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Chemistry For Engineers - Lab GEN 0103L: 2 Semester AY 2020 - 2021

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Chemistry for Engineers – Lab

GEN 0103L
2nd Semester AY 2020 - 2021

Engr. Veronica F. Acosta


EXPERIMENT NO. 1

BASIC LABORATORY TECHNIQUES


Objectives:

1. To learn the use of common, simple laboratory equipments.


2. To become familiar with the metric system of measurement.
3. To be able to convert units from Metric to English system and vice versa
Discussion
Chemistry is an experimental science, It depends upon careful observation and the use of good
laboratory techniques. In this experiment, you will become familiar with some basic operations that will help
you throughout this course. Your success as well as your safety in future experiments will depend upon your
mastering these fundamental operations.

Because every measurement made in the laboratory is really an approximation, it is important that
the numbers you record reflect the accuracy and precision of the device you use to make the measurement.

In 1960, an international agreement was reached specifying the particular choice of the Metric
System of units. In this system the basic units for length, mass and time are the meter, kilogram and second.
This system of units is also known as the International System of units, or commonly referred to as the SI
system and is preferred in scientific work.
Materials and Apparatus
Distilled water Bunsen burner

Triple beam balance/electronic balance ruler/meter stick

250mL beaker pipette

50 or 100mL graduated cylinder aspirator

Large test tube ring stand/iron stand

thermometer iron ring

wire gauze
Procedure
A. The Meter Stick / Ruler

1. Examine the meter stick/ruler and observe that one side is ruled in inches,
whereas the other is ruled in centimeters.
2. Measure and record the length and the width of your laboratory manual
in both units.
3. Mathematically convert the two measurements to show that they are
equivalent.
A. The Meter Stick/Ruler
Result:
A. The Meter Stick/Ruler
Result:
A. The Meter Stick/Ruler
Result:
A. The Meter Stick/Ruler
Result:
A. The Meter Stick/Ruler
Procedure
B. Graduated Cylinder
1. Examine the 100mL graduated cylinder that is calibrated in milliliters.
2. Fill the cylinder approximately half full with water. Notice that the meniscus
(curve surface of the water) is concave. The lowest point on the curve is always
read to record the volume, never the upper level. Avoid errors due to parallax
effects; different and erroneous readings are obtained if the eye is not on level
with the scale. Read the volume of the water to the nearest 1 mL.
3. Measure the maximum amount of water that your largest test tube will hold.
Record this volume. Make at least three trials.
Graduated Cylinder
100 mL
50 mL
Result: Volume of a half-filled
graduated cylinder
Empty Largest Test tube

Largest Test Tube filled


with water
Results: Volume of Largest Test Tube
Trial 1 Trial 2 Trial 3
Procedure
C. The thermometer and its calibration
This part of the experiment is performed to check the accuracy of your thermometer. The exercise will show how measured
temperatures (read from thermometer) compare with the true temperature (the boiling and freezing point of water). The freezing
point of water is 0 C; the boiling point depends upon atmosphere pressure and is calculated as shown below.

1. Fill a beaker about half full of distilled water.


2. Place the beaker on a wire gauze and iron ring and begin heating the water. Periodically determine the temperature of the water
with thermometer, but be careful not to touch the walls of the beaker with thermometer bulb.
3. Record the boiling point of water. Using the formula below, determine the true boiling point at the observed atmospheric
pressure. Obtain the atmospheric pressure from your laboratory instructor.
Formula:
Boiling point correction = (760mmHg – atmospheric pressure) x (0.037 C/mm)
True boiling point = boiling point of water – boiling point correction
Set – up Iron stand
How to Use Bunsen Burner
The thermometer
and its calibration
The Thermometer and its
Calibration
Result: The thermometer
Result: Boiling Point
of water
Procedure
D. Laboratory Balance
Weighing an object on a single-pan balance is a simple matter. Considering the
inherent sensitivity and the cost of the balance you must be careful in its use.
Directions for operation of a single pan balance vary with maker and model. Your
laboratory instructor will explain how to use the balance.

1. Weigh the water whose volume you measured in part B. First pour the water into a previously
weighed beaker and record the weight of the water and beaker. Then subtract the weight of the
beaker to obtain the weight of the water alone.

2. Place a five peso coin and record its weight.


The Laboratory Balance
Beaker
Result: Mass of beaker
Beaker and water
Result: Mass of beaker and water
Mass of a five peso coin
Result: Mass of a five peso coin
REFERENCES
Elizares, L.M. & Acosta, V. F. (2018) Chemistry for Engineers Laboratory Manual.

Stoker, H. Stephen (2016). General Chemistry. Andover: Cengage

Zumdahl, Steven S. (2015). Introductory Chemistry: A Foundation. USA: Cengage Learning Asia Ptd
Ltd., USA

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