Avg. Engine Rust Rating, min. 7.6 7.7
1-H2 Top Groove Fill, % vol. max. 45
Weighted Total Demerits, max. 140
Ring Side Clearance Loss, in. max. 0.0005
CD 1-G2 Top Groove Fill, % vol. max. 80
Weighted Total Demerits, max. 300
Ring Side Clearance Loss, in. max. 0.0005
L-38 Bearing Weight Loss, mg. max. 50
Piston Skirt Varnish Rating, min. 9.0
CD-II I-G2 Top Groove Fill, % vol. max. 80
Weighted Total Demerits, max. 300
Ring Side Clearance Loss, in. max. 0.0005
L-38 Bearing Weight Loss, mg. max. 50
Piston Varnish Rating, min. 9.0
6V-53T Piston Area
Weighted Total Demerits, avg. max. 400
Hot Stuck Rings None
2 and 3 Ring Face Distress
avg. Demerits, max. 13
01/08 - Crankcase - 23
API Diesel Engine Performance Criteria
Test Primary Performance Criteria Limits
CE 1G2 Top Groove Fill, % vol. max. 80
Weighted Total Demerits, max. 300
Ring Side Clearance loss, in. max. 0.0005
L-38 Bearing Weight Loss, mg. max. 50
T-6 Merit Rating, min. 90
T-7 Avg. Rate of Viscosity increase
0.040
during last 50 hrs, cSt. 100°C/hr. max.
NTC-400 Candidate oil consumption second
order regression curve must fall
Oil Consumption completely below the published mean
plus one standard deviation curve for
the applicable reference oil
Camshaft Roller Follower Pin Wear
0.051 (0.002)
average, max. mm. (in).
Crown Land (Top Land) Deposits,
% area covered with heavy carbon, 25
average, max.
Piston Deposits, Third Ring Land,
total CRC demerits for all six 40
pistons, max.
01/08 - Crankcase - 24
API Diesel Engine Performance Criteria
01/08 - Crankcase - 25
API Diesel Engine Performance Criteria
Test Primary Performance Criteria Number of Test Runs
1 2 3
CG-4 1N WDN (Weighted Demerits-1N), avg. max. 286.2 311.7 323.0
TGF (Top Groove Fill), % vol.
20 23 25
avg. max.
TLHC (Top Land Heavy Carbon),
% avg. max. 3 4 5
01/08 - Crankcase - 26
API Diesel Engine Performance Criteria
Test Primary Performance Criteria Number of Test Runs
1 2 3
CH-4 1P WDP (Weighted Demerits - 1P), max, 350 378 390
TGC (Top Groove carbon), %, vol. max, 36 39 41
TLC (Top land Carbon), %, max, 40 46 49
Avg. Oil Consumption, 0-360 hours, 11.0 max./test
Final oil Consumption, 336-360 hours, 10.0 max./test
M-11 Crosshead Weight Loss, 4.5% soot, mg, max, 6.5 7.5 8.0
Sludge, min, 8.7 8.6 8.5
Differential Pressure/Oil Filter, kPa, max, 79 93 100
T-9 Avg. Liner wear, µm, max, 25.4 26.6 27.1
Top Ring Weight Loss, mg, max, 120 136 144
Increase in Lead Content, ppm, max, 25 32 36
T8-E Viscosity Increase, 3.8% soot cSt, max, 11.5 12.5 13.0
Relative Viscosity, 4.8% soot, max, 2.1 2.2 2.3
1K WDK (Weighted Demerits - 1K), max, 332 347 353
TGF (Top Groove Fill), % vol, max, 24 27 29
TLHC (Top Land Heavy Carbon), %, max, 4 5 5
Oil Consumption, g/bhp-hr, max, 0.5 0.5 0.5
Piston, Ring and Liner Scuffing, None None None
RFWT Pin Wear, mils, max, 0.30 0.33 0.36
D6984 60 h viscosity at 40˚C, increase from 10 min 295 295
295
(Sequence IIIF) sample, %, max, (MTAC) (MTAC)
or 150 150
Kinematic viscosity, % increase at 40˚C, max, 150
Sequence IIIG (MTAC) (MTAC)
D 892 (Option Foaming/Settling, mL, max,
A not allowed) Sequence I, 10/0
Sequence II, 20/0
Sequence III, 10/0
D 5800 SAE 10W-30 SAE 15W-40
or % volatility loss at 250˚C, max,
20 18
D 6417 % volatility loss at 371˚C, max, 17 15
D 6278 SAE XW-30 SAE XW-40
Kinematic viscosity after shearing, cSt min,
9.3 12.5
EOAT Aeration Volume, %, max, 8.0 8.0 8.0
Bench Copper, ppm, Increase, max, 20 20 20
Corrosion Lead, ppm, Increase, max, 120 120 120
Tin, ppm, Increase, max, 50 50 50
Copper Corrosion, ASTM D 130, max, 3 3 3
01/08 - Crankcase - 27
API Diesel Engine Performance Criteria
Test Primary Performance Criteria Number of Test Runs
1 2 3
CI-4 D6923 (1R) Weighted demerits (WDP), max 382 396 402
or Top groove carbon (TGC), demerits, max 52 57 402
Top land carbon (TLC), demerits, max 31 35 36
Initial oil consumption (IOC),
13.1 13.1 13.1
(0-252 h), g/h, average
D6681 (1P) Weighted demerits (WDP), max 350 378 390
Top groove carbon (TGC), demerits, max 36 39 41
Top land carbon (TLC), demerits, max 40 46 49
Average oil consumption, g/h (0-360 h), max 12.4 12.4 12.4
Final oil consumption, g/h (312-360 h), max 14.6 14.6 14.6
Piston, ring, and liner scuffing none none none
D6987 (T10) Merit rating, min
or 1000 1000 1000
D6987m (T12)
01/08 - Crankcase - 28
API Diesel Engine Performance Criteria
Test Primary Performance Criteria Number of Test Runs
1 2 3
CI-4 D6594 (135˚C Copper, mg/kg (ppm) increase, max 20
HTCBT) Lead, mg/kg (ppm) increase, max 120
Tin, mg/kg (ppm) increase, max 50
Copper strip rating, max 3
D6278 Kinematic viscosity after shearing, cSt, min SAE XW-30 / SAE XW-40
9.3 / 12.5
Foaming/settlng, max, mL
Sequence I 10/0
D892
Sequence II 20/0
Sequence III 10/0
Elastomer Compatibility
Limits Tensile
Elastomer Volume Change Elongation
Hardness Strength
Nitrile +5/-3 +7/-5 +10/-TMC 1006 +1-/-TMC 1006
Silicone + TMC 1006/-3 +5/-TMC 1006 +10/-45 +20/-30
Polyacrylate +5/-3 +8/-5 +18/-15 +10/-35
Fluoroelastomer +5/-2 +7/-5 +10/-TMC 1006 +10/-TMC 1006
01/08 - Crankcase - 29
API Diesel Engine Performance Criteria
Number of Test Runs
Test Primary Performance Criteria
1 2 3
CJ-4 T-12 Merit rating, min, 1000 1000 1000
ISM Merit rating, min, 1000 1000 1000
Top ring weight loss, mg, max, 100 100 100
C-13 Merit rating, min, 1000 1000 1000
Hot-stuck piston ring, none none none
D 7156 (T-11) TGA % Soot at 4.0 cSt increase, at 100˚C, min, 3.5 3.4 3.3
TGA % Soot at 12.0 cSt increase, at 100˚C min, 6.0 5.9 5.9
TGA % Soot at 15.0 cSt increase, at 100˚C min, 6.7 6.6 6.5
ISB Slider tappet weight loss, mg, average, max, 100 108 112
Cam lobe wear, µm, average, max, 55 59 61
Crosshead weight loss, mg, average, report report report
D 6750 (1N) Weighted demerits (WDN), max, 286.2 311.7 323.0
Top groove fill (TGF), %, max, 20 23 25
Top land heavy carbon (TLHC), %, max, 3 4 5
Oil consumption, g/kW-h, (0-252 h), max, 0.5 0.5 0.5
Piston, ring, and liner scuffing, none none none
Piston ring sticking, none none none
D 5966 (RFWT) Average pin wear, mils, max, 0.30 0.33 0.36
(µm, max), (7.6) (8.4) (9.1)
D 6984
Kinematic viscosity (at 40˚C) % increase, max, 275 275 (MTAC) 275 (MTAC)
( Seq, IIIF)
Or, alternately, 150 150 (MTAC) 150 (MTAC)
Kinematic viscosity (at 40˚C), % increase, max,
Sequence IIIG
D 6894 (EOAT) Aeration, volume, %, max, 8.0 8.0 (MTAC) 8.0 (MTAC)
D 4683 (High Viscosity at 150˚C, mPa-s, min,
temperature/ 3.5
High shear)
D 6594 (135˚C Copper, mg/kg (ppm) increase, max, 20
HTCBT) Lead, mg/kg (ppm) increase, max, 120
Copper strip rating, max, 3
D 7109 Kinematic viscosity after 90 pass, SAE XW-30 / SAE XW-40
shearing, cSt at 100˚C, min, 9.3 / 12.5
D 5800 (Noack) Evaporative loss at 250˚C, %, max,
13
(Viscosities other than SAE 10W-30)
Evaporative loss at 250˚C, %, max,
15
(SAE 10W-30 viscosity)
D 892 Foaming/settling, mL, max,
Sequence I 10/0
Sequence II 20/0
Sequence III 10/0
D 6896 (MRV Viscosity of the 180 h used oil drain sample
TP-1) from a T-11 test, tested at -20˚C 25,000
mPa-s, max,
If yield stress is detected, use the modified
test method (external preheat), then 25,000
measure the viscosity, mPa-s, max,
Measure the yield stress, Pa <35
01/08 - Crankcase - 30
API Diesel Engine Performance Criteria
01/08 - Crankcase - 31
ACEA 2007 Service-Fill Oils for Gasoline and Diesel Engines
Requirements Method Properties Unit Limits
A1 / A3 / A3 / A5 /
B1-04 B3-04 B4-04 B5-04
Viscosity SAE J300 No restriction except as defined by
grades Latest active shear stability and HT/HS requirements.
Manufacturers may indicate specific viscosity
issue requirements related to ambient temperature.
Shear CEC-L-14-A- 100˚C Viscosity xW-20
stability 93 or after 30 cycles stay in
ASTM D6278 grade All grades All grades All grades
mm²/s xW-30 ≥ to be stay to be stay to be stay
8.6 in grade in grade in grade
xW-40 ≥
12.0
01/08 - Crankcase - 32
ACEA 2007 Service-Fill Oils For Gasoline and Diesel Engines Engine Tests
Requirements Method Properties Units Limits
A1 / A3 / A3 / A5 /
B1 -04 B3 -04 B4 -04 B5 -04
High temperature CEC-L-88-T-02 Ring Sticking (each part), merit, max 9.0 9.0 9.0 9.0
deposits (TU5JP-L4) Piston Varnish
(6 elements, average of 4 pistons), merit, min
Ring sticking RL 216 RL 216 RL 216 RL 216
Oil thickening 72 Hour test
Absolute viscosity increase
0.8 x 0.8 x 0.8 x
at 40˚C between min and max mm2/s, max RL 216
RL 216 RL 216 RL 216
values during test,
Oil consumption, kg/test Report Report Report Report
Low ASTM D6593-00 Average engine sludge, merit, min 7.8 7.8 7.8 7.8
temperature (Sequence VG) Rocker cover sludge, merit, min 8.0 8.0 8.0 8.0
sludge (2) Under protocol Average piston skirt varnish, 7.5 7.5 7.5 7.5
merit, min
& requirements
Average engine varnish, merit, min 8.9 8.9 8.9 8.9
for API
Compression ring (hot stuck), none none none none
Oil screen clogging, %, max 20 20 20 20
Valve train CEC-L-38-A-94 Average cam wear, µm, max 10 10 10 10
scuffing wear (TU3M) Cam wear, µm, max 15 15 15 15
Pad merit (Ave. of 8 pads), merit, min 7.5 7.5 7.5 7.5
Black sludge CEC-L-53-T-95 Average engine sludge, merit, min
(M111) RL 140 RL 140 RL 140 RL 140
(2) The limits shown are based upon those applied in U.S market requirements. ACEA will continuously review the situation to ensure
that these limits are appropriate for European vehicles and lubricants.
01/08 - Crankcase - 33
ACEA 2007 Service-Fill Oils For Gasoline and Diesel Engines Engine Tests
Requirements Method Properties Units Limits
A1 / A3 / A3 / A5 /
B1 -04 B3 -04 B4 -04 B5 -04
Fuel economy (3) CEC-L-54-T-96 Fuel economy improvement vs. %, min
2.5 - - 2.5
(M111) Reference oil RL191 (15W-40),
Ring sticking and CEC-L-46-T-93 Ring sticking, merit, min RL 148 RL 148 - -
piston cleanliness (4) (VW 1.6 TC D) Piston cleanliness, merit, min RL 148 RL 148 - -
Medium temperature CEC-L-093 Absolute viscosity increase mm2/s, max 0.06 x 0.06 x 0.06 x 0.06 x
dispersivity (5) (DV4TD) at 100˚C and 6% soot, RL223 result RL223 result RL223 result RL223 result
Piston merit (6) merit, min (RL223- (RL223- (RL223- (RL223-
2.5pts) 2.5pts) 2.5pts) 2.5pts)
(3) ACEA considers the CEC-L-54-T-96 test the only valid comparator against which claims of lubricant fuel economy improvement should be made.
(4) The test according to CEC-L-78-T-99 may be run instead of CEC-L-46-T-93 for A1/B1 and A3/B3. The limits shall be as A3/B4.
(5) XUD11 BTE passing results obtained before the end of 2005 can be used instead of the DV4.
(6) Piston merit is not vet an official CEC barometer.
01/08 - Crankcase - 34
ACEA 2007 Service-Fill Oils For Gasoline and Diesel Engines
Requirements Method Properties Units Limits
A1 / A3 / A3 / A5 /
B1 -04 B3 -04 B4 -04 B5 -04
Wear, Viscosity OM602 A Average cam wear. (New tappet), µm, max 50.0 50.0 50.0 50.0
stability & Oil Viscosity increase at 40˚C, %, max 90 90 90 90
consumption (7) Bore polishing, %, max 7.0 7.0 7.0 7.0
Average cylinder wear, µm, max 20.0 20.0 20.0 20.0
Oil consumption, kg/test, max 10.0 10.0 10.0 10.0
DI Diesel Piston CEC-L-78-T-99 Piston cleanliness, merit, min - - RL 206 - 3pts RL 206
cleanliness & (VW DI) Ring sticking (Rings 1 & 2)
Ring sticking Average of all 8 rings, ASF, max - - 1.2 1.2
Max. for any 1st ring, ASF, max - - 2.5 2.5
Max. for any 2nd ring, ASF, max - - 0.0 0.0
(7) OM646LA results at an equivalent performance level can be used as soon as the test becomes avilable
as a CEC test. In the event of OM602A and OM646 are not available, ACEA will define an alternative.
01/08 - Crankcase - 35
ACEA 2007 Service-Fill Oils For Gasoline And Diesel Engines With After Treatment Devices
Requirements Method Properties Units Limits
Viscosity grades SAE J300 No restriction except as defined by shear stability and HT/HS requirements.
Latest active issue Manufacturers may indicate specific viscosity requirements related
to ambient temperature.
Shear stability CEC-L-14-A-93 100˚C Viscosity after mm2/s
or 30 cycles, stay in grade stay in grade stay in grade stay in grade
ASTM D6278
01/08 - Crankcase - 36
ACEA 2007 Service-Fill Oils For Gasoline And Diesel Engines With After Treatment Devices
Requirements Method Properties Units Limits
(1) Use either complete Daimler Chrysler requirements (VDA 675301, 7 days +/- 2h, 4 materials (NBR: NBR34 DIN 53538 T3 (100˚C +/-2˚C ); FPM: AK6 (150˚C +/- 2˚C);
ACM: E7503 (150˚C +/-2˚C); AEM: D 8948/200.1 (150˚C +/-2˚C)) + RE3, or complete requirements as above + DC requirements for AEM
01/08 - Crankcase - 37
ACEA 2007 Service-Fill Oils For Gasoline And Diesel Engines With After Treatment Devices
Requirements Method Properties Units Limits
High CEC-L-88-T-02 Ring sticking (each part), merit, min 9.0 9.0 9.0 9.0
temperature (TU5JP-L4) Piston varnish, merit, min
deposits 72 Hour test RL 216 RL 216 RL 216 RL 216
(6 elements, average of 4 pistons),
2
Absolute viscosity increase at mm /s, max
Ring sticking 0.8 x 0.8 x 0.8 x 0.8 x
40˚C between min and max
Oil thickening RL 216 RL 216 RL 216 RL 216
values during test,
(2) T he limits shown are based upon those applied in U.S. market requirements. ACEA will continuously review the situation to ensure that these limits
are appropriate for European vehicles and lubricants.
(3) ACEA considers the CEC-L-54-T-96 test the only valid comparator against which claims of lubricant fuel economy improvement should be made.
01/08 - Crankcase - 38
ACEA 2007 Service-Fill Oils For Gasoline And Diesel Engines With After Treatment Devices
Requirements Method Properties Units Limits
Medium temperature CEC-L-093 Absolute viscosity increase mm2/s, max 0.60 x 0.60 x 0.60 x 0.60 x
dispersivity (DV4TD) at 100˚C and 6% soot RL223 result RL223 result RL223 result RL223 result
Piston merit (4) merit, min (RL223 - (RL223 - (RL223 - (RL223 -
2.5pts) 2.5pts) 2.5pts) 2.5pts)
DI diesel CEC-L-78-T-99 Piston cleanliness merit, min RL206 RL206 RL206 RL206
(VW DI)
Piston Ring sticking (Rings 1 & 2)
cleanliness
Average of all 8 rings (ASF), max 1.2 1.2 1.2 1.2
& Ring sticking
Max. for any 1st ring (ASF), max 2.5 2.5 2.5 2.5
Max. for any 2nd ring (ASF), max 0.0 0.0 0.0 0.0
Wear, OM602A Cam wear average µm, max 50.0 50.0 45.0 45.0
Viscosity stability & Viscosity increase @ 40˚C %, max 90 90 70.0 70.0
Oil consumption (5) Bore polishing 7.0 7.0 4.5 4.5
%, max
Average Cylinder wear µm, max 20.0 20.0 15.0 15.0
Oil consumption kg/test, max 10.0 10.0 10.0 10.0
01/08 - Crankcase - 39
ACEA 2007 Service-Fill Oils For Heavy Duty Diesel Engines
Requirements Method Properties Units Limits
01/08 - Crankcase - 40
ACEA 2007 Service-Fill Oils For Heavy Duty Diesel Engines
Requirements Method Properties Units Limits
01/08 - Crankcase - 41
ACEA 2007 Service-Fill Oils For Heavy Duty Diesel Engines
Requirements Method Properties Units Limits
Wear (3) CEC-L-51-A-97 Cam wear, µm, max 50.0 50.0 50.0 50.0
(OM602A) Viscosity increase at 40˚C, %, max - 90 90 90
Bore polishing, %, max - 7.0 7.0 7.0
Cylinder wear, µm, max - 20.0 20.0 20.0
Oil consumption, kg/test, max - 10 10 10
Soot in oil (4) ASTM D5967 Test duration: (hours) - 300 300 300
(Mack T-8E) Relative viscosity at 1 test/2 - 4.8% soot
ASTM D4485 test/3 test average, mm2/s, max - 2.1/2.2/2.3 2.1/2.2/2.3 2.1/2.2/2.3
(Mack T-8)
Relative viscosity at 1 test/2 - 3.8% soot
test/3 test average, mm2/s, max - 11.5/12.5/13.0 11.5/12.5/13.0 11.5/12.5/13.0
Filter plugging, Diff, pressure kPa, max - 138 138 138
Oil consumption, g/kWh, max - 0.304 0.304 0.304
Bore polishing CEC L-52-T-97 Bore polishing, %, max - 2.0 2.0 2.0
Piston cleanliness (OM441LA) Piston cleanliness, merit, max - 40.0 40.0 40.0
Turbocharger - 4 4 4
Boost pressure loss at 400 hrs, %, max
deposits (5)
Oil consumption, kg/test, max - 40 40 40
(2) Results from a CEC-L-52-T-97 (OM441LA) test as part of a Daimler Chrysler sheet 228.1 approval can be used as an alternative. Only tests according to CEC-L-52-T-97 are acceptable.
(3) OM646LA results at an equivalent performance level can be used as soon as the test becomes available as a CEC test. In the event the OM602A and the OM646 are not available, then
ACEA will define an alternative.
(4) Mack T11 (ASTM D7156) results obtained as part of an API CI-4, CI-4 plus or API CJ-4 approval program, can be used in place of Mack T8E.
(5) OM501LA results at an equivalent performance level can be used as soon as the test becomes available as a CEC test.
01/08 - Crankcase - 42
ACEA 2007 Service-Fill Oils For Heavy Duty Diesel Engines
Requirements Method Properties Units Limits
(6) Results from Cummins a M11 HST (ASTM D6838) at API CH-4 or M11 EGR test (ASTM D6975) at API CI-4 or CI-4. Plus can be used in place of the Cummins ISM test.
(7) Mack T12 results can be used in place of Mack T10. In this case the merit scale for CI-4 plus approvals must be applied to the Mack T12 results. Maximum allowable values
for the Mack T12 test are given in parentheses.
01/08 - Crankcase - 43
US Military Specifications: Engine Test Requirements
MIL-L 46152D 46152E 2104E
L-38 Bearing Weight Loss, mg. max. 40 40 50
IID Avg. Rust, min. 8.5 8.5 8.1
Stuck Lifters None None None
IIIE Viscosity Increase 64 hrs. 40°C. %. max. 375 375 -
Piston Varnish, min. 8.9 8.9 -
Oil Ring Land Varnish, min. 3.5 3.5 -
Sludge, min. 9.2 9.2 -
Ring Sticking None None -
Lifter Sticking None None -
Cam or Lifter Scuffing None None None
Cam plus Lifter Wear, avg. max. μm. 30 30 64
max. μm. 64 64 178
VE Avg. Sludge, min. 9.0 9.0 8.5
Rocker Cover Sludge, min. 7.0 7.0 6.5
Avg. Varnish, min. 5.0 5.0 4.2
Piston Varnish, min. 6.5 6.5 6.0
Oil Ring Clogging, %. max. 15 15 15
Oil Screen Plugging, %. max. 20 20 23
Ring Sticking None None None
Cam Wear, avg. max. μm. 127 127 203
max. μm. 381 381 457
1-H2 TGF, vol. %. max. 45 45 -
WTD, max. 140 140 -
1-G2 TGF, vol. %. max. - - 80
WTD, max. - - 300
01/08 - Crankcase - 44
Additional Test Requirements for MIL-L-2104E
01/08 - Crankcase - 45
MIL-L-2104F Engine Test Requirements
01/08 - Crankcase - 46
MIL-L-2104F Transmission Test Requirements
Graphite Paper
5500 0 -5,000 5,000 - 10,000
Allison C-4 Slip Time at Cycles, secs. max. 0.74 0.67 0.56
Friction Mid-Point Co-efficient of Friction at Cycles min. 0.097 0.066 0.086
Seals Total Immersion (Buna N)
Volume change, % 0 to +5
Hardness change, pts. -5 to +5
Dip Cycle (Polyacrylate)
Volume change, % 0 to +10
Hardness change, pts. 0 to +5
Tip Cycle (Silicone)
Volume change, % 0 to +5
Hardness change, pts. -10 to 0
Total Immersion (Flouroelastomer)
Volume change, % 0 to +4
Hardness change, pts. -4 to +4
01/08 - Crankcase - 47
JASO 2007 Diesel Engine Oil Standards
Units Performance Criteria
DH-1-05 DH-2-05 DL-1-05
Viscosity Grade - - XW-30,XW-20
Jaso Hot Tube Merit
Test Hot Surface Rating
Deposit Control @ 280˚C, 7.0 min. 7.0 min. 7.0 min.
01/08 - Crankcase - 48
JASO 2007 Diesel Engine Oil Standards
Units Performance Criteria
DH-1-05 DH-2-05 DL-1-05
Seal RE3 Hardness Change Point -25 to +1 -25 to +1 -25 to +1
Compatibility (Silicon) Tensile Strength Rate %
-45 to +10 -45 to +10 -45 to +10
of Change
Elongation rate of Change % -20 to +10 -20 to +10 -20 to +10
Volume rate of Change % -1 to +30 -1 to +30 -1 to +30
RE4 Hardness Change Point -5 to +5 -5 to +5 -5 to +5
(Nitrile) Tensile Strength Rate of %
-20 to +20 -20 to +20 -20 to +20
Change
Elongation rate of Change % -50 to +10 -50 to +10 -50 to +10
Volume rate of Change % -5 to +5 -5 to +5 -5 to +5
AEM Hardness Change Point Per Per Per
(Ethylene Tensile Strength Rate of % agreement agreement agreement
Acrylic) Change between between between
Elongation rate of Change % concerned concerned concerned
parties parties parties
Volume rate of Change %
Nissan TD25 TGF (Top Groove Fill) vol % 60.0 60.0 60.0
(M336) Piston Ring Stickings All free All free All free
Piston
Deposits on Ring Lands Merit
Detergency Report Report Report
Rating
Mitsubishi Average Cam Diameter Loss µm,
4D34T4 (Normalised at 4.5 mass % Carbon max 95.0 95.0 95.0
Valve Train Residue Increase),
Wear Protection
Maximum Cam diameter Loss µm,
(M354)
(Normalised at 4.5 mass % max 210 210 210
Carbon Residue Increase),
01/08 - Crankcase - 49
Global Engine Oil Service Specification DHD-1 Laboratory Tests
Test Performance Criteria Limits
Corrosion Bench Test Used Oil Element Content Copper 20,
above Baseline, ppm, max. Lead 120, Tin 50
Elastomer Variation after 7 days fresh oil, Elastomer Type
Compatibility * No pre-aging RE 1 RE 2 RE 3 RE 4
Hardness DIDC, points, max. -1/+5 -5/+5 -25/+1 -5/+5
Tensile Strength, %. max. -50/+10 -15/+10 -45/+1 -20/+10
Elongation rupture, %. max. -60/+10 -35/+10 -20/+10 -50/+10
Volume variation, %. max. -1/+5 -5/+5 -1/+30 -5/+5
Foaming Tendency Tendency / Stability, ml. max. Sequence I (24°C) 10 - nil
after 1 min. settling Sequence II (94°C) 50 - nil
Sequence III (24°C) 10 - nil
Foaming - High Tendency / Stability, ml. max.
Sequence IV (150°C) 200 - 50
Temperature after 1 min. settling
PDSC Oxid. Induction Time, min. min. 35
Shear Stability Viscosity after 30 Cycles,
Stay-in-grade
Bosch Injector Test measured at 100°C.
Sulphated Ash Mass %. max. 2.0
HT/HS Viscosity
Tapered Bearing High Tempeature / High Shear Rate 35
Simulator / Ravenfield Viscosity, cP. min.
NOACK Volatility % Mass Loss, max. 15
Note:
(*) The Elastomer Compatability Limits are those stated in ACEA 1999 European Oil Sequences
and apply to the elastomer batches available at that time. Consult the most recent ACEA Oil Sequence
publication for the information on the limits with more recent elastomer batches.
01/08 - Crankcase - 50
Global Engine Oil Service Specification DHD-1 Engine Tests
Test Performance Criteria Limits
Caterpillar 1R ( )1
Weighted Demerits (WDR), max. 397 416 440
Total Groove Carbon, %. max. 40 42 44
Top Land Carbon, %. max. 37 42 46
Oil Consumption g./hr. Initial max./Final max. 13.1 / 1.5 X Initial
Cummins M11 HST (3) Oil Filter Diff. Press. kPa. max. 79 93 100
Eng. Sludge, CEC Merits, min. 8.7 8.6 8.5
Rocker Pad Average Weight Loss,
6.5 7.5 8.0
Normalized to 4.5% soot mg. max.
Mack T-9 (4) Used Oil Lead, ppm. max. 15 ( )
2
01/08 - Crankcase - 51
Two-Stroke Classification: API TC
Engine Parameter Limits
API TC (CEC TSC-3) Yamaha CE 50S Tightening, Mean Torque Drop ≤ Ref. Oil
Yamaha CE 50S Pre-ignition, occurences 1 max. in 50 hr. test
Yamaha 350 M2 Piston Varnish
Ring Sticking
Better than or equal to reference oil
Piston Deposits
Piston Scuffing
Notes:
TA (TSC-1) not released as a full specification, but the test methods are recognised by ASTM as valid for assessing the capabilities of two stroke oils.
TB (TSC-2) not released as a full specification due to the withdrawal of the supporting OEM. No new work is in progress.
01/08 - Crankcase - 52
Two-Stroke Classification: ISO/JASO
ISO - EGB EGC EGD
JASO FA FB FC -
Lubricity 90 min. 95 min. 95 min. 95 min.
Torque Index 98 min. 98 min. 98 min. 98 min.
Detergency 80 min. 85 min. 95 min. 125 min.
Piston Skirt Deposits - 85 min. 90 min. 95 min.
Exhaust Smoke 40 min. 45 min. 85 min. 85 min.
Exhaust Blocking 30 min. 45 min. 90 min. 90 min.
Notes:
All limits are indices relative to reference oil, JATRE-1
Test Engines
Honda DIO AF27 Lubricity
Torque Index
Detergency, Piston Skirt Varnish
Suzuki SX800R Exhaust Smoke
Exhaust Blocking
01/08 - Crankcase - 53
Two-Stroke Classification: TISI 1040
01/08 - Crankcase - 54
Two-Stroke Classification: NMMA TC-W3
Test Parameter Limits
ASTM Lubricity Torque Drop, average ≤ Reference oil
NMMA Detergency Top Ring Sticking, average Max. 0.6 points below reference oil
Piston Deposits, average Max. 0.6 points below reference oil
Spark Plug Fouling, occurrences Max. 1 more than reference oil
Exhaust Port Blocking Max. 10% greater than reference oil
Pre-ignition, occurrences ≤ Reference oil
ASTM Pre-ignition Pre-ignition (major), occurrences Max. of 1 in 100 hr test
NMMA Rust Test - Equal or better than reference oil
SAE Miscibility Fluidity - Category 3 or 4 of SAE J1536
NMMA Filterability Decrease in Flow Rate, % 20 max.
Note:
This specification was introduced in April 1992 to replace NMMA TC-W2 and offers improved ring-stick protection and lubricity, with higher anti-scuff performance.
01/08 - Crankcase - 55
Four-Stroke Classification: JASO T903, 2006
Requirements Performance Criteria Test Procedure
Sulphated Ash, mass %, max 1.2 JIS K 2272
Phosphorus Content mass %, min 0.08 0.12 JPI-5S-38
Evaporative Loss mass %, max 20 JPI-5S-41
Sequence I 10/0 JIS K 2518
Foaming Tendency
Sequence II ml 50/0
(foaming/settling)
Sequence III 10/0
xW-30: 9.0 JPI-5S-29 (1)
Shear Stability xW-40: 12.0
(Kinematic Viscosity (100˚C) mm2/s, xW-50: 15.0
min after test) Other grades:
stay in grade
High temperature high shear viscosity mPa2s 2.9 min JPI-5S-36
(1) Test shall be conducted by diesel injector method under the standard test conditions (30 cycles)
The JASO T903 specifications were implemented to ensure oils with the correct viscosity and friction characteristics were
available in the market for 4 stroke motorcycles. These oils must meet a minimum requirement of API SG, SH. SJ, SL,
SM or ILSAC GF-2, GF-3 or ACEA A1/B1, A3/B3, A5/B5, C2, C3 and must meet these physical/chemical requirements in
addition to the JASO T904: 2006 friction test.
01/08 - Crankcase - 56
Four-Stroke Classification NMMA FCW
Engine Tests Test Method Result
-Cam lobes
-Cam caps
-Cam journals
-Cam bearings
-Piston rings
-Piston
-Con rod bearing
-Cylinder bore
-Main bearing
-Crank journals
-Fuel pump lobe, reference only
NMMA developed the FCW specification for four-stroke outboard engines, in response to the increasing need for a
dedicated lubricant for this application, as opposed to the use of a traditional passenger car engine oil. Oils seeking
NMMA FCW approval must meet a minimum of API SG in addition to responsding to the corrosion inhibition and
anti-wear requirements of an outboard engine.
01/08 - Crankcase - 57
OEM Specification: Mercedes-Benz Sheets for Passenger Car Engine Oils
Sheet Number 229.1 229.3 229.31 229.5 229.51
ACEA Any valid Ax, Bx, or Cx category
Viscosity Grades, SAE (1) 5W-30, 5W-40, 5W-50,
10W-30, 10W-40, 10W-50, 0W-,5W-, 0W-,5W-, 0W-,5W-, 0W-,5W-,
10W-60, 15W-40, 15W-50, 10W-x 10W-x 10W-x 10W-x
20W-40, 20W-50
Laboratory Tests,
Sulfated Ash (DIN 51575 or ASTM D874) % b.w, max, 1.5 1.5 0.8 1.5 0.8
TBN (ISO 3771 or ASTM D2896 fresh oil), mgKOH/g, min, 6.0 7.0 6.0 8.0 6.0
TBN (ASTM D4739 fresh oil) mgKOH/g, min, Rate & Rate & Rate & Rate & Rate &
Report Report Report Report Report
Pour point (ISO 3016 or ASTM D97) ˚C, max, -27 -27 -27 -27 -27
Evaporative loss CEC L-40-A-93, ASTM 5800, Noack, %, max, 13.0 13.0 12.0 10.0 10.0
Viscosity @high temp./high shear rate (CEC L-36-A-97), mPa.s, min, 3.5 3.5 3.5 3.5 3.5
Sulfur (DIN EN ISO 14596 or ASTM 2622), % b.w, max, Rate
0.50 0.20 0.50 0.20
& Report
Phosphorous (DIN 51363-2/-3 or ASTM 4951), % b.w, max, Rate Rate
0.08 0.11 0.08
& Report & Report
Chlorine (DIN 51577-2/-3), % b.w, max, Rate
0.0150 0.0150 0.0150 0.0150
& Report
01/08 - Crankcase - 58
OEM Specification: Mercedes-Benz Sheets for Passenger Car Engine Oils
Engine Tests
M 271 (MB DL, Sludge) (2) (3)
Engine sludge avg. (with fuel batch 1), merit, min 8.5 8.8 8.8 9.1 9.1
M 271 (MB DL, Wear 250 h) (2) (4)
Cam wear inlet / outlet valve (avg. max wear 8 cams), µm, max 5.0 / 5.0 5.0 / 5.0 5.0 / 5.0 5.0 / 5.0 5.0 / 5.0
Piston wear radial @ ring 1 / ring 2 avg, µm, max 5.0 / 12.0 5.0 / 12.0 5.0 / 12.0 5.0 / 12.0 5.0 / 12.0
Piston wear axial @ ring 1 / groove 1 avg, µm, max 5.0 / 15.0 5.0 / 15.0 5.0 / 15.0 5.0 / 15.0 5.0 / 15.0
Ring Sticking, max none none none none none
Bore polishing (9mm) - max. value of 4 cylinders, %, max 3.5 3.5 3.5 3.5 3.5
Main bearing wear, avg, max, µm 1.5 / 3.5 1.5 / 3.5 1.5 / 3.5 1.5 / 3.5 1.5 / 3.5
Conrod Bearing wear, avg, max, µm 1.5 / 3.5 1.5 / 3.5 1.5 / 3.5 1.5 / 3.5 1.5 / 3.5
Timing chain wear (elongation), %, max 0.25 0.25 0.25 0.25 0.25
Timing chain wear (single chain link), %, max 1.0 1.0 1.0 1.0 1.0
M 111 (CEC L-54-T-96)
Fuel economy improvement vs. RL 191 (15W-40), %, min - 1.0 1.0 1.7 1.7
01/08 - Crankcase - 59
OEM Specification: Mercedes-Benz Sheets for Passenger Car Engine Oils
Sheet Number 229.1 229.3 229.31 229.5 229.51
01/08 - Crankcase - 60
OEM Specification: Mercedes-Benz Sheets for Passenger Car Engine Oils
Sheet Number 229.1 229.3 229.31 229.5 229.51
2
( ) Rerating by MB, department EP/MOR for all related engine parts and,
(3) M271 sludge test is the successor test for the M111 sludge test is mandatory for all sheets after 1.1.2006. M111 sludge is not accepted anymore.
(4) M271 wear test for all sheets 229.1/.3/.31/.5/.51 is mandatory after 1.1.2005. Verification for all sheets 229.x until 1.1.2006.
(5) For sheets 229.31 and 229.51 both tests OM 611 DE 22 LA and OM 602 A have to be run as long as the OM 602 A test is available. Both tests will be replaced by new OM 646 DE 22 LA
CEC test. For all other MB sheets and after 01/01/2004 the OM 602 A test will not be mandatory anymore.
01/08 - Crankcase - 61
OEM Specification: Volkswagen
Requirements VW 501.011 VW 502.001 VW 504.001 VW 505.001 VW 505.011 VW 507.001
01/08 - Crankcase - 63
OEM Specification: Volkswagen
Requirements VW 501.011 VW 502.001 VW 504.001 VW 505.001 VW 505.011 VW 507.001
(2) Possible approval combinations are VW 501.01/505.00, VW 505.00, VW 502.00/505.00, VW 502.00/505.01, VW 504.00/507.00
(2) Discuss with Volkswagen
(3) Needs to be discussed with VW on a case by case basis
01/08 - Crankcase - 64
OEM Specification: Mercedes-Benz Sheets For Heavy Duty Diesel Engine Oils
Sheet Number 228.0/.1 228.2/.3 228.31 228.5 228.51
01/08 - Crankcase - 65
OEM Specification: Mercedes-Benz sheets For Heavy Duty Diesel Engine Oils
Sheet Number 228.0/.1 228.2/.3 228.31 228.5 228.51
01/08 - Crankcase - 66
OEM Specification: Mercedes-Benz Sheets for Heavy Duty Diesel Engine Oils
Piston cleanliness (avg. 4 pistons), merit, min 23.0 25.0 25.0 27.0 27.0
Ring sticking, (ASF 2.5, max) no no no no no
Engine sludge avg, merit, min 8.0 8.5 8.5 9.0 9.0
Viscosity increase at 100˚C - target value, max, % 100 100 100 90 90
Oil consumption - target value, max, g/test 6000 6000 6000 6000 6000
Bore polishing (13mm) - max. value of 4 cyl, max, % 4.0 3.5 3.5 3.0 3.0
Timing chain wear (elongation) - target value, max, % 0.4 0.4 0.4 0.4 0.4
Cylinder wear (avg. 4 cylinder), max, µm 7.0 7.0 7.0 5.2 5.2
Cam wear. inlet / outlet value (avg. max. wear 8 cams), max, µm 140 / 155 140 / 155 140 / 155 120 / 140 120 / 140
Bearing wear. main / con rod bearing max, µm 2.1 / 2.1 2.1 / 2.1 2.1 / 2.1 2.1 / 2.1 2.1 / 2.1
Piston ring wear axial @ ring 1 / ring 2 / ring 3 max, µm 10.4 / 4.2 / 2.4 10.4 / 4.2 / 2.4 10.4 / 4.2 / 2.4 8.7 / 2.8 / 2.4 8.7 / 2.8 / 2.4
Piston ring wear axial @ ring 1 / ring 2 / ring 3 max, µm 5.6 / 8.4 / 8.0 5.6 / 8.4 / 8.0 5.6 / 8.4 / 8.0 5.6 / 8.4 / 8.0 5.6 / 8.4 / 8.0
OM 441 LA Euro 2 (CEC L-52-T-97 (3) (4)
Engine sludge avg, min, merit 9.0 9.0 9.0 9.0 9.0
Piston cleanliness, min, merit 20.0 25.0 25.0 40.0 40.0
General engine deposits, max, demerit 3.0 3.0 3.0 3.0 3.0
Wear rating avg, max, demerit 2.5 2.5 2.5 2.5 2.5
Bore polishing, max, % 3.0 2.0 2.0 2.0 2.0
Cylinder wear avg, max, µm 0.008 0.008 0.008 0.008 0.008
Ring sticking 2. piston rings, max, ASF 1.0 1.0 1.0 1.0 1.0
Specific oil consumption, max, g/h 100.0 100.0 100.0 100.0 100.0
Boost pressure loss at 400 hours, max, % Rate & Report (5) 9.0 (5) 9.0 (5) 4.0 (5) 4.0 (5)
Mack T-12 EGR (6)
Mack Merit Rating, min, merit - - 1000 -
01/08 - Crankcase - 67
OEM Specification: Mercedes-Benz Sheets for Heavy Duty Diesel Engine Oils
01/08 - Crankcase - 68
OEM Specification: Mercedes-Benz Sheets for Heavy Duty Diesel Engine Oils
01/08 - Crankcase - 69
OEM Specifications: MAN 270, MAN 271
Additional Notes
1. MWM ‘B’ tests are no longer required or accepted for new oil approvals.
Approvals based on MWM ‘B’ tests invalid after 31 May 1996.
01/08 Crankcase - 70
OEM Specifications: MAN 270, MAN 271
01/08 - Crankcase - 71
OEM Specification: MAN M 3275
01/08 - Crankcase - 72
OEM Specification: MAN M 3277
01/08 - Crankcase - 73
OEM Specification: MAN M 3477
Notes:
(1) Deposits on intercooler or turbocharger with individual rating of 5 will not be accepted.
(2) Test run to be aborted if oil consumption exceeds 9.5 kg oil during the first 100 hrs.
01/08 - Crankcase - 74
OEM Specification: Volvo Drain Specification (VDS)
Field Trial Minimum of three trucks required equipped with Volvo 12 litre intercooled
Requirements engine. Field trial shall run for minimum 300,000 km. with 50,000 km. oil
and filter changes. Test vehicles should be run on fuel with max. 0.7%
by weight sulphur. Oil samples taken after 15,000, 30,000 and 50,000 km.
of the change interval are tested for viscosity at 100°C (ASTM D445).
The values must not be less than:
TBN (ASTM D2896) value must not be less than 50% of the fresh oil
value. Wear rate must not increase during the test. Oil consumption
must not increase during the test. Bore polishing to be 300 cm2 max.
for the entire engine (100 cm2 max. for any individual liner).
01/08 Crankcase - 75
OEM Specification: Volvo Drain Specification - 2 (VDS-2)
VDS-2 is the oil quality intended for Volvo Truck engines meeting the 1996
European (Euro 2) emission requirements.
Field Test Field test to be run for minimum of 300,000 km. with 60,000 km.
oil drain intervals.
Oil samples are taken after 15,000, 30,000, 45,000 and 60,000 km. of the
drain interval and checked with respect to:
In addition, oil and fuel consumption are measured during the test,
oil consumption must not increase.
Inspection Upon completion of the field test, the following engine components
and Evaluation are inspected: Pistons, Piston rings, Cylinder liners, Tappets, Camshaft,
Rocker arms, Valves, Bearings. Cleanliness of covers and oil sump also
inspected.
01/08 Crankcase - 76
OEM Specification: Volvo Drain Specification - 3 (VDS-3)
VDS-3 is the oil quality intended for Volvo Truck Euro 3 engines.
Engine: D12C (any version > 400 hp) fitted to FH12 or FM12 trucks.
Field Test: European Long Haul Service only, two trucks minimum.
Test Length GVW up to 44t: 3 x 100,000 km oil drains with oil samples
and Drain taken at 0, 25,000, 50,000, 75,000 and 100,000 km.
Intervals: GVW over 44t: 4 x 75,000 km oil drains with oil samples
taken at 0, 25,000, 50,000 and 75,000 km.
For new VDS-3 trials to start - Mack EO-M+ limits in the Mack T9.
Engine Test The Volvo D12D engine test can now be run, in place of field trials to
Alternative: qualify an oil against the VDS-2 and VDS-3 specifications. The limits
are similar, but VDS-3 requires a merit rating of 1250 in the Mack T10
engine test.
Criteria
VDS-2 VDS-3
Piston cleanliness points ≥ 40 ≥ 40
Ring riding % Max. 50 Max. 50
Oil Consumption
(total and final 100h) g/h Max. 35 Max. 35
Bore Polish
2
(based on OM441LA Procedure) cm Max. 170 Max. 170
Other needed criteria - ACEA C7 ACEA C7 + Merit
of 1250 in Mack T10
01/08 Crankcase - 77
OEM Specification: Volvo Drain Specification-4 (VDS-4)
Requirements Limits
01/08 - Crankcase - 78
OEM Specification: Volvo Drain Specification-4 (VDS-4)
Requirements Limits
01/08 - Crankcase - 79
OEM Specification: Volvo Drain Specification-4 (VDS-4)
Requirements Limits
01/08 - Crankcase - 80
OEM Specification: Volvo Drain Specification-4 (VDS-4)
Requirements Limits
01/08 - Crankcase - 81
OEM Category: MTU MTL 5044
Monograde Multigrade
Oil Category 1 to 3 3.1
Viscosity grade 5W-40
5W-3
SAE 30 SAE 40 10W-40 10W-40
10W-30
15W-40
Appearance Clear & free from insoluble material
Kinematic viscosity @ 100˚C mm2s-1 9.3-12.5 12.5-16.3 9.3-12.5 12.5-16.3 12.5-16.3
Kinematic viscosity @ 100˚C, mm2s-1
- - 9.3 12.5 12.5
after shearing, min
Flash point, COC, min ˚C 225 225 225 225 225
Noack volatility, max %wt 10 10 13 13 13
Sulphated ash %wt 1.0-2.0 1.0-2.0 1.0-2.0 1.0-2.0 <1.0
TBN, min mgKOH/g 8 8 8 8 8
Chlorine, max ppm 150 150 150 150 50
Zinc, min %wt 0.035 0.035 0.035 0.035 0.035
Elastomer compatibility
SRE-NBR 28 Volume change % 0 to +10
Shore A hardness
0 to +10
change
Tensile strength %
max. -20
change
Elongation rupture %
max. -35
change
FKM-AK6 Volume change % 0 to +5
Shore A hardness
-5 to +5
change
Tensile strength %
max. -50
change
Elongation rupture %
max. -55
change
FZG rig Test load
min. 11
stage
Air absorbtion and release capability Tested by MTU
Foaming test / at 150˚C ml Max. 200/50
MTU deposit test mg - max. 120
01/08 - Crankcase - 82
OEM Specification: MTU MTL 5044
Engine Test OM 364 LA 1) OM 441 LA 1) OM 611
CEC L-42-T-99 CEC L-52-T-97 (MB Dauerlauf, 300h)
Oil Category 1 1 2 3/3.1 1 2 3/3.1
Bore polishing, max 3.5 3.0 2.0 2.0 4.0 3.5 3.0
Piaton cleanliness, min 40 20 25 40 23 25 27
Cylinder wear, avg, µm, max 3.5 8.00 8.0 8.0 7.0 7.0 5.2
Cam wear, avg, µm, max 140 (2) 140 (2) 120 (2)
- - - -
155 (3) 155 (3) 140 (3)
Engine sludge, avg, min, merit 9.4 9.0 9.0 9.0 8.0 8.5 9.0
Oil consumption, max, kg/test 16 100g/h 100g/h 100g/h 6 6 6
Viscosity rating, max, % - - - report - - -
Wear rating, max, merit - 2.5 2.5 2.5 - - -
General engine deposits, max, merit - 3.0 3.0 3.0 - - -
Oildrain interval, hrs - 200 400 400 - - -
01/08 - Crankcase - 83
OEM Specification: Scania LDF-2
Test oil sulphur and Phosphorous contents according ASTM D5185 have
to be reported.
Valve head deposit limits according CRC MANUAL No 20 has been raised
from 7 to 8
01/08 Crankcase - 84
OEM Specification: Caterpillar
01/08 - Crankcase - 85
OEM Specification: Caterpillar
(1) For Cat ECF-1-a run either, Mack T9, Mack T10, or Mack 12
For Cat ECF-2 run either, Mack T11 or Mack T12
01/08 - Crankcase - 86
OEM Specification: Caterpillar
Engine Tests
API CI-4, CI-4 +
API CH-4 Only CJ-4
CJ-4 Acceptable
Cummins ISM EGR Use if CJ-4
Cummins Merit Rating, min - - 1000
Top Ring Wt. Loss, mg max - - 100
Crosshead Wear. Loss, mg max - 7.5 / 7.8 / 7.9 -
OFDP @ 150 hrs, kPa max - 55 / 67 / 74 -
Avg. Engine Sludge, merit min - 8.1 / 8.0 / 8.0 -
Cummins M-11 (D6838)
Crosshead Wt. Loss, mg, max 6.5 / 7.5 / 8.0 - -
OFDP, kPa, max 79 / 93 / 100 - -
Sludge rating, merits, min 8.7 / 8.6 / 8.5 - -
Cummins M-11 EGR(2)
Avg Crosshead Wt. Loss, mg, max - 20.0 / 21.8 / 22.6 -
Avg Top Ring Wt. Loss, mg, max - report -
OFDP at 250hr, kPa, max - 275 / 320 / 341 -
Avg Engine Sludge rating, merits at EOT, min - 7.8 / 7.6 / 7.5 -
Cummins ISB
Avg. Slider Tappet Wt. Loss, mg, max - - 100 / 108 / 112
Avg. Cam Lobe Wear, um. Max - - 55 / 59 / 112
Avg. Crosshead Wt. Loss, mg max - - Report
Caterpillar C13
Caterpillar Merit Rating, min - 1000 1000
Hot stuck piston ring - None None
Caterpillar 1R(3)
Weighted Total Demerits, max - 382 / 396 / 402 -
Top Grove Carbon, Demerits, max - 52 / 57 / 59 -
Top Land Carbon , Demerits, max - 31 / 35 / 36 -
Initial Oil Consumption, g/h, max - 13.1 / 13.1 / 13.1 -
Final Oil Consumption, g/h, max - I.O.C. + 1.8 -
Piston ring & liner scuffing, ring sticking - None -
Caterpillar 1P (D6681) -
Weighted Total Demerits, max 350 / 378 / 390 - -
Top Groove Carbon, %, max 36 / 39 / 41 - -
Top Land Carbon, %, max 40 / 46 / 49 - -
Avg. Oil Consumption, g/hr, max 12.4 / 12.4 / 12.4 - -
Final Oil Consumption, g/hr, max 14.6 / 14.6 / 14.6 - -
Piston ring and liner scuffing None - -
01/08 - Crankcase - 87
OEM Specification: Caterpillar
Caterpillar 1N
Weighted Demerits, max - 286.2 / 311.7 / 323.0 286.2 / 311.7 / 323.0
Top Grove Fill, % max - 20 / 23 / 25 20 / 23 / 25
Top Land Heavy Carbon, % max - 3/4/5 3/4/5
Oil Consumption, g/Kw-h max) - 0.5 / 0.5 / 0.5 0.5 / 0.5 / 0.5
Piston/ring/liner scuffing - None None
Piston ring sticking - None None
Caterpillar 1K
Weighted total demerits, max 332 / 347 / 353 332 / 347 / 353 -
Top Groove Fill, %, max 24 / 27 / 29 24 / 27 / 29 -
Top Land Heavy Carbon, % max 4/5/5 4/5/5 -
Avg Oil Consumption, g/bhp-hr, max 0.5 / 0.5 / 0.5 0.5 / 0.5 / 0.5 -
Piston ring and liner None None -
Sequence IIIF (ASTM D 6984)
EOT KV % Increase @ 40C, max - 275 (MTAC) 275 (MTAC)
Viscosity Increase @ 60 hrs, % max 295 (MTAC) - -
Sequence IIIG (D7320)(4)
EOT KV % Increased @ 40C, max 150 (MTAC) 150 (MTAC) 150 (MTAC)
RFWT (D 5596)
Avg. pin wear, mils max. - 0.3 / 0.33 / 0.36 0.3 / 0.33 / 0.36
EOAT (D 6894)
Oil aeration volume, % max 8.0 (MTAC) 8.0 (MTAC) 8.0 (MTAC)
(4) For Cat ECF-1-a, ECF-2 & ECF-3 run Sequence IIIF or Sequence IIIG
(5) For Cat ECF-2 run Cat IN or Cat 1K
01/08 - Crankcase - 88
OEM Specification: Cummins
Cummins 20078 Cummins 20081
Bench Tests
CI-4 / CI-4 + CJ-4
SAE J300, latest active SAE J300, latest active
SAE Grade
issue issue
Sulfated Ash, (D874) wt %, max 1.85 1.00 / 1.02 / 1.03
TBN, mg KOH/g, m 10 Report
Noack, (D5800) %, max 15 13:xW40, 15:xW30
HTHS Viscosity, (D4683) mPa.s, min 3.5 3.5
Sulfur, wt, %, max - 0.4
Phosphorus, wt %, max - 0.12
Gelation Index (D5133), max 12 -
Mack T-11A 180 hr Used Oil MRV, mPa.s, max - 18,000
Mack T-11A 180hr Used Oil Yield Stress, max - 35
Mack T-10A 75hr Used Oil MRV, mPa.s, max 25,000 -
Mack T-10A 75hr Used Oil Yield Stress, max 35 -
Corrosion (D6594)
Cu, ppm increase, max 20 20
Pb, ppm increase, max 120 120
Sn, ppm increase, max 50 50
Cu strip rating, max 3 3
Shear Stability (D7109) by ASTM D6278
100˚C viscosity after 90 cycles, cSt Stay in grade Stay in grade
Foaming (ASTM D892)
Sequence I (w/o Option A) 10 / 0 10 / 0
Sequence II (w/o Option A) 20 / 0 20 / 0
Sequence III (w/o Option A) 10 / 0 10 / 0
Elastomer Compatibility
API CJ-4 (D7216) Seal Compatibility - Pass
API CI-4 Seal Compatibility Pass -
Engine Tests
Mack T-12 EGR (1)
Mack Merit rating, min - 1000
Avg Liner Wear, um, max - 20
Avg Top Ring Wt. Loss, mg, max - 105
Delta Pb, 0 - 300 hr, ppm, max - 30
Delta Pb, 250 - 300 hr, ppm, max - 12
Oil Consumption, g/hr, max - 80
01/08 - Crankcase - 89
Specification: Cummins
Bench Tests Cummins 20078 Cummins 20081
CI-4 / CI-4 + CJ-4
Mack T-11 (ASTM D7156)
TGA % Soot @ 4 cSt Increase, at 100˚C, min - 3.5
TGA % Soot @ 12 cSt Increase, at 100˚C, min - 6.0
TGA % Soot @ 15 cSt Increase, at 100˚C, min - 6.7
Mack T-10 EGR (1)
Merit Rating, min 1000 -
Avg. Liner Wear, µm, max 32 -
Avg. TRWL, mg, max 158 -
EOT Used Oil/New Oil Pb Content, ppm max 35 -
Pb Increase 250 - 300 hrs, ppm, max 14 -
Mack T-8E (D5967-96 EXT)
Relative Viscosity @ 4.8% Soot, cSt, max 1.8 max -
Viscosity increase @ 3.8% Soot, cSt, max Report -
Cummins ISM
Cummins Merit Rating, min - 1000
Crosshead Wt. Loss, mg max 7.5 7.1
OFDP @ 150 hrs, kPa max 55 19
Avg. Engine Sludge, merit min 8.1 8.7
Avg. Adj. Screw Wt. Loss, mg max - 45
Cummins M-11 EGR
Avg crosshead Wt. Loss, mg, max 20 -
Top Ring Wt. Loss, mg max 175 -
OFDP @ 150 hrs, kPa max 275 -
EOT Sludge Rating, merits, min 7.8 -
JASO M354-2000
Cam Lobe Wear, µm, max 95 -
Cummins ISB EGR
Avg. Slider Tappet Wt. Loss, mg max - 100 / 108 / 112
Avg. Cam Lobe Wear, mm, max - 50 / 53 / 55
Avg. Crosshead Wt. Loss, mg max - Report
Caterpillar C13
Caterpillar Merit rating, min - Report
Hot stuck piston ring - Report
Delta Oil Consumption, g/hr max - Report
Avg Top Land Carbon, Demerit max - Report
Avg Top Groove Carbon, Dermerit max - Report
2nd Ring Top Carbon, Demerit max - Report
1
( ) For Cummins 20078, run Mack T12 or T10
01/08 - Crankcase - 90
Specification: Cummins
Engine Tests Cummins 20078 Cummins 20081
CI-4 / CI-4 + CJ-4
Caterpillar 1R
Weighted Demerits, max 382 -
Top Groove Carbon, Demerits, max 52 -
Top Land Carbon, Demerits, max 31 -
Initial Oil Consumption, g/h, max 13.1 -
Final Oil Consumption, g/h, max IOC + 1.8 -
Piston ring & liner scuffing, ring sticking None -
Caterpillar 1N
Wt. Demerits, max 286 286.2
Top Groove Fill, % max 20 20
Top Land Heavy Carbon, % max 3 3
Oil Consumption, g/kW-h max 0.5 0.5
Piston/ring/liner scuffing None None
Piston ring sticking None None
Caterpillar 1K
Weighted Total Demerits, max 332 -
Top Groove Fill, %, max 24 -
Top Land Heavy Carbon, % max 4 -
Avg Oil Consumption, g/bhp-hr, max 0.5 -
Piston ring & liner scuffing None -
Sequence IIIF (2) (ASTM D6984)
EOT KV % Increase @ 40˚C, max 275 275
Cam + Tappet Wear, µm, max 20
Oil Consumption, Litres, max 5.2
Sequence IIIG (2)
EOT KV % Increase @ 40˚C, max - -
RFWT (D5596)
Avg. pin wear, mils max 0.3 0.3
EOAT (D6894)
Oil aeration volume, % max 8.0 8.0
01/08 - Crankcase - 91
IOEM Specifications: DDC
01/08 - Crankcase - 92
IOEM Specifications: DDC
OM 501LA Euro 5
Parameters & Limits TBD - - TBD(2)
Mack T-12 EGR(1)
Mack Merit Rating, min 1000 1000 1000
Mack T-11 (ASTM D7156)
TGA % Soot @ 4 cSt Increase, at 100˚C, min - - 3.5 3.4 3.3
TGA % Soot @ 12 cSt Increase, at 100˚C, min 6.00 - 6.0 5.9 5.9
TGA % Soot @ 15 cSt Increase, at 100˚C, min - - 6.7 6.6 6.6
Mack T-10 EGR(1)
Merit Rating, min 1000 1000 -
Avg Liner Wear, µm, max 32 32 34 35 -
Avg. Top Ring Weight Loss, mg, max 158 150 159 163 -
EOT Used Oil/New Oil Pb Content, ppm, max 35 50 56 59 -
Pb Increase 250 - 300 hrs, ppm, max 14 - -
Avg. Oil Consumption, g/h, max 65 65 -
Mack T-8E (D5967-96 EXT)
Relative Viscosity @ 4.8% Soot, cSt, max - 2.1 2.2 2.3 -
Viscosity Increase @ 3.8% Soot, cSt, max - 11.5 12.5 13.0 -
Cummins ISM
Cummins Merit Rating, min 1000 1000 1000
Crosshead wt loss, mg, max 7.5 7.5 100
Cummins M-11
Crosshead Wt. Loss, mg, max - 6.5 7.5 8.0 -
OFDP, kPa, max - 79 93 100 -
Sludge rating, merits, min - 8.7 8.6 8.5 -
(1) For DDC 93K214 & 93K215, run either Mack T12 or T10
(2) TBD=Limit to be determined
01/08 - Crankcase - 93
IOEM Specifications: DDC
01/08 - Crankcase - 94
IOEM Specifications: DDC
Caterpillar C13
Caterpillar Merit Rating, min - - 1000
Hot stuck piston ring - - None
Caterpillar 1R
Weighted Demerits, max 382 - -
Top Groove Carbon, Demerits, max 52 - -
Top Land Carbon, Demerits, max 31 - -
Initial Oil Consumption, g/h, max 13.1 - -
Final Oil Consumption, g/h, max IOC + 1.8 - -
Piston ring and liner scuffing, ring sticking None - -
Caterpillar 1P (D6681)
Weighted Demerits, max - 350 378 390 -
Top Groove Carbon, %, max - 36 39 41 -
Top Land Carbon, %, max - 40 46 49 -
Avg. Oil Consumption, g/hr, max - 12.4 12.4 12.4 -
Final Oil Consumption, g/hr, max - 14.6 14.6 14.6 -
Piston ring and liner scuffing - None -
Caterpillar 1N (D6750)
Wt. Demerits, max 286.2 - 286.2 311.7 323.0
Top Grove Fill, %, max 20 - 20 23 25
Top Land Heavy Carbon, %, max 3 - 3 4 5
Oil Consumption, g/kW-h max 0.5 - 0.5
Piston/ring/liner scuffing None - None
Piston ring sticking None - None
Caterpillar 1K
Weighted Demerits, max 332 332 347 353 -
Top Groove Fill, %, max 24 24 27 29 -
Top Land Heavy Carbon, %, max 4 4 5 5 -
Avg Oil Consumption, g/kW-h, max 0.5 0.5 0.5 0.5 -
Piston ring and liner scuffing None None -
Sequence IIIF(2) (ASTM D6984)
EOT KV % Increase @ 40˚C, max 275 - 275
Viscosity Increase @ 60 hrs, %, max - 295 -
Oil Consumption, litres, max 5.2 - -
Sequence IIIG (2)
EOT KV % Increase @ 40˚C, max - - 150
RFWT (D5596)
Avg. pin wear, mils, max 0.3 0.3 0.33 0.36 0.3 0.33 0.36
EOAT (D6894)
Oil aeration volume, %, max 8.0 8.0 8.0
2
( ) For DDC 93K218, run either Sequence IIIF or IIIG
01/08 - Crankcase - 95
OEM Specifications: Mack
01/08 - Crankcase - 96
OEM Specifications: Mack
01/08 - Crankcase - 97
OEM Specifications: Mack
Sequence IIIG
EOT KV % Increase @ 40˚C, max - 150
KV 40˚C Increase parameters
100 hr unadjusted (B), % - Report
80 hr unadjusted (C), % - Report
60 hr unadjusted (D), % - Report
EOT ratio [(B-C)/(C-D)] max - 2.5
RFWT (D5596)
Avg. pin wear, mils, max 0.3 0.3 0.33 0.36
EOAT (D6894)
Oil aeration volume, %, max 8.0 8.0
Volvo D12D460
Piston Deposits, merit, min - 40
Ring Riding, %, max - 50
Bore Polish. cm2, max - 150
Oil Consumption (400 hr), g/hr, max - 35
Oil Consumption (final 100 hr), g/hr, max - 35
VD3 Approval Required -
01/08 - Crankcase - 98
European OEM Seal Test Requirements for Automotive Engine Oils
Test
Test Limits
Conditions
OEM Specification Test Elastomer Temp Time Change in Tensile Change in Elongation Change in Volume Weight Cracking
Method (˚C) (Hrs) Hardness Strength Tensile at break (%) elongation Change Change
(Shore A) at Break Strength at break (%) (%)
(N/mm2) at yield (%) (%)
Mercedes 229.1, 229.3, 229.31, VDA NBR 34 100 168 -8+2 - -20 max - -35 max 0/+10 - -
Benz 229.5, 229.52, 675301 AK6 150 168 -5/+5 - -50 max - -55 max 0/+5 - -
228.0/1, 228.2/3, ACM E7503 150 168 -2/+6 - -30 max - -50 max -3/+10 - -
228.31, 228.5, 228.51
EAM
150 168 -5/+10 - -35 max - -50 max -5/+15 - -
D8948-200
Volkswagen 505.00 PV 3344 AK6 150 3 X 94 - 8 min -50 max 160 min -50 max - - No Cracks
501.01 AK6 150 3 X 94 - 8 min -50 max 160 min -50 max - - No Cracks
502 PV 3344 ACM 150 168 -5/+6 - -30 max - -30 max - -2/+4 -
505.01 VAMAC 150 168 -8/+8 - -30 max - -30 max - -3/+15 -
AK6 150 168 - 7 min -60 max 160 min -50 max - - No Cracks
504.00 PV 3344 ACM 150 500 -4/+10 - -40 max - -40 max - -2/+6 -
507.00
VAMAC 150 500 -4/+10 - -40 max - -40 max - -3/+10 -
270, 271 NBR 28 100 168 -10 max - -20 max - -30 max 0/+10 - -
DIN
MAN M3275 AK6 150 168 -5/+5 - -30 max - -40 max -2/+5 - -
53521
M3277
01/08 - Crankcase - 99
Driveline
Driveline
Contents Driveline
Automotive Gear:
Caterpillar TO - 4 Requirements
Ford MERCON® and MERCON® V Specifications
General Motors Allison C-4 Specification
General Motors DEXRON® II, IIE and III Specifications
General Motors DEXRON® VI
01/08 Driveline - 1
API Lubricant Service Designation for Automotive Manual Transmission(1) & Axles
This material was prepared by the Lubricants service Classification Task Force
of the Fuels and Lubricants Committee, Marketing Department, American
Petroleum Institute, to assist manufacturers and users of automotive
equipment in the selection of transmission and axle lubricants for the
operating conditions as described.
In developing the language for the service classifications, a need was recognised
to supplement the descriptions for certain gear lubricants, particularly those for
hypoid gears, by referring to a series of tests which would serve as a “test
language” to provide more detailed information on the performance requirements
of such lubricant. This “test language” was developed by Section III of Technical
Division B on Automotive Lubricants of ASTM Committee D-2, and reference is
made to these test procedures in the API service designations described below.
This system of designations replaced all previous API gear lubricant designations
and became effective May 1, 1969. These designations are as follows:-
API-GL-1 Designates the type of service characteristic of automotive spiral-bevel and worm-gear
axles and some manually operated transmissions operating under such mild conditions
of low unit pressures and sliding velocities, that straight mineral oil can be used
satisfactorily. Oxidation and rust inhibitors, defoamers, and pour depressants may be
utilised to improve the characteristics of lubricants for this service. Frictional modifiers
and extreme pressure agents shall not be utilised.
01/08 Driveline - 2
API Lubricant Service Designation
API-GL-4 This classification is still used commercially to describe lubricants, but the
equipment required for the anti-scoring test procedures to verify lubricant
performance is no longer available.
Lubricants suitable for this service are those which provide anti-score
protection equal to or better than that defined by CRC Reference Gear Oil
RGO-105 and have been subjected to the test procedures and provide the
performance levels described in ASTM STP-512A, dated March 1987(3).
Lubricants suitable for this service are those which provide anti-score
protection equal to or better than that defined by CRC Reference Gear Oil
RGO-110 and have been subjected to the test procedures and provide the
performance levels described in ASTM STP-512A dated March 1987(2).
API-GL-6 This category is obsolete and is listed for historical reference only.
The equipment used to measure performance is no longer available.
Note: API GL-4 oils are not suitable for highly-loaded hypoid axles. API GL-4 oils
are used in synchronised manual transmissions and transaxles as well as
in mild hypoid and spiral bevel axles.
01/08 Driveline - 3
SAE J306 Automotive Gear Viscosity Classification Axle and Manual Transmission Lubricant Viscosity Classification
01/08 - Driveline - 4
DEF STAN 91-59/1 Lubricating Oil, Extreme Pressure
Grades 75W and 80W90: Joint Service Designation OEP-38 and OEP-220 Respectively
Note:
(1) Test facilities for these tests are available at DQA/TS Woolwich.
The above requirements are absolute and not subject to correction for tolerance of test method.
This specification is currently (March 2000) under review.
01/08 - Driveline - 5
MACK GO-H Covering SAE 90, SAE 140, SAE 80W-90 and SAE 85W-140 oils
Test Parameters Limits
Power Divider Condition of cams and divider wedges:
Snap Test 5GT11 Breakage none
Chipping none
Scoring none
Hard snaps during test none
MIL-L-2105D Full approval required
Test for Transmission and Carrier Radial Immersion at 93°C for 100 hours:
Lip Seal 5 GT 75 Appearance as original
Blistering none
Gum none
Tackiness none
Brittleness none
Swelling none
Timken Bearing Sample heated for 6 hours at 150°C. Bearing dipped in sample and drained for 1 hr
Corrosion 09196 Bearing placed in humidity cabinet for 3 hrs at 60°C in 100% humidity.
Rust at end of test, max. none
Thermal Oxidation Stability 200g/sample in uncovered 400 ml. beaker for 100 hrs. at 150°C in a gravity convection oven
Evaporation Loss, max, % 10
Viscosity Increase at 99°C, max, % 15
Precipitation Number, max. 0.65
Gear Oil Spalling Test 5 GT 71A Minimum B 10 life of 50% above the GO-G reference 160 hours minimum
Transmission Test for Evaluation of Minimum
No missed shifts and no measurable shifter fork wear at the centre of the pads
Thermally Stable Gear Oils 5 GT 73 65,000 cycles
Note:
The lubricant must be a blend from well-refined virgin base stocks (high viscosity index - 95 min.) compounded with load-carrying and lubricity ingredients.
The oil shall be stable and contain no abrasive or corrosive ingredients.
01/08 - Driveline - 6
MACK GO-J and GO-J Plus Gear Oil Requirements
Extended Drain (GO-J Plus) Standard Drain (GO-J)
Highway (Class A, B)(1) 500,000 Miles or 3 Years 250,000 Miles or 2 Years
Vocational (Class AA, BB, C, CC)(1) 80,000 Miles or 1 Year or 1,200 hrs 40,000 Miles or 1 Year or 1,200 hrs
Off-Road (Class D)(1) 6 Months 6 Months
01/08 - Driveline - 7
MACK TO - A Plus Transmission Oil Requirements
Extended Drain (TO-A Plus)
Highway (Class A,B)(1) 500,000 Miles or 3 Years
Vocational (Class AA, BB, C, CC)(1) 80,000 Miles or 1 Year or 1,200 hrs
Off-Road (Class D) Not Available
01/08 - Driveline - 8
MAN 341-1 Specification continued
01/08 - Driveline - 9
MAN 341-1 Specification
01/08 - Driveline - 10
MAN 341-2 Specification continued
01/08 - Driveline - 11
MAN 341-2 Specification
01/08 - Driveline - 12
MAN 342 Specification
01/08 - Driveline - 13
MAN 3343 Specification
Type M S
SAE Viscosity Class 80W90 85W90 75W90
Density at 15°C, g/ml Report Report Report
Maximum Temperature at which the Brookfield Viscosity is 150,000 mPa.s,°C -26 -12 -40
Kinematic Viscosity at 40°C, mm2/s Report Report Report
Kinematic Viscosity at 100°C, mm2/s 13.5 min 13.5 min 13.5 min
Viscosity at 100°C after Shear (20hr KRL), mm2/s Stay in Grade
Flash Point, °C 190 min 200 min 200 min
Pour Point, °C <-27 max <-21 max <-40 max
Total Acid No., mg KOH/g Report Report Report
Calcium, Magnesium, Zinc, Barium, mg/kg Report Report Report
Phosphorus, % mass Report Report Report
Chlorine, mg/kg 100 max 100 max 100 max
Oxidation Stability (for 192hrs) - CEC-L-48-A-95B at 150°C at 160°C
Viscosity Increase at 100°C, mm2/s 130 max 130 max 130 max
Change in Total Acid Number, mg KOH/g 10 max 10 max 10 max
Sludge Formation Report Report None
Steel Corrosion (DIN ISO 7120 Method A) - Metallic elements in oil after test to be reported no rust no rust no rust
Copper Corrosion (3 hrs ar 120°C) ASTM D130 - Copper in oil after test to be reported 2 max 2 max 2 max
Foaming Tendency / Stability
Sequence I 20/0 20/0 20/0
Sequence II 50/0 50/0 50/0
Sequence III 20/0 20/0 20/0
MAN Static Seal Tests (168hr: 100°C NBR-28, 150°C AK6 & ACM 121433) Pass Pass Pass
01/08 - Driveline - 14
Performance Requirements for MIL-L-2105D (GL-5) Lubricants Draft 2005
SAE Viscosity Grade 75W 80W-90 85W-140
ASTM D5704 (formerly L-60-1 or L-60)
Thermal Oxidation Stability 100°C Viscosity Increase at 50 hrs, max, % 100 100 100
Pentane Insolubles, max, % 3 3 3
Toluene Insolubles, max, % 2 2 2
ASTM D5704 (formerly L-33-1)
Moisture Corrosion Final rust merit rating, min 9 9 9
CRC L-37 (ASTM D6121)
High Speed - Low Torque “Green” Gears Pass Pass NR
CRC L-42
High Speed-Shock Equal to or better than
Ring & Pinion Tooth Scoring, max. % NR
Loading Axle Test Passing reference oil
ASTM D-130 (3h@ 121°C)
Copper Strip Corrosion Strip Rating, max. 3 3 3
ASTM D892
Foam Tendency max. Sequence I 20 20 20
Sequence II 50 50 50
Sequence III 50 50 50
Notes:
NR: Not Required, if 80W90 passes in the same base stock. Lower L-37 and L-42 test temperatures are required for 75W oils often referred to as Canadian versions
01/08 - Driveline - 15
Performance Requirements for SAE J2360 (formerly MIL-PRF-2105E) November 1998
SAE Viscosity Grade 75W 80W90 85W140
2
Viscosity at 100°C min, mm /s 4.1 13.5 24.0
2
max, mm /s - 18.5 32.5
Viscosity at 150,000 mPa.s, -40 -26 -12
max temp °C
Channel Point, min, °C -45 -35 -20
Flash Point, min, °C 150 165 180
CRC L-60-1 (ASTM D5704)
Thermal Oxidation Stability 100°C Viscosity Increase at 50 hrs, max., % 100 100 100
Pentane Insolubles, max., % 3 3 3
Toluene Insolubles, max., % 2 2 2
Carbon Varnish, min., Rating 7.5 7.5 7.5
Sludge, max, Rating 9.4 9.4 9.4
CRC L-33-1 (ASTM D7038)
Moisture Corrosion Rust on Gear Teeth Bearings and Cover plate, Rating, min 9.0 9.0 9.0
CRC L-37 (ASTM D6121)
High Speed - Low Torque “Green Gears” Pass Pass NR
High Torque - Low Speed “Lubrited” Gears Pass Pass NR
CRC L-42
High Speed-Shock Ring and Pinion Tooth Scoring, max., % Equal to or better than NR
Loading Axle Test passing reference oil
Cycle Durability (ASTM D5579)
MACK Cycling Test No. of Cycles Equal to or better than average of past 5 reference runs.
ASTM D-130
Copper Corrosion/3 hrs at 121°C Strip Rating, max. 3 3 3
Elastomer Compatibility (ASTM D5662) Polyacrylate Fluoroelastomer Nitrile
Polyacrylate + Fluoroelastomer Elongation Change, min, % -60 -75 -60
at 150°C for 240 hrs Hardness Change, Points -25 to + 5 -5 to + 10 -10 to + 5
Nitrile at 100°C for 240 hrs Volume Change, % -5 to + 30 -5 to + 15 -5 to + 20
ASTM D892
Foam Tendency/Stability, ml, max. Sequence I 20/0 20/0 20/0
Sequence II 50/0 50/0 50/0
Sequence III 20/0 20/0 20/0
SS&C FTM 791
Storage Stability & Compatibility Method 3340 Pass Pass Pass
Notes:
NR: Not required, if 80W90 passes in the same base stock. Lower L-37 and L-42 Test Temperatures are required for 75W oils.
01/08 - Driveline - 16
MT-1 Category Tests and Acceptance Criteria
(2) Shall pass the performance requirements as specified in the MIL-L-2105D specification when tested
in accordance with Federal Test Method 3440.1.
01/08 - Driveline - 17
Scania STO 1:0
01/08 - Driveline - 18
Volvo Transmission Oil Specification 1273.07
01/08 - Driveline - 19
Volvo Transmission Oil Specification 1273.12
01/08 - Driveline - 20
ZF Specifications: Master List
01/08 - Driveline - 21
ZF Specifications: Master List
01/08 - Driveline - 22
ZF Specifications: Master List
01/08 - Driveline - 23
ZF Specifications: Master List
01/08 - Driveline - 24
Caterpillar TO - 4 Transmission and Drive Train Fluid Requirements
Requirements Test Method
Physical Properties
Rust Control Less than 6 rust spots per linear inch on two Modified International Harvester BT-9
out of three test specimens (175 hours under dynamic humidity conditions)
Copper Corrosion 1a max. ASTM D130 (2 hours at 100°C)
Fluid Compatibility No sedimentation or precipitation Mix 50 mls test oil with 50 mls reference oil; heat to 204°C,
cool to ambient; centrifuge for 30 min at 6000G
Homogeneity No sedimentation or precipitation Test oil held at -32°C for 24h, warmed to ambient, centrifuged
Foam, tendency/stability, mls Sequence I - 25/0 ASTM D892 Part 1: No water added
Sequence II - 50/0 Part 2: 0.1% water in oil
Sequence III - 25/0
Flash Point 160°C min. ASTM D92
Fire Point 175°C min. ASTM D92
Elastomer Compatibility
Fluoroelastomer Av. Elongation of elastomer in aged test oil must
not be greater than Av. Elongation with reference oil
ASTM D471 (240 hours; 150°C)
D Elongation with test oil must be less than
or equal to D Elongation with reference oil + 10%
Allison C-4 Elastomer Test See Allison C-4 Specification See Allison C-4 Specification
Oxidation Test
Thermal Oxidation Stability (THOT) See Allison C-4 Specification
01/08 - Driveline - 26
Ford MERCON® Specifications
Test Method MERCON® V MERCON®
Miscibility MERCON® Appendix 1 No separation No separation
Viscosity
at 100°C ASTM D 445 6.8 mm2/s,min 6.8 mm2/s,min
at -20°C ASTM D 2983 1,500 mPa.s, max 1,500 mPa.s, max
at -40°C ASTM D 2983 13,000 mPa.s, max 20,000 mPa.s, max
Shear Stability
Degraded 100°C ASTM D445/KRL 20hr 6.0 mm2/s,min
Apparent Vis at 150°C ASTM D4683
ULSV 40 passes FISST Read & Report
UHSV (D5275) Read & Report
DLSV Read & Report
DHSV 2.6 mm2/s,min
Apparent Vis at 100°C ASTM D 4683
DHSV 5.4 mm2/s,min
Vis after mod. NOACK at -40°C ASTM 2983 ASTM 2983 2,000 mPa.s maximum change
Evaporation Loss Modified NOACK (150°C, 2 hrs) 10% maximum change 10% maximum change
Flash Point ASTM D 92 180°C, min 177°C, min
Copper Strip ASTM D 130 1b, max 1b, max
Non-Corrosion and Non-Rusting Properties ASTM D 665 A No visible rust No visible rust
Colour ASTM D 1500 Red 6.0 - 8.0 6.0 - 8.0
Vane Pump Wear Test ASTM D 2882 10mg, max 10mg, max
FZG Wear Test ASTM D 5182, 1450 rpm, 11 Load Stage Pass
15 min. at 150°C
Four Ball Wear ASTM D 4172 Average scar diameter of two runs
600rpm, 100°C 0.61 mm maximum
600rpm, 150°C 0.61 mm maximum
Falex EP Test ASTM D 3233
Method B No seizure at 100°C Average of 750lbs. Minimum
No seizure at 150°C Average of 750lbs. Minimum
MERCON® Timken ASTM D 2782 No scoring
9lb. Load, 150°C, 10 min Average 0.60 mm maximum
01/08 - Driveline - 27
Ford MERCON® Specifications
Test Method MERCON® V MERCON®
Anti-shudder Evaluation MERCON® V Appendix 4 Candidate Fluid Equiv. to Reference
Clutch Friction Evaluation and Durability MERCON® V Appendix 5 SD 1777
Midpoint Coeff. , 0.140 - 0.170 Midpoint Coeff. , 0.13 - 0.16
20K Friction Durability Low Speed Dynamic, 0.135 - 0.160 Low Speed Dynamic, 0.12 - 0.16
Stop Time, s 0.70 - 0.90 Engagement time, s 0.75 - 1.0
E/M (S1/D) Ratio, 0.85 - 1.07 E/M (S1/D) Ratio, 0.90 - 1.0
Static Breakaway, 0.100 - 0.155 Static Breakaway, 0.10 - 0.15
S2/DRatio, Rate Report
Anti-foaming Properties ASTM D 892 Tendancy/Stability Tendancy/Stability
Sequence 1: 50/0 max Sequence 1: 100/0 max
Sequence 2: 50/0 max Sequence 2: 100/0 max
Sequence 3: 50/0 max Sequence 3: 100/0 max
Sequence 4: 100/0 max Sequence 4: 100/0 max
Elastomer Compatibility MERCON® V Appendix 7 ATRR 101, +6 to +14% / ±7 ATRR 101, +6 to +14% / ±6
(Volume Change/Hardness Change) Volume/Hardness ATRR 200, +3.0 to +8.0% / ±5 ATRR 200, +3.0 to +8.0% / ±5
ATRR 300, +20 to +48% / -15 to -40 ATRR 300, +20 to +48% / -15 to -40
ATRR 400, +1.0 to +6.0% / ±8 ATRR 400, 0 to +4.0% / ±5
ATRR 500, +4 to +16% / ±5 ATRR 500, +8 to +22% / ±10
ATRR 600, Rate & Report ATRR 600, Rate & Report
ATRR 700, Rate & Report ATRR 700, Rate & Report
Aluminum Beaker Oxidation Test MERCON® V Appendix 8 Pentane Insolubles <0.35% Pentane Insolubles <1%
Delta TAN, 3.5 maximum Delta TAN, 4.0 maximum
Delta IR, 30 maximum Delta IR, 40 maximum
Visc. Inc. at 40°C, 25% maximum Visc. Inc. at 40°C, 40% maximum
Cu Strip Rating, 3b max Cu Strip Rating, 3b max
Al Strip Rating, No Varnish Al Strip Rating, No Varnish
Sludge, No Sludge Sludge, No Sludge
Viscosity at -40°C, Rate & Report Viscosity at -40°C, Rate & Report
Calculated % wt loss, Rate & report Calculated % wt loss, Rate & report
Cycling Test GM-6297-M plus post test viscosity limits Pass GM cycling test Pass GM cycling test
20K cycle used oil vis at 100°C 6.0 mm2/s,min
20K cycle used oil vis at 40°C Rate & Report
20K cycle used oil vis at -40°C Rate & Report
Shift Feel MERCON® V Candidate Fluid Equiv. to Reference Candidate Fluid Equiv. to Reference
Notes: (1) Introduced February 1987 - now obsolete (2) Revised September 1992
01/08 - Driveline - 28
Allison Transmission Division General Motors C-4 Heavy Duty Transmission Fluid Specification
Test Requirements Test Method
Chemical Analysis
Metals Content
Barium Report Emission spectroscopy: ICP
Boron Report Emission spectroscopy: ICP
Calcium Report Emission spectroscopy: ICP
Magnesium Report Emission spectroscopy: ICP
Phosphorus Report Emission spectroscopy: ICP
Silicon Report Emission spectroscopy: ICP
Sodium Report Emission spectroscopy: ICP
Zinc Report Emission spectroscopy: ICP
Non metals Content
Chlorine Report ASTM D808
Nitrogen Report ASTM D3228
Sulphur Report ASTM D4951 or ASTM D129
Total Acid Number Report ASTM D664
Total Base Number Report ASTM D4739 or D2896
Infrared Spectrum Report ASTM E168
Physical Properties
Flash Point, °C min. 170 ASTM D92
Fire Point, °C min. 185 ASTM D92
Viscosity Characteristics
Kinematic Viscosity at 40°C Report * ASTM D445
Kinematic Viscosity at 100°C Report * ASTM D445
Apparent Viscosity Report * ASTM D2602
Brookfield Viscosity Report Temperature at 3500 mPa.s ASTM D2983
Stable Pour Point Report * ASTM D97
Note:
* Fluids shall meet SAE J300 Viscosity grades and in addition ATFs must meet DEXRON® III and MERCON® requirements.
01/08 - Driveline - 29
Allison Transmission Division General Motors C-4 Heavy Duty Transmission Fluid Specification
Requirements Test Method
Bench Tests
Foaming Tendency
Foam at 95°C, max. Nil GM 6297-M,Test M
Foam at 135°C, mm max. 10
Break time at 135°C, secs. max 23
Copper Corrosion No blackening or flaking ASTM D130, 3 hours at 150°C
Corrosion/Rust Protection No visible rust on test pins ASTM D665, procedure “A” for 24 hours
Rust Protection No rust or corrosion on any test surface ASTM D1748, 98% humidity, 50 hrs at 40°C
Elastomer Compatibility Limits are adjusted for each new elastomer batch
V1 Volume difference, % 0 to 20
Hardness difference, points -15 to 0
V2 Volume difference, % 0 to 12
Hardness difference, points -7 to +3
V3 Volume difference, % 0 to 22
Hardness difference, points - 14 to 0
P1 Volume difference, % 0 to 8
Hardness difference, points -10 to 0
P2 Volume difference % 0 to 8 GM 6137-M
Hardness change, points -11 to +3
P3 Volume difference % 0 to 4
Hardness change, points -8 to +4
F1 Volume difference % 0 to 3
Hardness change, points -5 to +4
F2 Volume difference % 0 to 4
Hardness change, points -2 to +5
N1 Volume difference % 0 to 5
Hardness change, points -12 to +12
N2 Volume difference % 0 to 6
01/08 - Driveline - 30
Allison Transmission Division General Motors C-4 Heavy Duty Transmission Fluid Specification
01/08 - Driveline - 31
A Comparison of GM DEXRON® II, IIE & III Specification Requirements
General Motors ATF Specification GM 6137-M DEXRON® II DEXRON® IIE DEXRON® III (GM 6417 - M)
01/08 - Driveline - 32
A Comparison of GM DEXRON® II, IIE & III Specification Requirements
General Motors ATF Specification GM 6137-M DEXRON® II DEXRON® IIE DEXRON® III (GM 6417 - M)
Note:
* Tensile strength and elongation are now required to be reported but no limits have been set yet.
01/08 - Driveline - 33
A Comparison of GM DEXRON® II, IIE & III Specification Requirements
General Motors ATF Specification GM 6137-M DEXRON® II DEXRON® IIE DEXRON® III (GM 6417 - M)
Test Method Requirement Requirement Requirement
Saginaw Power Steering GM Method Parts condition to be equal
Pump Test to or better than that obtained
with reference fluid
Vane Pump Wear Test ASTM D2882 Mod
80+/-3°C weight loss < 15mg weight loss < 15mg
6.9 MPa
HEFCAD - Plate Clutch Test GM Method Satisfactory operation Satisfactory operation Satisfactory
for 100 hours for 100 hours operation for 100 hours
DEXRON® II uses No unusual clutch plate No unusual wear or No unusual wear or
SD-715 Clutch Plates wear or flaking flaking on test parts flaking on test parts
Between 24 and 100 hours Between 20 and 100 hours Between 10 and 100
DEXRON® IIE uses of operation:- of operation:- hours of operation:-
SD-1777 Clutch Plates 115Nm < Midpoint Dynamic 150Nm < Midpoint Dynamic 150Nm < Midpoint Dynamic
Torque < 175Nm Torque <180Nm Torque < 180Nm
DEXRON® III uses Delta Torque < 14Nm Maximum Torque > 150Nm Maximum Torque > 150Nm
SD-1777 Clutch Plates
0.45s < Engagement Delta Torque < 30Nm DeltaTorque < 30Nm
Time < 0.75s
Stop time between Stop time between
0.45 and 60s 0.50 and 0.60s
01/08 - Driveline - 34
A Comparison of GM DEXRON® II, IIE & III Specification Requirements
General Motors ATF Specification GM 6137-M DEXRON® II DEXRON® IIE DEXRON® III (GM 6417 - M)
Band Clutch Test GM Method Uses 3T40 Not Required Satisfactory operation for 100 hours Satisfactory operation for 100 hours
Band & Drum No unusual wear or flaking on test parts No unusual wear or flaking on test parts
Between 20 and 100 hours of operation:- Between 20 and 100 hours of operation:-
145Nm < Midpoint Dynamic 180Nm < Midpoint Dynamic
Torque < 220Nm Torque < 225Nm
End Torque > 170Nm End Torque > 170Nm
Delta Torque < 80Nm Delta Torque < 80Nm
Stop time between 0.40 and 0.60 s Stop time between 0.35 and 0.55 s
Report Maximum Torque, Nm Report Maximum Torque, Nm
THOT - Oxidation GM Method Satisfactory operation for 300 hours Satisfactory operation for 300 hrs. Satisfactory operation for 300 hours
Test THM-350 Transmission parts cleanliness and physical Transmission parts cleanliness & physical Transmission parts condition must
DEXRON® II uses condition must be equal to or better than condition must be equal to or better than be equal to or better than that
Transmission that obtained with Reference Fluid that obtained with Reference Fluid obtained with Reference Fluid
Total Acid Number Increase, 7.0 max. Total Acid Number Increase < 4.5 Total Acid Number Increase < 3.25
DEXRON® IIE and III Carbonyl Absorbance Increase, 0.8 max. Carbonyl Absorbance Increase < 0.55 Carbonyl Absorbance Increase < 0.45
use Hydra-matic 4L60 Min. O2 content of transmission Min O2 content of transmission
Report effluent gas O2 content
Transmission effluent gas 2% effluent gas 4%
Used Fluid Viscosity at - 23.3°C
Used Fluid Viscosity at -20°C < 3,000 mPa.s Used Fluid Viscosity at -20°C < 2000 mPa.s
6000mPa.s max;- 40°C Report
Used Fluid Viscosity at 100°C, 5.5 mm2/s min. Used Fluid Viscosity at 100°C > 5.5 mm2/s Used Fluid Viscosity at 100°C > 5.5 mm2/s
01/08 - Driveline - 35
A Comparison of GM DEXRON® II, IIE & III Specification Requirements
General Motors ATF Specification GM 6137-M DEXRON® II DEXRON® IIE DEXRON® III (GM 6417 - M)
THCT - Cycling Test GM Method Satisfactory operation for 20,000 cycles Satisfactory operation for 20,000 cycles Satisfactory operation for 20,000 cycles
DEXRON® II uses Transmission parts cleanliness & physical Condition of transmission parts must be Condition of transmission parts must be
THM 350 transmission condition must be equal to or better than equal to or better than that obtained equal to or better than that obtained
that obtained with the Reference Fluid with the Reference Fluid with the Reference Fluid
DEXRON® IIE and III 0.35s < 1-2 Shift Time < 0.70s Total Acid Number Increase < 2.50 Total Acid Number Increase < 2.0
use Hydra-matic 4L60 0.20s < 2-3 Shift Time < 0.55s Carbonyl Absorbance Increase < 0.35 Carbonyl Absorbance Increase < 0.30
transmission Total Acid Number Increase, 6.0 max. 1-2 Shift Time between 0.35 and 0.75s 1-2 Shift Time between 0.30 and 0.75s
Carbonyl Absorbance Increase, 0.7,max. 2-3 Shift Time between 0.30 and 0.75s 2-3 Shift Time between 0.30 and 0.75s
Report 3-4 Shift Time, s Report 3-4 Shift Time, s
Used Fluid Viscosity at 100°C 5.5 mm2/s min. Used Fluid Viscosity at 100°C, > 5.0 mm2/s Used Fluid Viscosity at 100°C, > 5.0 mm2/s
during and at end of test Used Fluid Viscosity at -20°C < 2000 mPa.s
Used Fluid Viscosity at -20°C < 2000 mPa.s
No expulsion of ATF from Vent
Vehicle Shift performance essentially equal Shift performance essentially equal Shift performance essentially equal
GM Method
Performance Test to that obtained with the Reference Fluid to that obtained with the Reference Fluid to that obtained with the Reference Fluid
ECCC Vehicle
GM Method Not Required Not Required Equal to or better than Reference Fluid
Performance Test
Sprag Wear Test GM Method Not Required Not Required Maximum Weight Loss - 60 mg
01/08 - Driveline - 36
DEXRON® -III, H Revision [GMN 10055]
01/08 - Driveline - 37
DEXRON® -III, H Revision [GMN 10055]
01/08 - Driveline - 38
DEXRON® -VI [GMN 10060]
01/08 - Driveline - 39
DEXRON® -VI [GMN 10060] Continued
01/08 - Driveline - 40
DEXRON® -VI [GMN 10060] Continued
01/08 - Driveline - 41
Industrial
Industrial
Contents Industrial
Hydraulic:
European Specifications:
Denison Hydraulic Requirements - TP30560
Denison Biofluid Requirements - TP30560
DIN 51524 Part 1
DIN 51524 Part 2
DIN 51524 Part 3
German Steel Industry Specifications SEB 181222
US Specifications:
Cincinnati Machine Anti-Wear Hydraulic Specifications
General Motors Hydraulic Lubricant Standards
US Military MIL-L-17672D Amendment 3
US Steel Hydraulic Standards US Steel 126 & 127
ASTM D6158 Requirements for Type HM Mineral Oil Hydraulic Fluids (antiwear)
ISO 11158 Hydraulic Fluids
JCMAS P041 (HK) Hydraulic Fluids for Construction Machinery
Industrial Gear:
Compressor:
01/08 - Industrial - 1
Contents Industrial
Turbine:
Slideway:
01/08 - Industrial - 2
Denison Hydraulic Requirements - TP30560 05 March 2007
Test HF-0 HF-1 HF-2 HF-3 HF-4 HF-5 Test Method
Viscosity cSt at 40°C Report Report Report 65 to 140cSt Report Report D445
Viscosity cSt at 100°C Report Report Report Report Report Report D445
Viscosity index, min 90 90 90 90 90 90 D2270
Gravity API (Specific) 840 to 900 840 to 900 840 to 900 900 to 970 1050 to 1090 950 to 1300
Zinc, % wt Report Report Report
Pour Point, °C Report Report Report D97
PH at 25°C 8.5 to 10.5
Aniline Point > 100°C (3) > 100°C (3) > 100°C (3) D611
Flash Point, °C Report Report Report D92
Water % 37 to 45 40 to 45
Acid Number Report Report Report D664
Rust Test
Distilled Water No rust No rust No rust No rust No rust No rust D665A
Synthetic Sea Water No rust No rust No rust No rust No rust No rust D665B
Foam
None None None None D892
Allowable Foam after 10mn
Filterability (1)
Filtration Time without water (4) (4) (4) TP-02100
Filtration Time with 2% water (4) (4) (4) (Denison)
01/08 - Industrial - 3
Denison Hydraulic Requirements - TP30560 05 March 2007
Test HF-0 HF-1 HF-2 HF-3 HF-4 HF-5 Test Method
Demulsibility 40/37/3 (30minutes) 40/37/3 (30minutes) 40/37/3 (30minutes) D1401
Sludge and Corrosion
Neutralisation Number after 1000 hrs max 1 mgKOH 1 mgKOH 1 mgKOH
D4310 (2)
Insoluble Sludge max 100 mg 100 mg 100 mg
Total Copper max 200 mg 200 mg 200 mg
Thermal Stability
After 168 hours at 135°C
CINCINNATI
Sludge max 100mg/100ml 100mg/100ml 100mg/100ml
P70 (ISO 46)
Copper wt loss 10 mg 10 mg 10 mg
Copper rod rating Report Report Report
Hydrolytic Stability
Copper specimen wt loss max 0.2 mg/cm2 0.2 mg/cm2 0.2 mg/cm2 D2619
Acidity of Water Layer max 4.0 mgKOH 4.0 mgKOH 4.0 mgKOH/g
FZG, Load stage before damage Report Report Report DIN 51524 Teil 2
Deaeration (ISO 46) < 7 mn < 7 mn < 7 mn < 7 mn < 7 mn < 7 mn NFT 60149
Pump Wear max (vanes + pins) 15 mg 15 mg T6M20C
Pump Wear max for 9 pistons 300 mg 300 mg T6H20C
Shear test (High VI only) 15 % 15 % 15 % KRL (20 hrs)
T6H20C (5) after 307 hrs
T6H20C (5) (5) (5) after 608 hrs
01/08 - Industrial - 4
Denison Biofluid Requirements - TP30560 5 March 2007
Test HF-6 Test Method
Viscosity cSt at 40°C Report D445
Viscosity cSt at 100°C Report D445
Viscosity index, min 90 D2270
Gravity API (Specific) 840 to 900
Zinc, % wt Report
Pour Point, °C Report D97
Aniline Point > 100°C (3) D611
Flash Point, °C Report D92
Acid Number Report D664
Rust Test
Distilled Water No rust D665A
Synthetic Sea Water No rust D665 B
Foam
None D892
Allowable Foam after 10mn
Filterability ()
1
(2) Instructions available on request: Same as used in Military specification MIL-H-24459 Appendixes A & B.
(3) If < 100°C to do seal test DIN 51524.
(4) 600 seconds maximum. Do not exceed twice the filtration time without water.
(5) Viscosity at 40°C (Start - End) > 40 cSt for ISO 46 (-8 cSt)
01/08 - Industrial - 5
DIN 51524 Part 1 (April 2006) Rust and Oxidation Protected Hydraulic Oils
Grade HL10 HL15 HL22 HL32 HL46 HL68 HL100 HL150
ISO Viscosity Class (DIN 51519) VG10 VG15 VG22 VG32 VG46 VG68 VG100 VG150
Kinematic Viscosity at 0°C/(-20°C), mm2/s, max. 90 (600) 150 300 420 780 1400 2560 4500
Kinematic Viscosity at 100°C, mm2/s, min. 2.4 3.2 4.1 5.0 6.1 7.8 9.9 14
Pour Point, °C, max. (ISO 3016) -30 -27 -21 -18 -15 -12 -12 -12
Flash Point (COC), °C, min. (ISO 2592) 125 140 165 175 185 195 205 215
Contents of undissolved matter, mg/kg, max. (ISO 4405) 50
Water content, expressed as a proportion by mass, in % 0.05
Steel Corrosion, max. (DIN 51585) Method A Pass
Copper Corrosion, 3h at 100ºC, max. (DIN 51759) 2
Air Release, 50°C, minutes, max. (DIN 51381) 5 10 17 25
Demulsibility, minutes, max. (DIN 51599/ASTM D1401) 20 (54ºC) 30 (54ºC) 30 (82ºC)
Oxidation Stability, Acidity max. mg KOH/g
≤2.0
at 1000 hrs. (DIN 51587/ASTM D943)
Behaviour towards the Relative
SRE-NBR 1 sealant specified Change % 0 to 18 0 to 15 0 to 12 0 to 10
in DIN 53538 Part 1, after 7 in volume
days ± 2h at 100 ± 1 °C Change in
Shore A 0 to -10 0 to -8 0 to -7 0 to -6
hardness
Foam Volume, ml, max Sequence I 150/0
DIN 51566 Sequence II 75/0
Sequence III 150/0
Density at 15°C , in g/ml To be specified by supplier
Ash (oxide ash), expressed as a proportion by mass, in % To be specified by supplier
Neutralization number (acid or alkaline), in mg KOH/g To be specified by supplier
Cleanliness Class (ISO 4406) 21 / 19 / 16
Wet Filtration (ISO 13357-1) F1, % 70
F2, % 50
Dry Filtration (ISO 13357-2) F1, % 80
F2, % 60
01/08 - Industrial - 6
DIN 51524 Part 2 (April 2006) Anti-Wear Hydraulic Oils
Grade HLP10 HLP15 HLP22 HLP32 HLP46 HLP68 HLP100 HLP150
ISO Viscosity Class (DIN 51502) VG10 VE15 VG22 VG32 VG46 VG68 VG100 VG150
Kinematic Viscosity at 0°C/ (-20°C), mm2/s, max. 90 (600) 150 300 420 780 1400 2560 4500
Kinematic Viscosity at 100°C, mm2/s, min. 2.5 3.2 4.1 5.0 6.1 7.8 9.9 14.0
Pour Point, °C, max. (ISO 3016) -30 -27 -21 -18 -15 -12 -12 -12
Flash Point (COC), °C, min. (ISO 2592) 125 140 165 175 185 195 205 215
Cleanliness Class, (ISO 4406) 21 / 19 / 16
Contents of undissolved matter, (ISO 4405)
50
expressed as a proportion by mass, mg/kg
Water content, expressed as a proportion by mass,
0.05
in % m/m (DIN ENISO 12937)
Steel Corrosion, max. (DIN ISO 7120) Class 0 - Method A
Copper Corrosion, 3h at 100ºC, max. (DIN ENISO 2160) 2
Air Release, 50°C, minutes, max. (DIN ISO 9120) 5 10 13 21 32
Demulsibility, minutes, max. (DIN ISO 6614) 20 (56ºC) 30 (54ºC) 30 (82ºC)
FZG A/8.3/90: Load Stage Fail, min. (DIN 51354-2) - 10
Vane Pump Wear, mg, max. (DIN ENISO 20763)
Ring - 120 -
Vanes - 30 -
Oxidation Stability, Acidity max. mg KOH/g
2.0
at 1000 hrs (DIN 51587)
Behaviour towards the Relative
SRE-NBR 1 sealant specified Change % 0 to 18 0 to 15 0 to 12 0 to 10
in DIN 53538 Part 1, after 7 in volume
days ± 2h at 100 ± 1 °C Change in
Shore A 0 to -10 0 to -8 0 to -7 0 to -6
hardness
Foam Volume, ml, max Sequence I 150/0
ISO 6247 Sequence II 75/0
Sequence III 150/0
01/08 - Industrial - 7
DIN 51524 Part 2 (April 2006) Anti-Wear Hydraulic Oils
Grade HLP10 HLP15 HLP22 HLP32 HLP46 HLP68 HLP100 HLP150
Density at 15°C (DIN 51757) To be specified by supplier
Ash (oxide ash), expressed as a proportion by mass,
To be specified by supplier
in % (DIN 51575)
Neutralization number (acid or alkaline),
To be specified by supplier
in mg KOH/g (DIN 51558-1)
Filtration Test (ISO 13357-2) F1, min % 80
F2, min % 60
Filtration Test (ISO 13357-1) F1, min % 70
F2, min % 50
01/08 - Industrial - 8
DIN 51524 Part 3 (April 2006) HVLP Hydraulic Oils
Grade HVLP10 HVLP15 HVLP22 HVLP32 HVLP46 HVLP68 HVLP100 HVLP150
ISO Viscosity Class (DIN 51519) ISO VG 10 ISO VG 15 ISO VG 22 ISO VG 32 ISO VG 46 ISO VG 68 ISO VG 100 ISO VG 150
Kinematic Viscosity at -20°C, mm2/s To be specified by supplier - - -
Kinematic Viscosity at 0°C, mm2/s To be specified by supplier
Kinematic Viscosity at 40°C, mm2/s ≤ 11.0 ≤ 16.5 ≤ 24.2 ≤ 35.2 ≤ 50.6 ≤ 74.8 ≤ 110 ≤ 165
≤ 9.0 ≥ 13.5 ≤ 19.8 ≥ 28.8 ≥ 41.4 ≥ 61.2 ≥ 90 ≤ 135
Kinematic Viscosity at 100°C, mm2/s To be specified by supplier
Viscosity index ≥ 140 ≥ 120
Pour Point, °C ≤ -39 ≤ -39 ≤ -39 ≤ -30 ≤ -27 ≤ -24 ≤ -21 ≤ -18
Flash Point, °C, ≥ 125 ≥ 125 ≥ 175 ≥ 175 ≥ 180 ≥ 180 ≥ 190 ≥ 200
Cleanliness Class (IS 4406) 21 / 19 / 16
Contents of undissolved matter, expressed as a
≤ 50
proportion by mass, mg/kg (ISO 4405)
Water content, expressed as a proportion by mass,
≤ 0.05
in % (DIN ENISO 12937)
Steel Corrosion, max. (DIN/ISO 7120) Maximum corrosion rating: Class 0 Method A
Copper Corrosion, 3hrs at 100ºC max. (DIN ENISO 2160) Maximum corrosion rating: 2
Air Release, 50°C, minutes, max. (DIN/ISO 9120) 5 13 21 32
Demulsibility, 54°C, minutes, max. (DIN 51599/ASTM D1401) ≤ 20 (54ºC) ≤ 30 (54ºC) ≤ 30 (82ºC)
Ageing behaviour (increase in neutralization number
≤ 2.0
after 1000 h), in mg KOH/g (DIN 51587)
Behaviour towards the Relative
SRE-NBR 1 sealant specified Change % 0 to 18 0 to 15 0 to 12 0 to 10
in DIN 53538 Part 1, after 7 in volume
days ± 2h at 100 ± 1 °C Change in
Shore A 0 to -10 0 to -8 0 to -7 0 to -6
hardness
Foam Volume, ml, max Sequence I ≤ 150/0
(ISO 6247) Sequence II ≤ 75/0
Sequence III ≤ 150/0
01/08 - Industrial - 9
DIN 51524 Part 3 (April 2006) HVLP Hydraulic Oils
Grade HVLP10 HVLP15 HVLP22 HVLP32 HVLP46 HVLP68 HVLP100 HVLP150
Behaviour in FZG gear rig test - ≥ 10
Loss of mass, in mg after mechanical Ring - ≤ 120 -
test by vane-pump (DIN ENISO 20763) Vane - ≤ 30 -
Relative Viscosity loss at 40ºC and 100ºC after 20 hours, % To be specified by supplier
Density at 15°C, in g/ml (DIN 51757) To be specified by supplier
Ash content (oxide ash) or sulphate ash,
To be specified by supplier
as a percentage by mass
Neutralization number (acid or alkaline),
To be specified by supplier
in mg KOH/g (DIN 51558-1)
Filtration Test (ISO 13357-2) F1, min % 80
F2, min % 60
Filtration Test (ISO 13357-1) F1, min % 70
F2, min % 50
01/08 - Industrial - 10
German Steel Industry Specifications SEB 181222 January 2007
Hydraulic Oil Type HLP 22 HLP 32 HLP 46 HLP 68 HLP 100 Test Method
Kinematic Viscosity, mm2/s. at 0°C, max. To be specified
at 40°C ± 10% 22 32 46 68 100 DIN 51550 + DIN 51562
at 100°C, min. 4.1 5.0 6.2 8.0 10.2
Viscosity Index Report DIN/ISO 2909
Pour Point, °C, max. -24 -21 -18 DIN/ISO 3016
Flash Point, °C, min. 180 200 220 DIN EN ISO 2592
Oil Cleanliness 21 / 18 / 15 ISO 4406
Water Content, Vol, -%, max 0.03 DIN/ISO 12937
Rust Prevention, max. Method B No Corrosion DIN/ISO 7120
Copper Corrosion (3 hrs at 125°C), max. Rating 1 DIN EN ISO 2160
Oxidation Stability, Acidity max. mg KOH/g
2.0 DIN 51587
at 1000 hrs (DIN 51587/ASTM D943)
Behaviour towards the SRE-NBR 1 sealant specified in
DIN 53538 part 1, after 7 days at 100°C
Relative change in volume, % max. 0 to +8 With DIN/ISO 1817
Shore A hardness, max. 0 to -6 DIN 53505
Contents of undisolved matter, ≤ mg/kg 50 SEB 181322
Air Release, minutes, max 5 (50ºC) 10 (50ºC) 15 (75ºC) DIN/ISO 9126
Foam volume, ml, max. Sequence I 100/0
Sequence II 50/0 ISO 6247
Sequence III 100/0
Demulsibility at 54°C, time to 40ml oil, minutes, max. 20 30
DIN/ISO 6614
Final State, max-min-max, ml 42-38-0
Demusability at 60ºC, time to 40ml oil, minutes To be specified
DIN/ISO 6614
Final state, ml To be specified
FZG Gear Testing (A/8.3/90)
Load Stage Fail, min. 10 12 DIN/ISO 14635-1
Work Related Weight Change, mg/ KWh To be specified by supplier
Vane Pump Wear, mg, max. Ring 60
DIN EN ISO 20763
Vanes 15
01/08 - Industrial - 11
German Steel Industry Specifications SEB 181222 December 1997
Hydraulic Oil Type HLP 22 HLP 32 HLP 46 HLP 68 HLP 100 Test Method
Density at 15°C, kg/m3 To be specified DIN 51757
Ash % mass To be specified DIN ENISO 6245
Neutralisation No., mg KOH/g To be specified DIN 51558
Filterability Without water, ≥ % 60 ISO 13357-2
With 0.2% water, ≥ % 60 ISO 13357-1
01/08 - Industrial - 12
Cincinnati Machine Anti-Wear Hydraulic Specifications 2000
Specifications P-68 (HM-32) P-69 (HM-68) P-70 (HM-46) Test Method
Viscosity classification ISO VG 32 ISO VG 68 ISO VG 46
A.P.I. Gravity at 60°F 30 to 33 29 to 31 28 to 31.5 ASTM D287
Kinematic Viscosity at 40°C, mm2/s 28.8 to 35.2 61.2 to 74.8 41.4 to 50.6 ASTM D445
Viscosity Index, min 90 90 90 ASTM D2270
Colour, max 2.0 3.0 3.0 ASTM D1500
Flash Point (COC), °F, min 370 385 385 ASTM D92
Fire Point (COC), °F, min 420 425 425 ASTM D92
Acid Number, mg KOH/g, max 1.5 1.5 1.5 ASTM D974
Steel Corrosion Pass Pass Pass ASTM D665A
Vickers pump wear test
50 50 50 ASTM D2882
Total Ring and Vane wt. loss, mg, max
CM Thermal Stability
Change in Kinematic Viscosity, %, max 5 5 5
Acid Number change, %, max ±50 ±50 ±50
Sludge, mg/100ml, max 25 25 25
Steel Rod Visual, max 1.5 1.5 1.5 CCM‘A’
Steel Rod Deposits per 200ml, mg, max 3.5 3.5 3.5
Steel Rod weight loss per 200ml, mg, max 1.0 1.0 1.0
Copper Rod Visual, CM rating, max 5 5 5
Copper Rod deposits per 200ml, mg, max 10.0 10.0 10.0
Copper Rod weight loss per 200ml, mg, max 10.0 10.0 10.0
01/08 - Industrial - 13
General Motors Hydraulic Lubricant Standards November 2004
Specification Antiwear Hydraulic Oil Zinc-Free Antiwear Hydraulic Oil ASTM
Product Code LH-02-1-04 LH-03-1-04 LH-04-1-04 LH-06-1-04 LH-02-1-04 LH-03-1-04 LH-04-1-04 LH-06-1-04 Method
Viscosity Grade 22 32 46 68 22 32 46 68 -
Viscosity at 40°C, mm2/s 19.8-24.2 28.8-35.2 41.4-50.6 61.2-74.8 19.8-24.2 28.8-35.2 41.4-50.6 61.2-74.8 D445
Viscosity at 100°C mm2/s 4.1 5.0 6.1 7.8 4.1 5.0 6.1 7.8 D445
Viscosity at 0°C mm2/s 300 420 780 1400 300 420 780 1400
Viscosity Index 95 95 D2270
API Gravity Report Report D287
Flash Point (COC), °C 175 190 195 175 190 195 D92
Pour Point, °C -21 -18 -15 -12 -21 -18 -15 -12 D97
Foam
Seq I 50/0 50/0
Seq II 50/0 50/0 D892
Seq III 50/0 50/0
Water seperability, 30 min., max. 40/40/0 40/40/0 D1401
Air Release at 50°C (IP 313), mins. 5 10 5 10 D3427
Copper Corrosion, 3 hours at 100°C 1b 1b D130
Steel Corrosion, Method B Pass Pass D665
Life TOST, hours to TAN of 2.0 mg KOH/g 1500 1500 D943
Cleanliness, as received, max. 19/16/13 19/16/13 ISO 4406
Acid number, max. 1.0 1.0 D664
Zn in final product, ppm, max. 1000 10 D4628
Thermal stability
Acid number change, % max. +/- 50 +/- 50
Viscosity change, 40/100°C, % max 5 5
Sludge, mg/100ml max. 25 25 D2070
Cu rod colour (Cin. Mil), max. 5 5
Cu weight loss, mg max. 10 10
Steel rod colour (Cin. Mil), max. No discolouration No discolouration
01/08 - Industrial - 14
General Motors Hydraulic Lubricant Standards November 2004
Specification Antiwear Hydraulic Oil Zinc-Free Antiwear Hydraulic Oil ASTM
Product Code LH-02-1-04 LH-03-1-04 LH-04-1-04 LH-06-1-04 LH-02-1-04 LH-03-1-04 LH-04-1-04 LH-06-1-04
01/08 - Industrial - 15
SAE MS1004 Type H Hydraulic Oil Specification
Specification HL Rust and Oxidation HM Anti-wear HV Anti-wear and Viscosity Improver ASTM
Viscosity Grade 10 15 22 32 46 68 100 10 15 22 32 46 68 100 10 15 22 32 46 68 100 D2422
Viscosity at 40°C, mm2/s ISO Grade +/- 10% ISO Grade +/- 10% ISO Grade +/- 10% D445
Viscosity Index, min. Report 95 140 120 D2270
Density @ 15 C, g/ml To be specified by supplier To be specified by supplier To be specified by supplier D287
Flash Point (COC), °C, min. 125 165 175 185 195 205 125 165 175 185 195 205 125 165 175 185 195 205 D92
Pour Point, °C, max. -30 -25 -21 -18 -15 -12 -30 -25 -21 -18 -15 -12 -30 -25 -21 -18 -15 -12 D97
Foam
Seq I, max 150/0 150/0 150/0
D892
Seq II, max 150/0 150/0 150/0
Seq III, max 150/0 150/0 150/0
Water seperability @ 54°C, min., max. 30 40 60 30 40 60 30 40 60 D1401
Water seperability @ 82°C, min., max. 60 60 60 D1401
Air Release (IP 313), mins, max. 5 10 5 10 5 10 D3427
Copper Corrosion, 3 hours at 100°C, max 2 2 2 D130
Steel Corrosion, Method A or B Pass Pass Pass D665
1000 hour TOST, TAN mg KOH/g max. 2 2 2 D943
Cleanliness, as received, max. 19/16/13 19/16/13 19/16/13 ISO 4406
Neutralization number, mgKOH/g max. To be specified by supplier To be specified by supplier To be specified by supplier D664
Water content, % mass Below limit of quantitive detectability Below limit of quantitive detectability Below limit of quantitive detectability D95
Contents of undissolved matter, % mass Below limit of quantitive detectability Below limit of quantitive detectability Below limit of quantitive detectability D4055
Ash (oxide ash), % mass To be specified by supplier To be specified by supplier To be specified by supplier D482
Thermal stability
Acid number change, % max. +/- 50 +/- 50 +/- 50
Viscosity change, 40/100C, % max 5 5 5
Sludge, mg/100ml max. 25 25 25 D2070
Cu rod colour (Cin. Mil), max. 5 5 5
Cu weight loss, mg max. 10 10 1
Steel rod colour (Cin. Mil), max. No discolouration No discolouration No discolouration
01/08 - Industrial - 16
SAE MS1004 Type H Hydraulic Oil Specification continued
Specification HL Rust and Oxidation HM Anti-wear HV Anti-wear and Viscosity Improver ASTM
Compatibility with SRE-NBRI seals
DIN 53538 (168h, 100C)
D471
Volume change % 0 to 18 0 to 15 0 to 12 0 to 10 0 to 18 0 to 15 0 to 12 0 to 10 0 to 18 0 to 15 0 to 12 0 to 10
Shore A hardness change 0 to -10 0 to -8 0 to -7 0 to -6 0 to -10 0 to -8 0 to -7 0 to -6 0 to -10 0 to -8 0 to -7 0 to -6
FZG A/8.3/904 11 fail 11 fail
Hydrolytic stability
Cu weight loss, mg/cm2 max. 0.2 0.2 0.2 D2619
Acidity of water layer, mgKOH, max. 4 4 4
Vickers 35VQ25 Pump test
Ring Wear, mg, max. 120 120 D2882
Ring Wear, mg, max. 30 30
No smearing, scoring, scratching, No smearing, scoring, scratching, No smearing, scoring, scratching, Denison
Denison Piston pump test
bronze transfer, corrosion bronze transfer, corrosion bronze transfer, corrosion P-46
01/08 - Industrial - 17
US Military MIL-L-17672D Amendment 3 31-May-95
Specification 2075 T-H 2110 T-H 2135 T-H Test Method
A.P.I. Gravity degrees Report Report Report ASTM D 287, D1298
Pour Point, °C , max -29 -23 -18 ASTM D97
Viscosity at 40°C, mm2/s 32 46 68 ASTM D445 or equivalent
Viscosity at 100°C, mm2/s, min Report ASTM D445 or equivalent
Viscosity Index, min 94 ASTM D2270
Total Acid Number, mg KOH/g, max 0.2 ASTM D974
Flash Point, °C, min 157, 163, 171 ASTM D92
Demulsibility, 30 minutes 40/37/3 ASTM D1401
Foam Test, Seq I 65/0
Seq II 65/0 ASTM D892
Seq III 65/0
Oil Oxidation after 1000 hours
Total Sludge, mg, max 100
Total Iron, mg, max 100 ASTM D943
Total Copper, mg, max 100
Time to reach TAN = 2.0, hrs, min 1000
Copper Corrosion,rating, max 1 ASTM D130
Steel Corrosion Pass ASTM D665B (Modified)
Water, % None ASTM D95
Sulphated Ash, %, max Report ASTM D874
Valve sticking characteristics (Note 1) Pass Appendix B
RPVOT Report ASTM D2272
Contamination, mg/100ml, max (Note 2) 4.0 ASTM F313
Colour Report ASTM D1500
Sulphur Report ASTM D129, D1552 or D2622
Carbon Residue Report ASTM D189
Notes:
1. If all three grades contain the same additive package, only one grade will be tested.
2. Filter pore size shall be 0.8 micrometer.
01/08 - Industrial - 18
US Steel Hydraulic Standards US Steel 126 & 127
Specification 126 127
Viscosity, D88 32, 46, 68 32, 46, 68
Viscosity Index, D567 80 min. 90 min.
COC Flash Point, D92 375°F min. 375°F min.
Hydraulic Pump Test, D2882 (100 hours at 2000 psi) 0.05% Total wear (by weight) 50 mg max.
Four Ball Wear Test, D2266 (40 Kg, 1800 rpm, 130°F, 1 hr) 0.80 mm scar diameter max. 0.50 mm scar diameter max.
RPVOT D2272 120 minutes min. 120 minutes min.
Low Temp Cycling Test (U.S. Steel method) Must pass at 15°F Must pass at 15°F
ml oil ml water ml emulsion minutes ml oil ml water ml emulsion minutes
Water Emulsion Test, D1401 at 130°F
40 37 3 ≤ 30 40 37 3 ≤ 30
Rust Prevention Test, D665 A No rust No rust
01/08 - Industrial - 19
ASTM D6158 Requirements for Type HM Mineral Oil Hydraulic Fluids (antiwear) 2005
Test ASTM Method
ISO - Viscosity grade 10 15 22 32 46 68 100 150 D2422
Kinematic Viscosity at 40°C, cSt 9.0-11.0 13.5-16.5 19.8-24.2 28.8-35.2 41.4-50.6 61.2-74.8 90.0-110 135-165 D445
Viscosity ≤ 750 cP °C, max -33 -23 -15 (-8) -2 4 10 16 D2983
Viscosity index, min 90 D2270
Specific gravity Report D1298
Appearance, visual, at 20°C Clear and bright
Flash point °C, min 125 145 165 175 185 195 205 215 D92
Pour Point °C, max -33 -24 -21 -18 -15 -12 -12 -12 D97
Acid Number mg KOH/g, max Report D974 / D664
Rust prevention, 24h Pass D665A and D665B
Copper corrosion, 3h at 100°C, max 2 D130
Water separability
time (mins) to 3ml emulsion max at 54°C 30 30 30 30 30 30 - - D1401
time (mins) to 3ml emulsion at 82°C - - - - - - 60 60
Elastomer compatibility
100 ± 1°C/288 ± 2h, SRE-NBR 1 Elastomer
(DIN53 538, Part 2 or AAMA 524, Part 2) D471
Relative volume change, %A Report Report 0 to 15 0 to 12 0 to 12 0 to 10 0 to 10 0 to 10
Change in Shore A hardness, ratingA Report Report 0 to -8 0 to -7 0 to -7 0 to -6 0 to -6 0 to -6
Foam
Seq I, ml max 150/0
D892
Seq II, ml max 75/0
Seq III, ml max 150/0
These numbers are provisional; ASTM is trying to establish a technical consensus for possible revision.
A
01/08 - Industrial - 20
ASTM D6158 2005
Test ASTM Method
Air release
time (mins) at 50°C, max 5 5 5 5 10 13 - - D3427
time (mins) at 75°C, max - - - - - - Report Report
Oxidation stability time for acid number
1000 D943
of 2mg KOH/g, h, min
Sludge tendancy
Total insoluble sludge, mg, max 200 D4310
Copper oil/water/sludge, mg Report
Thermal stability
Copper appearance, visual Report Report Report 5 5 5 Report Report
D2070
Steel appearance, visual Report Report Report 1 1 1 Report Report
Sludge, mg/100ml Report Report Report 25 25 25 Report Report
Wear protection
Weight loss vanes + ring, mg,
- - Report Report Report - - -
max at 65 6°C/100H D7043
Weight loss vanes + ring, mg,
- - - - - Report Report Report
max at 79 4°C/100H
01/08 - Industrial - 21
ISO 11158 Hydraulic Fluids (1) 15 December 97
Test HH HL HG Test Method
ISO VG 10 15 22 32 46 68 100 150 10 15 22 32 46 68 100 150 32 68
Kinematic Viscosity at 40°C, mm2/s In Grade In Grade In Grade ISO 3104 and 3105
Viscosity Index Report Report Report ISO 2909
Density at 15°C, kg/dm3 Report Report Report ISO 3675
Colour Report Report Report ISO 2049
Appearance at 25°C Clear and Bright Clear and Bright Clbr Visual
Total Acid Number, mg KOH/g, max 0.1 Report Report ISO 6618
Water content, %m/m, max 0.5 0.5 0.5 ISO 6614
Foam Test, Sequence I, ml, max 150/0 150/0
Sequence II, ml, max 75/0 75/0 ISO 6247
Sequence III, ml, max 150/0 150/0
Flash Point (COC), °C, min 100 140 140 160 180 180 180 180 100 140 140 160 180 180 180 180 160 180 ISO 2592
Flash Point (PMCC), °C, min 88 128 128 148 168 168 168 168 88 128 128 148 168 168 168 168 148 168 ISO 2719
Air Release at 50°C, mins, max 5 ISO 9120
Copper corrosion (3h at 100°C), rating, max 2 2 ISO 2160
Rust prevention, procedure A Pass Pass ISO 7120
Pour Point, °C, min -15 -12 -9 -6 -6 -6 -6 -6 -30 -21 -18 -15 -12 -12 -12 -12 -9 -9 ISO 3016
Water Separation
Time to 3mls emulsion at 54°C, mins, max Report 30 ISO 6614
Time to 3mls emulsion at 82°C, mins, max Report 30
Elastomer compatibility (2) Report Report Report ISO 6072
Oxidation Stability, 1000 hours
Delta acid number, mg KOH/g, max 2.0 ASTM D4310
Insoluble sludge, mg Report
Wear Protection, FZG A/8.3/90, fail stage 10 DIN 5134-2
Vane pump, mg, Report ASTM D2882
Notes :
(1) ISO 11184 replaces AFNOR NF E 48-603 Parts 1 and 2.
(2) The type of elastomer and definition of compatibility are to be agreed between the supplier and end user.
01/08 - Industrial - 22
JCMAS HK (JCHASP 041:2004) Hydraulic Fluid for
Construction Machinery 2004
01/08 - Industrial - 23
JCMAS HK (JCHASP 041:2004) Hydraulic Fluid for
Construction Machinery 2004
DIN51354
Load Carrying Capacity D5182
Part 2
FZG A/8, 3/90 Stage 8 min
High pressure piston Pump Test3
Komatsu HPV 35+35 Pump Pass (evaluate change of flow
JCMAS
Test (34.3MPa/2100rpm/95°C/ rate and used oil and wear
P044
62.5L500hr) of pump parts)
OR Rexworth A2F10 Pump Test
JCMAS
(35MPa/1500rpm/80°C/13L/Cu
P045
Cat./500hr)
Viscosity Increase Ratio D445 % 10 max
Acid Number Increase D974 mgKOH/g 2.0 max
Sludge, 0.8 µ Filter JIS B 9931 mg/100ml 10 max
Vane Pump Test Vickers4
Vickers 35VQ25 Pump Test D6973
Ring Wear - mg 75 max
Vane Wear - mg 15 max
OR Vickers V104C Pump Test D2882
Wear (ring + vane) - mg 50 max
Friction Characteristics5
JCMAS
Micron Clutch Test 0.08 min
P047
OR SAE No.2 clutch test (1000 JCMAS
0.07 min
cycles), µs P047
01/08 - Industrial - 24
British Standard Specification BS 489: 1999 R & O Turbine Oils
01/08 - Industrial - 25
AGMA 9005-E02 - Extreme Pressure Gear Lubricants December 2002
Test Test Method Requirements
ASTM
Viscosity grade D2422 32 46 68 100 150 220 320 460 680 1000-3200 > 3200
Viscosity at 40 ºC, mm2/s D445 28.8-35.2 41.4-50.6 61.2-74.8 90.0-110 135-165 198-242 288-352 414-506 612-748 900-2420 2880-3520
Viscosity at 100 ºC, mm2/s D445 Report
Viscosity index, min. D2270 90 85 Report
Bulk fluid dynamic viscosity at cold start-up,
D2983 150,000
mPa/s, max.
Flash point, ºC, min D92 180 200
Resistance to aging at 121 ºC - max,
D2893 6 8 10 15 Report
% increase in kinematic viscosity at 100 ºC
Water content, ppm, max D6304 300 Report
Foam suppression - 5 Minutes 10 Minutes 5 Minutes 10 Minutes
Volume of foam (ml), max. after: Blow Settle Blow Settle
Seq I at 24ºC D892 50 0 75 10
Seq II at 93.5ºC 50 0 75 10
Seq III at 24ºC 50 0 75 10
Cleanliness None visual Must be free of visible suspended or settled contaminants at the time it is installed for use
Water separation
% H2O in oil after 5h test, max 2.0 2.0 Report
D2711
Cuff after centrifuging, ml, max 1.0 4.0 Report
(Procedure B)
Total free H2O collected during entire test,
80.0 50.0 Report
starting with 90 ml H2O, ml, min.
Rust prevention, Part B D665 Pass
Copper corrosion prevention,
D130 1b
3h @ 100 ºC, rating, max
Scuffing load capacity, FZG visual method,
D5182 10 12 >12
A/8.3/90, fail stage, min
01/08 - Industrial - 26
AIST (US Steel) Requirements No. 224 Lead Free E.P. Gear Oil
Test Limits
API Gravity, D-287 25 min.
Viscosity Index, D-567 95 min.
Precipitation Number, D-91 Trace
Pour Point, D-97 -9°C max. (based on viscosity)
C.O.C. Flash Point, D-92
ISO Grade 150 and up 232.2°C min.
ISO Grade 68 and 100 203.4°C min.
3 Hour Copper Strip Corrosion, D-130 1b max.
Rust Test (A & B), D-665 Pass
S-200 Oxidation - 312 hours at 121.1°C (250°F)
Viscosity Increase at 98.9°C (210°F) 6% max.
Precipitation Number After Test 0.1% max.
Demulsibility, D-2711
Free Water 80.0 ml min.
Emulsion 1.0 ml max.
H2O in Oil 2.0% max.
Four Ball E.P. Test, D-2783
Load Wear Index 45 kg min.
Weld Point 250 kg min.
Four Ball Wear Test, D-2266
20 kg. at 1800 rpm for 1 hour Scar Diameter -0.35 mm max.
Timken Load Arm Test, D-2782 O.K. 60 lbs min.
FZG - Four Square Gear Test 11th stage min.
01/08 - Industrial - 27
David Brown Number S1.53 101 January 1985
Scope: This specification covers the requirements for ten grades and three classifica-
tions of mineral based lubricating oils for use in DAVID
BROWN enclosed gear units. The grades are numbered 0 to 9
and will be associated with a classification character.
Description: The lubricants shall be stable homogeneous blends of highly refined mineral
oils and additives. They should not contain any grit, abrasives, sediments or
other impurities. The lubricants should be branded products on general sale
or intended to be so.
Classification: For mineral based lubricant the following general classifications will be used:
Type E These lubricants will contain additives which are designed to improve
the load carrying properties of the base oil. They should not contain
any lead or lead based additives.
The requirements for all three lubricant types are the same or similar
in all respects except for carrying capacity.
01/08 Industrial - 28
David Brown Requirements for a Mineral Based Lubricant
DBGI Lubricant Grade
Title Test Method Conditions
Limit 0 1 2 3 4 5 6 7 8 9
Kinematic IP 71, ASTM D445 at 40°C min. 24.5 36.0 52.8 77.6 114 167 245 360 528 776
Viscosity mm2/s at 40°C max. 36.0 52.8 77.6 114 167 245 360 528 776 1140
at 100°C min. 5.1 6.4 8.1 10.5 13.6 17.4 22.3 28.5 36.5 46.2
Viscosity Index IP 226, ASTM 2270 min. 90 90 90 90 90 90 90 90 90 90
Pour Point (°C) IP 15, ASTM D97 max. -6 -6 -6 -6 -6 -3 -3 0 0 0
Load Carrying IP 334, A/8.3/90 FZG Load Stage
Capacity (Visual method) at which damage occurs
Lubricant Type M min. 5 5 6 6 6 6 7 7 7 7
Lubricant Type A min. 7 7 8 8 8 9 9 9 10 10
Lubricant Type E min. 11 11 12 12 12 12 12 > 12 > 12 > 12
Copper Strip Classification
Corrosion IP 154, ASTM D130 max. 1b 1b 1b 1b 1b 1b 1b 1b 1b 1b
after 3 hrs. at 100°C
Corrosion IP 135, ASTM D665 Rust Prevention in the
presence of water for 24hrs.
Lubricant Type M Pass PROCEDURES A AND B
Lubricant Types A & E Pass PROCEDURE A
Report DEGREE OF RUSTING - PROCEDURE B
Oxidation Stability ASTM D2893, % Change in Kinematic
max. 10 10 10 10 10 10 10 10 10 10
(at 95°C) Viscosity at 100°C
01/09 - Industrial - 29
David Brown Requirements for a Mineral Based Lubricant
DBGI Lubricant Grade
Title Test Method Conditions
Limit 0 1 2 3 4 5 6 7 8 9
Foam IP 146, ASTM D892 Volume of Foam (ml)
Tendency/Stability Sequence I (24°C)
After 5 mins blow max. 75 75 75 75 75 75 75 75 75 75
After 10 mins rest max. 10 10 10 10 10 10 10 10 10 10
Sequence II (93°C)
After 5 mins blow max. 75 75 75 75 75 75 75 75 75 75
After 10 mins rest max. 10 10 10 10 10 10 10 10 10 10
Sequence III (24°C)
After 5 mins blow max. 75 75 75 75 75 75 75 75 75 75
After 10 mins rest max. 10 10 10 10 10 10 10 10 10 10
Air Release IP 313 Minutes at 50°C max. 9 10 12 18 30 - - - - -
Minutes at 90°C max. - - - - - 9 10 12 16 24
Demulsibility ASTM D2711 Lubricant Types M & A
Water in Oil (%) max. 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5
Emulsion (ml) max. 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0
Total Free Water (ml) min. 30.0 30.0 30.0 30.0 30.0 300 30.0 30.0 30.0 30.0
ASTM D2711 Lubricant Type E
Appendix 12 Water in Oil (%) max. 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0
Emulsion in Oil (ml) max. 2.0 2.0 2.0 2.0 2.0 2.0 2.0 4.0 4.0 4.0
Total Free Water (ml)
min. 60.0 60.0 60.0 60.0 60.0 60.0 60.0 50.0 50.0 50.0
(Report average result)
01/09 - Industrial - 30
DIN 51517 Part 3 - Lubricating Oils CLP January 2004
Lubricant Type CLP 32 CLP 46 CLP 68 CLP 100 CLP 150 CLP 220 CLP 320 CLP 460 CLP 680 CLP 1000 CLP 1500 Test Method
Viscosity Grade 32 46 68 100 150 220 320 460 680 1000 1500 -
Viscosity at 40ºC, mm2/s 28.8-35.2 41.4-50.6 61.2-74.8 90-110 135-165 198-242 288-352 414-506 612-748 900-1100 1350-1650 DIN EN ISO 3104
Viscosity Index 90 85 DIN/ISO 2909
Flash Point (COC), ºC 180 200 DIN EN ISO 2592
Pour Point ºC -12 -9 -3 DIN/ISO 3016
Neutralisation Number, mg KOH/g Report DIN 51558-1
Density at 15ºC, kg/m3 Report DIN 51757
Water Content, % <0.1 max DIN/ISO 3733
Foam after 10 minutes, Sequence I, II & III 100/10 150/60 ISO 6427
Water Seperability, minutes, max. 30 60 DIN/ISO 6614
Copper Corrosion, 3 hours at 100ºC 1 max. DIN EN ISO 2160
Steel Corrosion, Method A Pass DIN/ISO 7120
Oxidation Stability, 95ºC for 312hrs 6 max.
ASTM D2893
Increase in viscosity at 100ºC, %
FZG Scuffing test, A/8.3/90 12 Fail min. DIN 51354-2
FAG FE-8 bearing wear test
Roller wear, mg 30 max. DIN 51819-3
Cage wear, mg Report
Compatibility with Seals SRE-NBR 28,
7 days @ 100ºC
Relative change in volume, % max. -5 to 10
DIN 53538-3
Change of Shore A hardness, % max. -10 to 10
Change of Tensile strength, % max. 30
Change of Elongation, % max. 40
01/09 - Industrial - 31
Flender Requirements Revision 9 06-12-2005
Lubricant Type Mineral Synthetic Test Method
* Flender has a basic requirement for oil to meet CLP quality in accordance with DIN 51517 Part III.
Latest DIN specification is dated January 2004.
** ≥10 is based on a profile deviation measurement only. Flender have now updated the micropitting requirements
as follows: In addition to profile deviation measurement, Flender now also specifically requires a GF class ‘high’
evaluated by a secondary evaluation method of the FVA 54/ 7 method looking at weight loss and micropitting area.
Also Flender now requires a stabilization of weight loss values and micropitting levels in the endurance phase.
The specification will be updated to reflect the change in requirements.
01/09 - Industrial - 32
Denison Biofluid Requirements - TP30560 5 March 2007
Test HF-6 Test Method
Viscosity cSt at 40°C Report D445
Viscosity cSt at 100°C Report D445
Viscosity index, min 90 D2270
Gravity API (Specific) 840 to 900
Zinc, % wt Report
Pour Point, °C Report D97
Aniline Point > 100°C (3) D611
Flash Point, °C Report D92
Acid Number Report D664
Rust Test
Distilled Water No rust D665A
Synthetic Sea Water No rust D665 B
Foam
None D892
Allowable Foam after 10mn
Filterability ()
1
(2) Instructions available on request: Same as used in Military specification MIL-H-24459 Appendixes A & B.
(3) If < 100°C to do seal test DIN 51524.
(4) 600 seconds maximum. Do not exceed twice the filtration time without water.
(5) Viscosity at 40°C (Start - End) > 40 cSt for ISO 46 (-8 cSt)
01/08 - Industrial - 33
ISO 12925-1 Enclosed Gears of Category CKC 1996
Test Specifications Test Method
Viscosity grade VG 32 VG 46 VG 68 VG 100 VG 150 VG 220 VG 320 VG 460 VG 680 VG 1000 VG 1500 ISO 3448
Appearance Bright & Clear Bright & Clear Bright & Clear Bright & Clear Bright & Clear Bright Bright Bright Bright Bright Bright (1)
Viscosity index, min 90 90 90 90 90 90 90 90 85 85 85 ISO 2909
Pour point °C, max -12 -12 -12 -12 -9 -9 -9 -9 -3 -3 -3 ISO 3016
Flash point °C, min 180 180 180 200 200 200 200 200 200 200 200 ISO 2592
Foaming tendancy / stability, max ml 100/10 100/10 100/10 100/10 100/10 100/10 100/10 100/10 100/10 100/10 100/10 ISO 6247
Copper corrosion, 3h at 100°C, max 1 1 1 1 1 1 1 1 1 1 1 ISO 2160
Demulsibility:
Method: Appendix X2 modification
(90 ml water at start):
ASTM D2711
Free water, min ml 80 80 80 80 80 80 80 80 80 80 80
Emulsion, max ml 1 1 1 1 1 1 1 1 1 1 1
Water-in-oil, max ml 2 2 2 2 2 2 2 2 2 2 2
Rust test: Methods A and B Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass ISO 7120
Oxidation stability at 95°C
Viscosity increase at 100°C, max % 6 6 6 6 6 6 6 6 6 6 6 ASTM D2893
Precipitation number, max 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1
Load-carrying property
FZG A/8, 3/90 °C 12 12 12 12 12 12 12 12 12 12 12 DIN 51354-2
Fail stage, min
(1) There is presently no accepted test method. Visual observation is to be reported as indicated. The objective is to ensure that the lubricant does not appear turbid or contain suspended
or settled impurities.
ISO 12925-1 Standard also covers other types of gear oils. Refer to official standard for further information.
01/08 - Industrial - 34
SEB 181226 Industrial Gear Specification July 2001
Specification CLP Type Oils Test Method
01/08 - Industrial - 35
Air Compressor Lubricant Standard DIN 51506 Table 1 September 1985
Compressed Air Temperature °C maximum
For compressors on moving equipment For compressors with storage tanks
Oil Classification for brakes, signals and tippers and pipe network systems
VDL 220 220
VC
220 160(1)
VCL
VB
140 140
VBL
Note:
(1) Some types of compressors up to 180°C with VCL or engine oils.
01/08 - Industrial - 36
Air Compressor Lubricant Standard DIN 51506 September 1985
Lube Oil Group VB and VBL VC and VCL
ISO Viscosity Grade 22 32 46 68 100 150 220 320 460 32 46 68 100 150
Kinematic Viscosity min. 19.8 28.8 41.4 61.2 90 135 198 288 414 28.8 41.4 61.2 90 135
(DIN 51561) to to to to to to to to to to to to to to
at 40°C, mm2/s max. 24.2 35.2 50.6 74.8 110 165 242 352 506 35.2 50.6 74.8 110 165
at 100°C, mm2/s, min. 4.3 5.4 6.6 8.8 11 15 19 23 30 5.4 6.6 8.8 11 15
Flash Point, °C (COC) min.
175 195 205 210 225 255 175 195 205 210
(ISO 2592)
Pour Point, °C, max. (ISO 3016) -9 -3 0 -9 -3
Ash, % m/m, max. (DIN 51675) VB & VC: 0.02 oxide ash VBL, VCL sulphated ash to be specified by supplier
Water soluble Acids (DIN 51558) Neutral
TAN, mg KOH/g max.
VB & VC: 0.15 VBL, VCL to be specified by supplier
(DIN 51558 Part 1)
Water, % Mass (ISO 3733) 0.1 max.
% Mass CRC max. after air
2.0 2.5 1.5 2.0
ageing (DIN 51352 Part 1)
% Mass CRC max. of 20%
Not required 0.3 0.75
distillation residue (DIN 51535)
Note:
Grades VB and VC are pure mineral oils. Grade VDL contains additives to increase ageing resistance.
Grades VBL and VCL are HD type Engine oils which are used as mineral oils.
01/08 - Industrial - 37
Air Compressor Lubricant Standard DIN 51506 September 1985
Lube Oil Group VDL
ISO Viscosity Grade 32 46 68 100 150
Kinematic Viscosity (DIN 51561)
at 40°C, mm2/s 28.8 to 35.2 41.4 to 50.6 61.2 to 74.8 90 to 110 135 to 165
at 100°C, mm2/s, min. 5.4 6.6 8.8 11 15
Flash Point, °C (COC) min. (ISO 2592) 175 195 205 210
Pour Point, °C, max. (ISO 3016) -9 -3
Ash, % mass, max. (DIN 51575) Sulphated ash to be specified by supplier
Water soluble acids (DIN 51558) Neutral
TAN, mg KOH/g, max. (DIN 51558 Part 1) To be specified by supplier
Water, % mass (ISO 3733) 0.1 max.
% mass CRC max. after air ageing
Not required
(DIN 51352 Part 1)
% mass CRC max. after air/Fe2O3 ageing
2.5 3.0
(DIN 51352 Part 2)
% mass CRC max. of 20% distillation
0.3 0.6
residue (DIN 51356)
Kinematic Viscosity at 40°C max. of 20%
Maximum of five times the value of the new oil
distillation residue mm2/s (DIN 51535)
01/08 - Industrial - 38
General Motors Compressor Lubricant Standards November 2004
Specification Type Compressor and turbine oils Synthetic compressor / turbine oil - ester based Synthetic compressor / turbine oil - non ester ASTM
Method
Product Code LJ-03-1-04 LJ-04-1-04 LJ-06-1-04 LJ-10-1-04 LJ-03-2-04 LJ-04-2-04 LJ-06-2-04 LJ-10-2-04 LJ-03-3-04 LJ-04-3-04 LJ-06-3-04 LJ-10-3-04
01/08 - Industrial - 39
General Motors Compressor Lubricant Standards November 2004
Specification Type Compressor and turbine oils Synthetic compressor / turbine oil - ester based Synthetic compressor / turbine oil - non ester ASTM
Product Code LJ-03-1-04 LJ-04-1-04 LJ-06-1-04 LJ-10-1-04 LJ-03-2-04 LJ-04-2-04 LJ-06-2-04 LJ-10-2-04 LJ-03-3-04 LJ-04-3-04 LJ-06-3-04 LJ-10-3-04
01/08 - Industrial - 40
SAE MSI003-2 Compressor Oils January 2004
Requirements Ester based Polyalphaolefin based
Type of lubricating oil DEA DEB DEC DEG DEH DEJ DPA DPB DPC DPG DPH DPJ ASTM
ISO Viscosity Classification VG 32-150 VG32-100 D2422
Kinematic Viscosity at 40°C, mm2/s ISO Grade ± 10% ISO Grade ± 10% D445
Viscosity Index - 130 min D2270
Pour Point°C ≤ -20 ≤ -35 D97
Flash Point°C VG 32 ≥ 220 VG 32 ≥ 210
VG 46 ≥ 230 VG 46 ≥ 230
D92
VG 68 ≥ 240 VG 68, 100 ≥ 250
VG 100 - 150 ≥ 250
Demulsibility - 40/37/3 min 40/40/0 min D1401
Demulsibility
Water in oil after 5h Report Report Report ≤ 1%
D2711
Emulsion after centrifuge Report Report Report ≤ 2 ml
Total free water Report Report Report ≥ 60 ml
Water content, ppm D95
≤ 100 ≤ 100
D1744
Corrosive effect on steel Not exceeding degree of corrosion ISO 7120 - 0 - A Not exceeding degree of corrosion ISO 7120 - 0 - A D665A
Corrosive effect on copper 3 hours at 100°C Not exceeding degree of corrosion 1B: ISO 2160 - 100A3 Not exceeding degree of corrosion 1B: ISO 2160 - 100A3 D130
Foam Volume, in ml.
Seq I ≤ 50/0 ≤ 50/0
D892
Seq II ≤ 50/0 ≤ 50/0
Seq III ≤ 50/0 ≤ 50/0
Oxidation stability TAN < 2, hours 1000 1500 2000 1000 1500 2000 2000 3000 4000 2000 3000 4000 D943
Autoignition Temperature, °C 380 min E-659
01/08 - Industrial - 41
SAE MSI003-2 Compressor Oils January 2004
Requirements Ester based Polyalphaolefin based
Type of lubricating oil DEA DEB DEC DEG DEH DEJ DPA DPB DPC DPG DPH DPJ ASTM
D4052
Density at 15ºC in g/ml To be specified by the supplier To be specified by the supplier
D1298
Four ball wear test (40kg load)
- ≤ 0.4 - ≤ 0.4 D4172
wear scar diameter, mm
Behaviour towards sealant.
-10 to +10 -10 to +10 D471
Relative change in % volume
Behaviour towards sealant.
-7 to +10 -7 to +10 D471
Change in Shore hardness
Level of Contamination by solid particles, max 20/18/14 20/18/14
Thermal Stability
Comparative IR Scan Report Report
Acid Number Change 0.15 0.15
Viscosity Change ≤ 5% ≤ 5%
D2070
Sludge, mg / 100 ml ≤ 25 ≤ 25
Copper rod colour ≤5 ≤5
Copper weight loss, mg ≤ 10 ≤ 10
Steel rod colour (Cinn, Mil.) 1 max 1 max
Neutralization number to be run on base oil only, 0.5 max D664
mg KOH/g 1.0 max D974
01/08 - Industrial - 42
DIN 51515 Part 1 June 2001 and Part 2 November 2004
Specification DIN 51515-1 DIN 51515-2
L-TD L-TG Test Method
ISO Viscosity Grade 32 46 68 100 32 46 -
Viscosity at 40°C, mm2/s 28.8-35.2 41.1-50.6 61.2-74.8 90.0-100.0 28.8-35.2 41.4-50.6 ISO 3104
Density at 15°C kg/m3 To be given by supplier To be given by supplier ISO 3675
Flash Point (COC), °C, min 160 185 205 215 160 185 ISO 2592
Pour Point, °C, max -6 -6 ISO 3016
Neutralisation Value mg KOH/g To be given by supplier To be given by supplier ISO 6618
Foam
Seq I 450/0
ISO 6247
Seq II 100/0
Seq III 450/0
Air Release (IP 313), mins. 5 5 6 No limit 5 DIN 51381
Steam Demulsibility, seconds 300 300 DIN 51589-1
Copper Corrosion
3 hrs at 100°C 2 max. ISO 2160
3 hrs at 125°C 2 max.
Steel Corrosion, Method A Pass Pass ISO 7120
Life TOST, hours to TAN of 2.0 mg KOH/g 2000 1500 1000 3000 ISO 4263-1
RPVOT, mins 800 ASTM D2722
RPVOT (modified), % of time in unmodified test 85 ASTM D2722
Purity 20/17/14 20/17/14 ISO 4406
Water content ppm 150 150 ISO 12937
Ash (oxide ash), %mass To be given by supplier To be given by supplier ISO 6245
01/08 - Industrial - 43
US Steel Turbine Standard Requirements
Specification 120 125 ASTM Method
General Requirements Good oxidation and corrosion resistance, water separation.
Suitable for producing oxidation stability, anti-foaming,
Compounding D88
rust protection and ordinary water separation.
Suitable for the application Suitable for the application intended. ASTM grades 150, 815,
Viscosity
465, 700 or 1000 at 100 °F suggested
Viscosity Index > 100 > 20 D567
API Gravity > 30 > 80 D287
Pour Point 20 ºF Max, Lower dependent upon application > 20 ºF. Lower dependent upon application. D97
COC Flash Point 375 °F Min > 375 °F D92
Rust Prevention Pass Pass D665
Oxidation Test Not to exceed 1.0 neutralization number after 1000 hours Not to exceed 2.0 neutralization number after 1000 hours D943
Minutes ml Oil ml Water ml Emulsion Minutes ml Oil ml Water ml Emulsion
Emulsion Characteristics @ 130°F D1401
≤ 20 40 37 3 ≤40 40 37 3
Field Test — Satisfactory for the application intended
01/08 - Industrial - 44
British Standard Specification BS 489: 1999 R & O Turbine Oils
01/08 - Industrial - 45
GEK Turbine Specifications
Specification GEK 107395a GEK 46357E GEK 46506D ASTM
01/08 - Industrial - 46
GEK Turbine Specifications
Specification GEK 107395a GEK 46357E GEK 46506D ASTM
01/08 - Industrial - 47
Mitsubishi Heavy Industry Turbine Specifications
Specifications High Temperature Turbines with EP High Temperature Turbines Steam and Low Temperature Test Method
Bearing Ambients Above 250ºC with Bearing Ambients Above 250ºC Turbine Applications
MS04-MA-CL002(R-1) MS04-MA-CL003(R-1) MS04-MA-CL001(R-1)
19th January 2007 21st August 2006 19th January 2007
Kinematic Viscosity
at 40°C, mm2/s 28.8~35.2 28.8~35.2 28.8 to 35.2 D445
at 100°C, mm2/s min. 5.0 min. 5.0 min. 5.0
Viscosity Index min. 95 min. 95 min. 95 -
Colour, Rating max. L1.0 max. L1.0 max. L1.0 D1500
Pour Point, °C max. -12 max. -12 max. -12 D97
Density at 15°C, g/cm3 Report Report Report D1289
Flash Point
Cleveland Open Cup, °C, min 200 200 200 D92
Pensky-Martens Closed Cup, °C Report Report Report D93
Acid Number, mg KOH/g, max 0.2 0.2 0.2 D974
Rust-preventing characteristics
Pass Pass Pass D665B
Synthetic sea water, after 24h at 60°C
Foaming
Seq I, 24°C, ml, max 50/0 50/0 150/0
D892
Seq II, 93.5°C, ml, max 50/0 50/0 50/0
Seq III, 24°C, ml, max 50/0 50/0 150/0
01/08 - Industrial - 48
Mitsubishi Heavy Industry Turbine Specifications
Specifications High Temperature Turbines with EP High Temperature Turbines Steam and Low Temperature Test Method
Bearing Ambients Above 250ºC with Bearing Ambients Above 250ºC Turbine Applications
MS04-MA-CL002(R-1) MS04-MA-CL003(R-1) MS04-MA-CL001(R-1)
19th January 2007 21st August 2006 19th January 2007
Oxidation Stability
1st method 0.4 0.4 0.4 D4310
Acid Number after 1000h, mgKOH/g, max
2nd method
4000 4000 2000 D943
Time to Acid Number of 2.0, hr, min
3rd method (dry -TOST at 120°C)
Sludge formation, mg/kg (1um filter), max 100mg/kg at 25%RPVOT 100mg/kg at 50%RPVOT 100mg/kg at 25%RPVOT -
Dry TOST life, hrs, min 500 at 25%RPVOT 700 at 50%RPVOT 400 at 25%RPVOT
RPVOT at 150°C, min 700 700 220
D2272
Modified RPVOT, % 85% of time in unmodified test 85% of time in unmodified test
Mixture stability - 1
Dry -TOST at 150°C of New oil / Report - Report -
Tested oil (Ratio: 50/50)1,%
Mixture stability - 2
Dry -TOST at 120°C of New oil /
100mg/kg at 25% RPVOT - 100mg/kg at 25% RPVOT -
Tested Oil (Ratio: 50/50)1
sludge formation mg/kg, max
Air Release
4 4 4 D3427
- 0.2% air at 50°C, mins, max
Water Separability
30 30 30 D1401
at 54°C, time to 3ml emulsion, mins, max
Corrosiveness to Copper, 3h at 100°C, rating, max 1 1 1 D130
Carbon Residue, mass %, max 0.05 0.05 0.1 D4530
Total Sulfur, ppm, max 1000 1000 Report (typically max.1000) D2622
Zinc Content, ppm, max 10 10 60 D5185
Evaporation Loss 760mmHg,
10 10 - D972
22h at 150°C, mass %, max
FZG Gear Ring Test, Failure load stage, min - 9 - D5182
1
Tested oil: The oil tested by dry TOST at 120°C until RPVOT value reaches 50% or less of new oil.
01/08 - Industrial - 49
OEM Turbine Specifications
Specification ALSTOM HTGD 90 117 V0001U Siemens TLV 9013 04:1999 Solar ES 9-224 Test Method
20th July 2005 July 1999 October 1999 ASTM
Viscosity Grade ISO 32 ISO 46 ISO 68 ISO 32 ISO 46 ISO 32 ISO 46 -
Viscosity at 40°C, mm2/s 28.8-35.2 41.1-50.6 61.2-74.8 28.8-35.2 41.4-50.6 28.8-35.2 41.4-50.6 D445
Viscosity index 90 min. D2270
Density at 15°C kg/m3, max 880 900 900 D941 / D1298
Flash Point (COC), °C, min 200 205 160 185 199 D92
Fire Point 227 232
Auto ignition temperature 310 E659
Pour Point, °C, max -9 -6 -6 D97
Colour, max 2 D1500
Neutralisation Value mg KOH/g
Without EP additive, max 0.2 0.20 D664 / D974
With EP additive, max 0.3 0.30
Foam
Seq I 300/0 400/450
D892
Seq II 50/0
Seq III 300/0
Air Release (IP 313), mins. 4 max. 7 max. 4 max. 5 6 D3427
Demulse Time to 40.37.3 at 54°C, mins 30 max. 20 max. 30 max to 40-40-0 D1401
Steam Demulsibility, (IP19) seconds 300 max. 300 max.
Copper Corrosion, 3 hrs at 100°C 2 max. 2 max. 1b D130
Steel Corrosion, Method B Pass Pass Pass D665
Life TOST, hours to TAN of 2.0 mg KOH/g At 2000h≤ 1 2500 min. 2000 min. D943
RBOT, mins > 300 Report D2272
Purity Class --/18/15 ≤17/14 ISO4406
Water content ppm < 200 ≤ 100 mg/kg D1533 / D1744
01/08 - Industrial - 50
OEM Turbine Specifications
Specification VERSION U Siemens TLV 9013 04:1999 Solar ES 9-224 Test Method
20th July 2005 July 1999 October 1999 ASTM
Filterability
Level 1% At least 93 ISO 13357-2
Level 2% At least 85
Zinc Content ≤ 5 ppm 0.005% wt. Optional
FZG A/8.3/90 8 fail min.1 8 fail min.1 6 fail min. 7 fail min. D5182
4 Ball wear, 1hr/120rpm/75C mwsd, mm 0.9
Resistivity, min@ 20°C, Ωm Report D1169
1
Additional requirements on turbine oils used in gear boxes.
01/08 - Industrial - 51
US Military MIL-PRF-17331J March 2007
Test Requirement Test Method
Acid Number, mg KOH/g oil, max 0.3 D974
Corrosion (in presence of salt water) None D665, Procedure B (1)
Corrosion test at 100°C (212°F), D130
Copper strip appearance, max 1
Bearing compatibility Pass FED (STD) 791 Method 3452
Oil Compatibility Pass (2)
Water, % None D95
Air release at 50°C, minutes. max 20 D3427
Flash point, °C (°F), min 204 (400) D92
Pour point, °C (°F), max -6 (20) D97, D5950
Viscosity cSt st 4.4°C (40°F), max 870 D445
Viscosity cSt st 40°C (104°F) 74 - 97 D445
Viscosity cSt st 100°C (212°F), min 8.0 D445
Demulsification at 30 minutes
41/-/3 D1401
Oil layer/water layer/emulsion, maximum
Oxidation test, time required in hours to reach
neutralization value of 2.0 mg KOH, min 1000 D943
1000 Hours TOST Test
Total sludge, mg maximum 100
D4310
Total iron, mg maximum 100
Total copper, mg maximum 100
Oxidation by rotating pressurised vessel Report D2272
Scuffing Load Capacity (FZG), Failure Load Stage Load Stage 9 D5182
4-Ball Wear Test, scar diameter, mm 0.33 D4172
max 15kg/80°C/600rpm/2h
Homogeneity, separation None Refer to actual specification
Foam characteristics, after blowing/after 10 minutes
Seq I, ml max 65/0
D892
Seq II, ml max 65/0
Seq III, ml max 65/0
Cleanliness, mg/100 ml max 4.0 D4898
Valve sticking characteristics Pass Refer to actual specification
Sulfur, % Report D129
Gravity, API Report D287
(1) Prior to the test, the oil shall be water - washed as follows: 300 grams of the oil to be tested shall be stirred with 50
grams of water for 30 minutes at 90°C (194°F) using the beaker and stirrer as specified in ASTM D665. After 30 minutes
stirring, the mixture shall be transferred to a separatory funnel and left to separate; then the water layer shall be drawn
off and the oil submitted to the salt-water corrosion test. The test shall be run for 24 hours.
(2) Oil compatibility. Oil shall be considered compatible with the referenced oils furnished by the Government if 1:1
mixtures of a test oil with all reference oil give passing values on the oxidation (ASTM D943), corrosion (salt water),
foam and emulsion tests.
01/08 - Industrial - 52
European Slideway Specifications
ISO 19 378 (2003) AFNOR E 60-203
Lubricants, industrial oils and related products: Lubricants, industrial oils and related products: Test Method
(Class L) - Machine Tool Lubricants - lubricants for lubrication and control of machine tools
Categories and Specifications and similar equipment, characteristics
01/08 - Industrial - 53
US Slideway Specifications
Specification CM P-53 CM P-47 CM P-50 GM LS2 (04) MIL-A-A-59113
Combination Heavy-Medium Heavy Way Oil GM Lubricant standard No. LW-03-1-04, LW-06-1-04, Lubricating oil, machine
Hydraulic & Way Oil Way Oil LW-22-1-04 Light, Medium and Heavy Way Oils tool slideways Test Method
01/08 - Industrial - 54
US Slideway Specifications
Specification CM P-53 CM P-47 CM P-50 GM LS2 (04) MIL-A-A-59113
Combination Heavy-Medium Heavy Way Oil GM Lubricant standard No. LW-03-1-04, LW-06-1-04, Lubricating oil, machine
Hydraulic & Way Oil Way Oil LW-22-1-04 Light, Medium and Heavy Way Oils tool slideways
01/08 - Industrial - 55
Off-highway
Off-highway
Contents Off-highway
STOU Specifications:
UTTO Specifications:
01/08 - Off-highway - 1
STOU Specifications (Super Tractor Oil Universal)
Test Massey Ferguson Ford John Deere
CMS-M1139 ESN-M2C-159-B J27
(April 1978) (July 1984) (January 1992)
API Engine Performance CD CD/SE CD/CE
Kinematic Viscosity, 100°C, mm2/s 10.1 - 12.0 B1 10W-30 SAE 10W-30
B2 15W-30 SAE 15W-40
B3 20W-40
Viscosity -18°C (Brookfield), mPa.s, max. 8000 NR NR
Pour Point, °C, max. -30 NR -33 (10W-30)
-30 (15W-40)
Flash Point, °C, min. (ASTM D92) NR 190 NR
Shear Stability
IP297/77, % loss at 100°C, max. NR 10 NR
JDQ102, Viscosity at 100°C, mm2/s NR NR 7.1
Foaming: (ASTM D892)
Sequence I, ml max. NR 20/0 25/0 (30 sec.
Sequence II, ml max. NR 50/0 50/0 break
Sequence III, ml max. NR 20/0 25/0 time)
Foaming with1% water added
Sequence I, ml max. 100/0 NR NR
Sequence II,ml max. 100/0 NR NR
Sequence III, ml max. 100/0 NR NR
Copper Strip Corrosion -
1a 1b NR
(3 hrs at 150°C, max.)
Rust Prevention:
ASTM D665A NR No Rust NR
MF Rust Test Pass NR NR
JDQ22, hrs min. - - 100
Oxidation Test (100 hrs at 150°C,)
Viscosity Increase at 100°C, %, max. 10 10 10
Sludging None NR None
Seal Test (168 hrs at 120°C)
Volume change, % 0 to +5 NR NR
Hardness change
+10 NR NR
(+ 21 days at 95°C), max.
Seal Test (70 hrs at 125°C)
Volume Change, % NR 0 to +10 NR
(1) Hardness Change, points NR ± 10
4-Ball
Wear Scar Diameter (1hr, 65°C,
0.4 0.4 NR
1500 rpm 40 kg), mm, max.
Load Wear Index, kg, min. 55 NR NR
IAE Gear Rig (2000 rpm, 110°C, 1pt/min.)
Scuff Load, kg, min. 52 NR NR
Water Sensitivity (0.5% v/v)
Sediment, ml, max. NR 0.1 0.1
Water Separation, max. NR Trace NR
Additive Loss (% mass), max. - - 15
Wet Brake Tests, various Pass Pass Pass
IPTO Clutch Tests, various Pass Pass Pass
Transmission Test Pass Pass Pass
Note: (1) 180° bend test on itself - No cracks.
01/08 - Off-highway - 2
STOU Specifications
01/08 - Off-highway - 3
UTTO Specifications
Test Massey Ferguson
M1127A M1127B M1135
(October 1980) (May 1969)
(U.S.A) (Europe)
Kinematic Viscosity, 100°C, mm2/s 11.0 max. 9.6 max. 10.3 - 11.7 (99°C)
Viscosity -18°C, cP (Brookfield) 6000 max. 4000 max. 10000 max.
Pour Point, °C - 30°C max. - 30 max. - 26 max.
Shear Stability, 100°C, mm2/s 8.8 min. 7.3 min. -
(ASTM D2603)
Viscosity Index 120 min. 95 min.
Copper Corrosion (3 hrs at 150°C) 1b max. 1a max.
(3 hrs at 121°C) 1a max.
Foaming (+ water):
Sequence I, ml 50/0 max. 100/0 max.
Sequence II, ml 50/0 max. 100/0 max.
Sequence III, ml 50/0 max. 100/0 max.
Seal Test (168 hours/120°C):
Volume % change 0.5 to 10 -2 to 5
Hardness (+21 days at 95°C) 10 IRHD max. 10 IRHD max.
Viscosity Stability on Heating; 100hrs at 150°C
% increase at 100°C 0 to 5 10 max.
Sludge nil nil
Steel Corrosion (MF methods):
Time to fail, hrs 100 min. -
Corrosion - nil
4 Ball Wear:
MWSD, mm (1 hr/65°C/1800 rpm/40 kg) 0.5 max.(1) -
MWSD, mm (1 hr/65°C/1500 rpm/40 kg) - 0.4 max.
4 Ball (ASTM D2783):
LWI 30 min.(1) -
Weld Point, kg 200 min.(1)
IAE Gear Rig
(2000 RPM/110°C/1 pint per min.):
Scuff Load, lb - 135 min.
MF Four Square Rig - Pass
Functional Tests Pass Pass
Note:
(1) Test as low temperature grade.
01/08 - Off-highway - 4
UTTO Specifications
Test Massey Ferguson Massey Ferguson
CMS-M1143 CMS-M1145
Kinematic Viscosity at 100°C / ISO 3104, mm2/s 13.5 13.5 max
Kinematic Viscosity at 100°C after shearing,
CEC L14A93 (250 cycles)
KV 100, mm2/s 9.0 min. 9.0 min
KRL (20h) CEC L45A99, mm2/s NR 6.8 min.
Dynamic Viscosity at -18°C ASTM D2983, mPa.s 4000 max. 4000 max.
Pour Point, ISO 3016, °C -34 max. -33 max.
Flash Point, (COC), ISO 2592, °C 200 min. 200 min.
Foaming Tendency/Stability NF T60-229
Sequence I (24°C), ml/ml 50/0 max. 50/0 max.
Sequence II (93°C), ml/ml 50/0 max. 50/0 max.
Sequence III (24°C), ml/ml 50/0 max. 50/0 max.
Copper Corrosion (3h/100°C), ISO 2160
Rating 1a max. 1a max.
Four Ball Wear (1h/40 daN), ASTM D4172
Scar Diameter, mm 0.4 max. 0.4 max.
Four Ball EP Test, ASTM D2783
Load Wear Index (LWI), kg 45 min. 47 min.
FZG Test (A/8.3/90), CEC LO7A95
Fail Stage 9 min. 9 Pass
Vickers V104C Vane Pump Test, NF E 48-617,
140 bar/250h/1460 rpm
Ring and Vane Weight Loss, mg 80 max. NR
Vickers 35VQ25 Vane Pump Test, ATS-373,
Cam weight loss, mg NR 40 max.
Vane weight loss, mg NR 15 max.
Rust Protection, ASTM D665B
Rating No Rust No Rust
Oxidation Test
192h/150°C, CEC L 48A00
KV 100°C change, % 25 max. 25 max.
Total Acid Number Change, % 75 max. 75 max.
Deposits None None
01/08 - Off-highway - 5
UTTO Specifications continued
Test Massey Ferguson Massey Ferguson
CMS-M1143 CMS-M1145
Elastomer Compatibility, CEC L 39T96
RE1 (150°C): Fluoro-elastomers
Var. in hardness DIDC, point 0/+5 0/+5
Var. in tensile strength, % -50/0 -50/0
Var. in elongation rupture, % -60/0 -60/0
Var. in volume, % 0/+5 0/+5
RE2 (150°C): ACM
Var. in hardness DIDC, point -5/+5 -5/+5
Var. in tensile strength, % -15/+10 -15/+10
Var. in elongation rupture, % -35/+10 -35/+10
Var. in volume, % -5/+5 -5/+5
RE3 (150°C): Silicone
Var. in hardness DIDC, point -25/0 -25/0
Var. in tensile strength, % -30/+10 -30/+10
Var. in elongation rupture, % -20/+10 -20/+10
Var. in volume, % 0/+30 0/+30
RE4 (150°C): NBR
Var. in hardness DIDC, point -5/+5 -5/+5
Var. in tensile strength, % -20/0 -20/0
Var. in elongation rupture, % -50/0 -50/0
Var. in volume, % -5/+5 -5/+5
Friction Test, Proprietary tests Pass CMS M1143 spec. Pass CMS M1145 spec.
Dry Filterability (mod. AFNOR), 1F 1.5 max. 1.5 max.
Wet Filterability (mod. AFNOR), 1F Report Report
Materials Compatibility, various NR Pass
01/08 - Off-highway - 6
UTTO Specifications(1)
Test Ford Ford John Deere
ESN-M2C-86C ESN-M2C-134D J20C(2) MS 1207
(European) (November 1989) (Revised Nov 2000) (Nov. 1986)
(U.S.A.) J20C J20D
Kinematic Viscosity, 100°C, mm2/s, min. 9.0 9.0 9.1 7.0 6.2
Viscosity -20°C (D2602) mPa.s, max. NR NR NR NR 3500
Viscosity -20°C (Brookfield) mPa.s, max. NR NR 5500 1500 NR
Viscosity -30°C (D2602) mPa.s NR NR NR NR 15,000 max.
Viscosity -18°C (Brookfield) mPa.s, max. 4000 4000 NR NR NR
Viscosity -35°C, mPa.s, max. NR NR 70000 NR NR
Viscosity -40ºC (Brookfield) mPa.s, max. NR NR NR 20,000 NR
Viscosity Index NR NR NR NR 95 - 115
Pour Point, °C, max. -37 -37 -36 -45 -37
Flash Point, °C, min. 190 190 200 150 195
Shear Stability % change, max., D3945 -16 -16 NR NR NR
Shear Stability % change, max., JD6102 NR NR 7.1 5.0 NR
Aniline Point NR NR NR NR 91 - 110
Foaming:
Sequence I, ml max. 20/0 20/0 25/0 25/0 50/10
Sequence II, ml max. 50/0 50/0 50/0 50/0 50/10
Sequence III, ml max. 20/0 20/0 25/0 25/0 50/10
Foam Break Time (secs): NR NR 30 max. 60 max NR
+ Water:
Sequence I, ml. max. NR NR NR NR 50/10
Sequence II, ml. max. NR NR NR NR 50/10
Sequence III, ml. max. NR NR NR NR 50/10
Copper Strip Corrosion 3 hrs at 150°C 2b max. 2b max. NR NR NR
Rust Prevention
ASTM D665A Pass Pass NR NR NR
Humidity Cabinet (min.) NR NR 100 hrs. 100 hrs. 100 hrs.
Oxidation Test (100 hrs at 150°C)
Viscosity Increase at 100°C, % max. Special
10 10 NR NR
Case Test
Oxidation Stability (JDQ 23)
Evaporation Loss (%) NR NR 5.0 max. 10 max. NR
Viscosity Increase (%) NR NR 10.0 max. 20 max. NR
Sludge Formation NR NR None None NR
Additive Separation NR NR None None NR
Seal Test (70 hrs at 125°C)
Volume Change, % 0 to +10 0 to +10 NR NR Various
Hardness Change ± 10 ± 10 NR NR Various
180° bend No cracks No cracks NR NR
4-Ball
MWSD, mm
(1 hr/65°C/1500 rpm/40 kg) max. 0.4 0.4 NR NR NR
Water Sensitivity
Sediment, ml. (% volume), max. 0.1 0.1 0.1 0.1
Special
Additive Loss (% mass), max. NR NR 15 15
Case Test
Water Separation, max. Trace Trace NR NR
Compatibility 50/50 mix Pass Pass Pass Pass Pass
Wet Brake Tests Various Pass Pass Pass Pass Pass
IPTO Clutch Tests Various Pass Pass Pass Pass NR
Transmission Tests Various Pass Pass Pass Pass Pass
Hydraulic Pump Tests Various Pass Pass Pass Pass NR
Drive Line Durability Various NR Pass NR NR Pass
Gear Wear Pass Pass Pass Pass Pass
Filterability NR NR NR Pass (-30ºC) Pass
Notes:
(1) UTTO = Universal Tractor Transmission Oil (not for tractor engines).
(2) J20D low viscosity UTTO for cold climates. Earlier UTTO specification versions on file.
01/08 - Off-highway - 7
UTTO Specifications
Test Case MS-1209 (Aug 1999)(1)
API Gravity, ASTM D1298 Report
Kinematic Viscosity at 100ºC, mm2/S, ASTM D445 6.20 min
Apparent Viscosity, cP, ASTM D2983
at -20 ºC 4500 max
at -30 ºC 25000 max
Viscosity Index, ASTM D2270 95-115
Flash point, ºC, ASTM D92 195 min
Pour point ºC, ASTM D97 -37 max
Colour, ASTM D1500 5.5-7.5
Trace Sediments, Volume %, ASTM D2273 0.005 max
Aniline point, ºC, ASTM D611 91-110
Water, Volume %, ASTM D95 0.1 max
Elemental Analysis, mass %
Barium, ASTM D4951 Report
Calcium, ASTM D4951 0.29 min
Chlorine, ASTM D1317 0.01 max
Magnesium, ASTM D4951 Report
Nitrogen Report
Phosphorus, ASTM D4951 0.04 min
Silicon, ASTM D4951 Report
Sodium. ASTM D4951 Report
Sulphur Report
Zinc, ASTM D4951 0.01 max
Foaming, ASTM D892
Sequence I, ml max 50/10
Sequence II, ml max 50/10
Sequence III, ml, max 50/10
Foam break time (secs) NR
Foaming with 1% water, CASE MT 803
Sequence I, ml max 50/10
Sequence II, ml max 50/10
Sequence III, ml, max 50/10
Air release time, minutes, 50ºC, ASTM D3427 13.5 max
Oxidation-corrosion, 190h at 145ºC, CASE MT 804
Aluminium, loss or deposit, mg 1.0 max
Copper, loss or deposit, mg 8.0 max
Brass, loss or deposit, mg 5.0 max
Steel, loss or deposit, mg 1.0 max
Precipitation number after test 0.01 max
Glassware rating A or B
Water Tolerance, Case MT 805
Precipitated volume, mL 0.2 max
Centrifuged volume, mL 0.1 max
Fluid Clarity Must be clear
Nephelometric Turbidity Units, NTU 75 max
Gear Wear, mass loss, mg, ASTM D4998 Equal to or better than reference fluid
Filterability, Case MT 807 Pass
01/08 - Off-highway - 8
UTTO Specifications continued
Test Case MS-1209 (Aug 1999)(1)
Fluid compatibility, 72h at 125ºC, Case MT808,50:50, 2 fluids to be tested
Evaporation loss, mass % 5.0 max
Viscosity Change at 100ºC, % +10 max
Sludge Formation or additive separation None allowed
Elastomer compatibility, aged fluid at 125ºC, modified ASTM D414,
2 reference elastomers
Volume change, % 0 to +10
Hardness change, points -5 to +5
Corrosion Resistance
Galvanic, 10 days @ 50% humidity, FTMS 5322.1 Pass
Humidity, 100 hours, Case MT 809 Pass
Hydrolytic Stability, Case MT 824
Appearance No clumps, no gel
Copper specimen appearance 1a or 1b
Volume of separated matter, mL, max 1.0
Fluid cleanliness, Case ES-B110 Level 2
Hydraulic Pump Performance, Case ES A7626 Pass
Frictional Performance Pass
Brake Noise (chatter) Pass
Gear performance Pass
Note:
(1) to qualify for requirements of Hy-Tran Ultra ®
01/08 - Off-highway - 9
UTTO
Test Case New Holland Case New Holland
MAT3525 rev D MAT3526 rev B
(134-D fluid) (F200-A fluid)
Kinematic Viscosity, mm2/s, ASTM D445
100ºC 9.1-9.8 8.5-9.0
40ºC, typical 55 35
Apparent Viscosity, -18ºC,
4000 4000
mm2/s, max, ASTM D2983
Viscosity index, min, ASTM D2270 130 130
Shear stability, 30 passes, min, %, ASTM D3945 -16 NR
Transmission/Hydraulic oil shear test,
NR 7.0
mm2/s, min, CNH 86548393
Thermal stability, 100hrs, 150ºC,
10 10
viscosity change, % max
Pour point, ºC, max, ASTM D97 -37 -45
Flash point, ºC, min, ASTM D92 190 160
Foaming, ASTM D892
Sequence I, ml, max 20/0 50/0
Sequence II, ml, max 50/0 50/0
Sequence III, ml, max 20/0 50/0
Copper Corrosion, 3hr, 150ºC, max, ASTM D130 2b 2b
Volatility, 48hr, 120ºC, weight loss, %, max 1.0 1.0
Rust protection, ASTM D665, method A Pass Pass
Wear test, 60 min, 1500 rpm, 85ºC, 40kg max,
0.40 0.40
scar diameter mm, ASTM D2266
Seal test, 70hr, 125ºC, ASTM D1414
Volume change, % -3 to +7 -3 to +7
Hardness change, IRHD points -5 to +5 -5 to +5
Water sensitivity (CNH test)
Sediment volume, ml 0.1 max 0.1 max
Water separation, ml Trace Trace
Jenkins cycle test, 600hr Pass Pass
Tandem pump durability test Pass Pass
16 x 16 Inching/Shifting test Pass Pass
16 x 16 Transmission, 400 cycle stall test Pass Pass
16 x 16 Transmission, 450 cycle high energy test Pass Pass
Field test, 2000hrs Pass Pass
Brake test Pass Pass
PTO clutch test Pass Pass
Dynamic co-efficient of friction 0.095-0.135 0.095-0.135
Static co-efficient of friction 0.085-0.110 0.085-0.110
Oil compatibility Pass Pass
01/08 - Off-highway - 10
Engine Tests
Engine Tests
Contents Engine Tests
European Tests:
PCMO
Mercedes Benz M111 Fuel Economy Test
Mercedes Benz M111 Sludge
Mercedes Benz M271 Sludge
Mercedes Benz M271 Wear
Mercedes Benz OM 602A
Mercedes Benz OM 611 DE22LA
Peugeot DV4 TD
Peugeot TU3M Valve Train Scuffing
Peugeot TU5JP-L4
VW Intercooled T/C Diesel
VW TDi Diesel
VW T4 (PV 1449)
HDDO
MAN D2876 LF04 (Meistersinger II)
Mercedes Benz OM 364LA
Mercedes Benz OM 441LA
Mercedes Benz OM 501LA
MWM KD 12E (MWM-B)
Volvo D12D
US Tests:
PCMO
Ball rust test
Sequence IIIF
Sequence IIIG
Sequence IVA
Sequence VG
Sequence VIB
Sequence VIII
Roller Follower Wear Test
HDDO
Caterpillar 1K
Caterpillar 1M-PC
Caterpillar 1N
Caterpillar 1P
Caterpillar C13
Cummins M11 - HST (obsolete)
Cummins M11 - EGR (obsolete)
Cummins ISB
Cummins ISM
Detroit Diesel 6V-92TA
Mack T-8/T-8E
Mack T-10 (obsolete)
Mack T-11
Mack T12
CEC L-54-T-96
Test The test procedure is based upon the ECE R15-04 and EUDC emissions
Conditions: test cycles. It uses flying flush oil systems to compare oils against a base
line calibration oil.
Method Fuel consumption through the test cycle is compared against that of a base
of Rating: line calibration oil
CEC L-53-T-95
Equipment Mercedes Benz M111 E20, four cylinder 2.0L gasoline injection with
Used: four valves per cylinder.
Special engine required (bearings, piston rings, tappets, cams, timing chain,
timing cover - cylinders differ in hardware set up).
Purpose: To evaluate the performance of engine oils to control the formation of black
sludge on engine internal surfaces. Also measured are piston deposits and
cam wear.
Fuel: RF-86-A-96.
MB In-house Method
Equipment 16 valve, 4 cylinder, 1.81 M271 E18 engine with port injection, intercooling
Used: and compressor supercharging
Purpose: To evaluate an oil’s ability to keep the engine free from sluge deposits
Test Following a 2.5 hour break-in, the engine is run for 250 hours with alternating
Conditions: hot and cold cycles. The maximum oil temperature is 145ºC.
Method Sludge rating of rocker cover, cylinder head, front cover, oil pan.
of Rating:
MB in-house Method
Equipment 16 valve, 4 cylinder, 1.81 M271 E18 engine with port injection, intercooling
Used: and compressor supercharging.
Purpose: To evaluate the ability of the oil to protect those components in the engine
that are susceptible to wear.
Test Following a 20.5 hour break-in, the engine is run for 250 hours with alternating
Conditions: test conditions. The maximum oil temperature is 145ºC.
Method Cam wear, piston ring wear, ring sticking, timing chain elongation,
of Rating: bore polishing, ring sticking, bearing wear.
CEC L-51-A-98
Equipment Mercedes Benz OM602A indirect injection, five cylinder in-line, turbocharged.
Used:
Purpose: To evaluate the performance of engine oils in respect of cam and cylinder wear
under a combination of stop and go, medium speed and high speed operating
conditions.
Test Complex test cycle of 60 mins., which is repeated 200 times giving a test
Conditions: duration of 200 hours.
Equipment OM 611 DE22LA 4 cylinder turbocharged and intercooled, 16V common rail
Used: direct injection engine
Purpose: To evaluate the protection offered by the oil against engine wear, sludge and
piston deposits.
CEC-L-093
Equipment 1.4L, 4 cylinder DV4 TD engine with Bosch EDC 16 common rail
Used: injection system.
Phase 1 Phase 2
Duration, mins 2 28
Speed, rpm 1100 400
Max. Torque, Nm 155
Boost Air Pressure, mbar 710
Boost Air Temperature, ºC 120
Oil Gallery Temperature 120
Oil Charge, g 4200
CEC L-38-A-94
Equipment OHC Peugeot TU3M, four cylinder gasoline engine, 1360cc, fitted with batch
Used: approved cams and followers.
Purpose: The method is used to evaluate the performance of engine oils in respect of
valve train scuffing in a combination of hot and cold running conditions.
Test The test comprises two individual sequences run under different test
Conditions: conditions.
Part A Part B
Duration, hrs. 40 60
Engine Speed, rpm. 1500 3000
Engine Torque, Nm. 10 35
Oil Temp., °C 40 100
Coolant Out Temp., °C 45 90
Fuel Consumption, kg/hr. 1.5 4.0
Fuel: RF 83-A-91
CEC-L-88-A-02
Equipment In-line four cylinder gasoline TU5JP engine with multi-point fuel injection and
Used: catalyst system at L4 depollution level.
Purpose: To evaluate high temperature deposits, ring sticking and oil thickening control
in a test that simulates high speed European highway driving.
Test Total test length of 72 hours consisting of six 12 hour, 2 stage cycles. Stage
Conditions: one is at wide open throttle, with an engine speed of 5600 rpm and oil
temperature of 150°C and Stage 2 is at idle. No oil top-up.
Stage 1 Stage 2
Duration. 11 hrs 50 mins 10 mins
Speed, rpm. 5600 Idle
Power, kW. 62
Coolant Outlet Temperature, °C 110
Exhaust Temperature, °C 860
Oil Temperature, °C 150
Fuel Specification RF 83-A-91
CEC L-46-T-93
Equipment VW four cylinder, 1.6 litre, turbocharged and intercooled diesel engine.
Used:
Purpose: Diesel detergency test for passenger car turbocharged diesel engines
run under high load conditions.
Method Pistons rated for groove and land deposits and for ring sticking
of Rating:
CEC L-78-T-99
Purpose: Diesel detergency test for passenger car diesel engines run
under high load conditions.
Method Pistons rated for groove and land deposits and for ring sticking
of Rating:
Equipment Four cylinder VW PV 1449 engine with digifant injection and ignition control.
Used:
Purpose: To evaluate the lubricant's ability to withstand oil oxidation and TBN depletion
under extended service conditions.
Test A two phase test consisting of 48 4-hour long three stage cycles, followed by
Conditions: 56 hours steady state, with no oil top-up.
Phase 1 Phase 2
1 2 3
Duration, hrs. 192 56
Duration, min. 120 72 48
Load,Nm. 159 80 idle 80
Temperature high high low high
Equipment Six cylinder MAN D2876 LF04 turbocharged Euro III engine with EGR,
Used: intercooler and reduced sump capacity.
Purpose: To evaluate the improvement in piston cleanliness, ring sticking and engine
deposits of the test oil versus a reference oil.
Stage 1 Stage 2
Duration, hrs. 35 65
Speed, rpm. 1900 1125
Power, kW. 338
Torque, Nm. 2100
Oil Charge, L 30
CEC L-42-T-99
Test The engine is run according to a cyclic procedure. Total duration 300 hours
Conditions: consisting of 3 x 100 hour phases of 20 x 21/2 hour cycles plus 50 hours
steady state.
CEC L-52-T-97
Purpose: To evaluate an oil's ability to prevent piston deposits and maintain engine
cleanliness in a low emission, high performance engine.
Test A 300 hour test with alternating and steady state cycles.
Conditions:
Equipment MWM KD 12E, single cylinder, naturally aspirated 850cc diesel engine.
Used: Compression ratio 22 to 1.
Purpose: To assess high performance diesel engine oils with respect to their
influence on piston cleanliness.
Method The three ring grooves and the first and second lands are assessed for
of Rating: deposits
Volvo TC415
Method Piston cleanliness, ring riding, bore polish and oil consumption.
of Rating:
ASTM D6557
Test The test simulates short trip service under typical winter conditions and
Conditions: correlates to the obsolete Sequence IID engine test. The oil is kept at a
temperature of 40°C. The balls are submerged in the oil for 18 hours,
during which time an air and acid mix is injected into the oil under controlled
flow rates.
Method The balls are rated either optically or by a computer or video system,
of Rating: for surface discolouration
ASTM D6984
Equipment 1996-97 3800 Series II General Motors V-6 gasoline engine, with an overhead
Used: valve design and equipped with an external oil sump cooler.
Purpose: The test simulates high-speed service, under relatively high ambient conditions
and evaluates the oil's performance with regards to oxidation induced oil
thickening, piston deposits and valve train wear.
Test The 100 hour long test is broken into 20 hour segments; at the end of each
Conditions: segment, an oil sample is taken and fresh oil is added.
Method Piston deposits, camshaft and lifter wear and increase in KV@40°C of the
of Rating: used oil
Equipment 1996-97 3800 Series II General Motors V-6 gasoline engine, with an overhead
Used: valve design and equipped with an external oil sump cooler.
Purpose: The test simulates high-speed service, under relatively high ambient conditions
and evaluates the oil's performance with regards to oxidation induced oil
thickening, piston deposits and valve train wear.
Test The 80 hour long test is broken into 10 hour segments; at the end of each
Conditions: segment, an oil sample is taken and measured for KV@40, and fresh oil
is added.
Method Piston deposits, camshaft and lifter wear, increase in KV@40°C of the used
of Rating: oil and low temperature used oil viscometrics
Equipment 1994 Nissan KA24E, in-line 4 cylinder engine with two inlet and one exhaust
Used: valve per cylinder.
Purpose: Designed to simulate excessive engine idling, this test measures the ability of
an oil to control camshaft lobe wear in engines equipped with an ovehead
valve train and sliding cam followers.
Stage 1 Stage 2
Duration, minutes 50 10
Speed, rpm. 800 1500
Torque, Nm. 25 25
Power, kW 2.1 3.9
Coolant Outlet Temperature, °C 50 55
Oil Temperature, °C 49 59
ASTM D6593
Equipment 1994 4.6 litre Ford V8 engine with 2 valves per cylinder.
Used:
Test A 216 hour cyclic test, with 54 cycles each lasting four hours and consisting
Conditions: of three stages.
Method Engine sludge and varnish, piston skirt varnish and oil screen clogging
of Rating:
ASTM D6837
Test A baseline, 5W-30 oil is run first, and the fuel consumption is measured at
Conditions: 5 distinct speed/load/temperature conditions.
The test oil is then introduced, and is aged for 16 hours at Aging Phase 1
conditions, and then the fuel consumption of the test oil is measured under the
same 5 speed/load/temperature conditions.
The test oil is then aged for a further 80 hours under Aging Phase 2 conditions,
and then the fuel consumption at the 5 distinct conditions is measured again.
The baseline oil is then reintroduced and the fuel consumption at 5 distinct
speed/load/temperature conditions is measured again.
Method FEI 1, relative fuel efficiency after 16 hours aging, and FEI 2 relative fuel
of Rating: efficiency after 96 hours aging, compared to the average fuel consumption
of the baseline candidate oil run immediately before and after the candidate
ASTM D6709
Purpose: Tests an oil's copper, tin, and lead bearing corrosion control capabilities and
evaluates shear stability under high temperature operating conditions.
Duration, hrs. 40
Speed, rpm. 3150
Oil Temperature, °C 143
Method Connecting rod bearing weight loss, used oil kinematic viscosity,
of Rating: 10 hour stripped viscosity for multigrade oils
ASTM D6750
Equipment Single cylinder supercharged diesel engine (1Y540) using one piece
Used: aluminium piston.
Purpose: Diesel detergency test for high speed, severe supercharged conditions.
Purpose: Evaluation of ring sticking, ring and cylinder wear and piston deposits.
Method Piston deposits rated to include top groove fill (TGF) %, top land heavy carbon
of Rating: (TLHC) % and weighted deposits (WDK)
Purpose: Evaluation of piston deposits and oil consumption when using two-piece
pistons with forged steel crown and aluminium skirt.
Method Total Weighted Piston Deposits (WDP), Top Groove and Top Land
of Rating: Carbon (TGC and TLC) and oil consumption rated
Method Top groove carbon, top land carbon, 2nd ring carbon deposits
of Rating: and oil consumption.
ASTM D6838
Equipment 1994 Cummins M-11 330E engine which is electronically controlled and has
Used: been modified to provide over-fueling and retarded injection.
Purpose: To evaluate soot abrasive wear of the valve train, oil filter plugging and sludge
formation on the rocker covers.
Test 200 hour long test consisting of 2 x 100 hour cycles alternating 50 hour
Conditions: segments with retarded and standard timing. The engine runs 15%
over-fuelled.
Stage 1 Stage 2
Duration, hrs. 50 50
Speed, rpm. 1800 1600
Coolant Outlet Temperature, °C 88
Oil Temperature, °C 115
Timing Retarded Standard
D6975-03
Equipment Cummins ISM 425 in-line six cylinder diesel engine which is turbocharged,
Used: aftercooled and has EGR.
Purpose: To evaluate the protection of an oil against soot related valve train wear, top
ring wear, engine sludge and filter plugging in an high soot, EGR environment.
Test 300 hour test length consisting of 3 x 100h hour 2 stage cycles, where
Conditions: stage 1 generates soot and stage 2 induces valve train wear.
Stage 1 Stage 2
Duration, hrs. 50 50
Speed, rpm. 1800 1600
Torque, Nm. 1300 1930
Inlet Manifold Temperature, °C 80 65.5
Coolant Outlet Temperature, °C 65.5
Oil Temperature, °C 115
Oil Charge, L 30
Purpose:
To evaluate an oils ability to inhibit soot-induced valve train wear
on a sliding tappet platform equipped with EGR.
Test
Conditions:
A 350 hour test consisting of 2 phases. Phase 1 is a 100hour long soot
generation phase, to reach 3.25% soot. Phase 2 is 250 hours of cyclical
operation to induce valve train wear.
Stage 1 Stage 2
Duration, hrs 100 250
Speed, rpm 1600 800 - 2600 variable
Injection timing, °BTDC 15 nominal variable
Inlet Manifold Temperature, °C 68 68
Coolant Outlet Temperature, °C 99
Oil Sump Temperature, °C 110
Oil Charge, kg 14.5
Fuel sulphur, ppm 10
Test A 200 hour test alternating between two 50 hour stages where stage
Conditions: 1 is a soot generation phase and stage 2 is run under heavy load conditions
Stage 1 Stage 2
Duration, hrs. 50 50
Speed, rpm 1800 1600
Injection timing Variable Fixed
Inlet Manifold Temperature, ºC 80 66.5
Coolant Outlet Temperature, ºC 65.5
Oil Gallery Temperature, ºC 115
Equipment Detroit Diesel 6V-92TA, six cylinder, two stroke turbocharged diesel engine.
Used:
Test Duration 100 hrs, consisting of six cycles. Half of running at full load,
Conditions: other half at full rated power.
Method Rings, liners, slipper bushings and piston skirts rated for distress
of Rating: which relates to overall engine life
ASTM D5967
ASTM D6987
Purpose: To evaluate an oil's performance with respect to piston, liner and bearing wear
in an EGR environment.
Test 300 hour two phase test where the first stage is a 75 hour soot generation
Conditions: phase, and the second phase is 225 hours at peak torque
Phase 1 Phase 2
Duration, hrs. 75 225
Speed, rpm. 1800 1200
Power, kW. ~257 ~324
Inlet Manifold Temperature, °C 70 66
Coolant Outlet Temperature, °C 66 85
Oil Temperature, °C 88 113
ASTM D7156
Equipment In-line, six cylinder Mack E-Tech V-Mac III diesel engine with EGR,
Used: turbocharging and intercooling.
Purpose: To evaluate the viscosity increase and soot loading performance of engine oils
in an EGR environment.
Test Single stage test lasting 252 hours, with variable timing to hit three different
Conditions: soot windows at 96h, 192h and 252h.
Equipment In-line 6 cylinder, 12L Mack E-TECH V-MAC III engine, turbocharged
Used: with heavy EGR .
Test Two stage test. First stage is 100 hrs, 35% EGR, rated speed conditions
Conditions: to generate ~ 4.3% soot, then second stage is 200 hrs, 15% EGR, peak
torque conditions to generate wear and corrosion.
Stage 1 Stage 2
Duration, hrs. 100 200
Speed, rpm 1800 1200
EGR, % 35 15
Inlet Manifold Temperature, ºC 80 80
Coolant Outlet Temperature, ºC 66 108
Oil Gallery Temperature, ºC 88 116
Fuel ULSD 7 -15 ppm sulphur
Method Increase in lead in oil, average liner wear, top ring weight loss.
of Rating:
Rig Tests
Contents Rig Tests
European Tests:
US Tests:
Scope: To evaluate the wear and filter blocking performance of hydraulic fluids in
controlled conditions with and without water contamination.
Equipment: Denison T6H20C Vane/Piston Pump Rig which circulates fluid while cycling
the pump output pressure and maintaining fluid flow.
Method: The same fluid is used for two 300-hr test phases, first with < 0.05% water
then with 1% water.
Scope: To assess sealing and wear capabilities of lubricants on oil seal materials.
Equipment: Test heads capable of applying different shaft speeds, temperatures and time
duration to a fixed position test oil seal.
Methods: Test oil seal samples are held in plates that are in turn fixed to an oil chamber.
A shaft then fits through the test seal and the chamber is half filled with
lubricant.
Ratings: Visual wear and leakage during test is monitored. Other parameters are also
rated including cracking, hardness and blistering.
Scope: The Rolling Bearing Lubricant Test Rig FE8 can be used to study the
tribological system “Rolling Bearing”
The test rig can be adapted to the most diverse operating and environmental
conditions. This makes it extremely versatile, allowing field applications as
well as lubricants, materials and roller bearings to be studied under their
specific operating conditions.
Equipment: FE8 test rig with adaptors to run oil or grease lubricants and roller or ball
bearings.
Method: A bearing is run to specific conditions for an allotted time either using a grease
or oil lubricant.
Rating: A visual check for pitting of the bearing surfaces and post test weight loss,
plus any increase in coefficient friction.
Method: The method consists of an enclosed gearbox with 1 litre of oil to be tested.
The gear pair are used to mix the oil with the air and effect foam formation
over a 5 minute period.
Rating: A visual rating on a numerical scale measuring the foam formation on top
of the test oil.
Significance: The addition of suitable additives to reduce the effects of foaming thus
reducing the possibilities of pitting and seizure.
Method: The four-ball EP tester is operated with one steel ball rotating against three
steel balls held stationary in the form of a cradle. The lubricant under test
covers the lower three balls. The speed of rotation is 1780 rpm. A series of
tests of 10 seconds duration are made at increasing load until welding occurs.
Load-Wear An index of the ability of the lubricant to prevent wear at applied loads. The
Index: equation for load-wear index reflects the ability of a lubricant to carry a high
load without welding and to allow only relatively small wear scars at loads
below the weld point.
Weld Point: The lowest load in kilograms at which the rotating ball welds to the three
stationary balls.
Specifications: The user should determine to his own satisfaction whether the results
correlate with field performance or other bench test machines.
ASTM D4172
Method: Three 12.7 mm diameter steel balls are clamped together and covered with
the lubricant under test. A fourth steel ball is pressed with a force of 147
or 392 N into the cavity formed by the three balls for the “three-point contact”.
The temperature of the test lubricant is regulated at 75°C and the top ball is
rotated at 1200 rpm for 60 minutes. Lubricants are compared by using the
average size of the scar diameters worn on the lower three clamped balls.
Specifications: The user of this method should determine to his own satisfaction whether
the results of this procedure correlate with field performance or other bench
test machines.
(Stage Test) The load on the tooth flanks is incresed in stages from Stage 1 to load
stage 10.
(Shock Test) The expected failure load is applied to an unused gear flank.
Ratings: The gears are inspected visually without removal at the end of each load
stage.
The failure load stage is reached when the sum of the damaged area’s width
exceeds 10mm.
Results:
Report the failure load stage as the result.
Scope: Assess the relative load-carrying capacities of oils when used to lubricate
steel/steel spur gears.
Equipment: The FZG spur gear test rig consists of a closed power circuit with drive and
test gears connected by two torsion shafts. One of the shafts has a positive
clutch for application of the load.
Method: Special gear wheels are run in the lubricant under test at a constant speed
for a fixed time. The initial oil temperature is controlled but allowed to rise
freely during each stage of the test. Loading is raised in stages. The test is
continued until the damage load stage is reached, but if no damage occurs
at load stage 12 the test is terminated.
Ratings: The gears are inspected visually, without removal, at the end of each load
stage.
Results:
The load stage in which failure occurs is reported together with the test
conditions; e.g. A/8.3/90, where A = gear type, 8.3 = pinion speed at pitch
circle in m/sec, and 90 = initial temperature in oil sump in °C. These are
the usual conditions, but they can be changed as required.
Specifications: Results are reported in terms of the highest pass stage for the CEC method
or the first fail load stage, for the DIN Method.
Scope: Based on a test originally developed by Chevron, this new procedure has been
adopted by ASTM D 4998-89 for the evaluation of final drive lubricants for use
in agriculture tractors and similar off-road applications.
Method: Using the same test equipment and gear wheels as for the FZG load-carrying
capacity test, this procedure requires a fixed load durability run to the
following conditions.
Results: The data is reported as total weight loss for both test gears, together with
the total number of teeth exhibiting wear. The precision of the method
has not been determined.
Note: CEC test method development working group has abandoned the method
until further research studies are completed. This is due to poor discrimination.
Method: The two part procedure comprises a load stage test followed by an endurance
test. During the load stage test, the ability of the gear lubricant tribological
systems to resist micropitting is determined. The endurance test provides
information on the progress of the damage after a higher number of
load cycles.
Results: The gears are examined for weight loss, area of micropitting involute
profile deviation.
Scope: To assess the relative EP/antiwear and anti-pitting properties of gear oils under
low speed - high torque non steady state conditions.
Equipment: The MB Planetary Gear rig is based upon a Mercedes-Benz screening rig
using vehicle hub reduction units.
Method: The test cycle below is repeated until a tooth breaks, excessive noise is heard,
or the iron content of the oil sample, taken every second cycle, shows a
significant increase.
Rating Method: The two sun gears and ten planetary gears are inspected for amount
of pitting and wear on the teeth.
Scope: The method evaluates oil in respect of static friction and stick slip behaviour
when used in machine slideway applications.
Method: A slideway supporting a sliding block is lubricated with the test oil. The
slideway is gradually inclined until the sliding block begins to move. The angle
at which the block moves 20 mm is used to calculate the ‘Schmidt Coefficient
of
Friction’ which uses a calculation developed by the Hans Schmidt Tribology
Laboratory for their original slideway test machine.
300 run-in cycles are carried out with the SKC 3 plastic test and 400 with the
Grey Cast Iron test. After completing the run-in, 10 test cycles are carried out
to determine the ‘Schmidt Coefficient of Friction’ of the oil.
Results:
Graphical plots of all the run-in and test cycles are presented along with the
calculated results of the 10 test cycles.
Scope: To correlate shear stability with the permanent viscosity drop expected
in field service.
Scope: To evaluate rust and corrosion properties of a lubricant with the presence
of water.
Method: Bearings run in an oil/water mixture for 8 hrs. The rig then stands idle for a
period of 16 hrs. This cycle is then repeated with a final running of 8 hrs
before standing idle for 108 hrs. The bearings are then rated.
Rating: Bearings are visually rated on a scale of 1-5 depending on the amount of
corrosion present.
Scope: The Brugger Test determines the load capacity of industrial, transmission and
hydraulic lubricants. The test provides a useful technique for evaluating the
wear protection of a lubricant under conditions of minimal lubrication.
Method: A 25 mm diameter steel friction roller is rotated at 940 rpm (1.2 m/sec) against
an 18 mm diameter fixed steel cylinder roller with a force of 400 N applied
by a lever mechanism for 30 seconds. The surfaces are lubricated with a 5 ml
sample poured over the assembly one minute before the start of the test.
Significance: The user should determine to his own satisfaction whether the
results correlate with field performance or other bench test machines.
Equipment: The test uses the Timken Wear and Lubricant Testing Machine, in which
a pivoted test block is applied to the periphery of a rotating cylinder (cup)
in such a way that the pressure of application can be controlled.
Method: The machine is operated with the steel cup rotating at 800 r/min. Two
determinations are made: the minimum load that will rupture the lubricant
film and cause scoring or seizure; and the maximum load (OK load) that
will not rupture the lubricant film.
Specifications: The method is widely used for specification purposes and is used to
differentiate between lubricants having low, medium or high extreme-pressure
characteristics. The results may not correlate with results from service.
Method: An adaptor, containing a standard single row taper roller bearing, is installed
in a Four-Ball test machine. 40ml of test oil is introduced into a cup
surrounding the bearing and the machine is run at 1500 r/min. with a 5 KN
bearing axial load, for test durations of 4, 8 and 20 hours. The oil
temperature is held at 60°C.
The percentage loss in kinematic viscosity of the oil after each test run
is plotted against time.
Significance: The method is being standardised for specification purposes and is a rapid
means of assessing the shear stability of a wide range of lubricants.
Note: Limited service correlation of data from this test method is available.
Scope: Evaluates the rust and corrosion inhibiting properties of a gear lubricant
when subjected to water contamination and elevated temperature.
Equipment: The test utilises an unloaded Dana Model 30 hypoid differential unit mounted
on a test stand which enables the unit to be motored over with heat lamps
playing on the outer surface.
Rating: At the end of storage, the unit is disassembled and rated for corrosion,
sludge and other deposits.
Equipment: The axle is driven by a 5.7 litre V8 gasoline engine which drives the test axle,
a 4 speed truck transmission and two high inertia dynamometers at a rate to
simulate hard acceleration to ca. 100 mph. The axle during testing is
periodically shock loaded through a dynamometer.
Method: After break-in, the axle is accelerated through the gears to a speed of
1050 r/min; then decelerated to 530 r/min. The cycle is repeated 5 times.
This high speed sequence is followed by 10 shock loadings - the shock
sequence.
Results: Each new batch of gears is referenced against two industry standardised
oils; RGO-110 (low-scoring) and RGO-108 (scoring). At least a 15%
difference in the metal score characteristics is required.
The drive gear and pinion are rated for coast side scoring.
The drive side score is only considered if scoring is significant.
CS3000B ANNEX D
Scope: Assess the ability of the oil to lubricate a hypoid automotive axle at high
sliding speed, and with high impact loading, without surface distress to the
gears.
Method: An automotive hypoid rear axle is fitted into the test vehicle (Avenger) which
is operated on a laboratory inertia roller rig. The severity level of the rig
is adjusted so that the requirements of the axle are such that, using the
CRC reference oil 10/90, the area of scuffing on the coast side of the
pinion teeth is not less than 25%.
The performance of the oil under test is evaluated by examination of the axle
components for tooth distress, corrosion and deposits.
Specifications: CS3000B requires the oil to have performance equal to or better than
that of the reference oil.
Scope: Evaluates the load carrying, wear and extreme pressure characteristics of gear
lubricants in a hypoid axle under high speed - low torque and low speed - high
torque operations.
Equipment: A Dana Model 60 hypoid axle (5.86 ratio) fitted with uncoated drive gear
and pinion is set up to drive 2 dynamometers from an 8 cyclinder, 5.7 litre
gasoline truck engine.
Method: The axle is fitted with the test oil and driven under varying conditions.
A high speed - low torque is first run for 100 minutes and the gears
visually assessed via an inspection plug. A low speed - high torque
sequence is then run for a further 24 hours.
Method: A measured sample of test oil is placed in a special gear case with two
spur gears and a copper catalyst strip. The test is run for 50 hours, at 163ºC,
whilst the gears are being driven at 1725 rpm and air is being bubbled
through the sample.
Results: Viscosity increase and pentane and toluene insolubles are determined.
Specifications: The gears are rated for carbon, varnish and sludge deposits.