Concrete Technology (Lab Manual)
Concrete Technology (Lab Manual)
Concrete Technology (Lab Manual)
CONCRETE
TECHNOLOGY LAB
COURSE CODE: CEE303
CREDIT UNITS:03
List of Experiments
1. FINENESS OF CEMENT
2. NORMAL CONSISTENCY OF CEMENT
3. INITIAL AND FINAL SETTING TIMES OF CEMENT
4. SPECIFIC GRAVITY OF CEMENT
5. SOUNDNESS OF CEMENT
6. FINENESS MODULUS OF FINE AND COARSE AGGREGATE
7. SPECIFIC GRAVITY, VOID RATIO, POROSITY AND BULK DENSITY
OF COARSE AND FINE AGGREGATES
8. BULKING OF SAND
9. WORKABILITY TESTS ON FRESH CONCRETE
10. COMPACTION FACTOR TEST
11. TEST FOR COMPRESSIVE STRENGTH OF CEMENT CONCRETE
FINENESS OF CEMENT
(IS: 269-1989 and IS: 4031-1988)
AIM: To determine the fineness of the given sample of cement by sieving.
APPARATUS: IS-90 micron sieve conforming to IS:460-1965, standard balance,
weights, brush.
INTRODUCTION: The fineness of cement has an important bearing on the rate of
hydration and hence on the rate of gain of strength and also on the rate of evolution of
heat. Finer cement offers a greater surface area for hydration and hence the faster and
greater the development of strength. Increase in fineness of cement is also found to
increase the drying shrinkage of concrete. Fineness of cement is tested either by
sieving or by determination of specific surface by air-permeability apparatus. Specific
surface is the total surface area of all the particles in one gram of cement.
1.
2.
3.
4.
FINENESS BY SIEVING:
PROCEDURE:
Weigh accurately 100 g of cement and place it on a standard 90 micron IS sieve.
Break down any air-set lumps in the cement sample with fingers.
Continuously sieve the sample giving circular and vertical motion for a period of
15 minutes.
Weigh the residue left on the sieve. As per IS code the percentage residue
should not exceed 10%.
PRECAUTIONS: Air set lumps in the cement sample are to be crushed using fingers
and not to be pressed with the sieve. Sieving shall be done holding the sieve in both
hands and with gentle wrist motion. More or less continuous rotation of the sieve shall
be carried out throughout sieving.
OBSERVATIONS:
S.No
weight of
taken(g)
Fineness (%)
3.
4.
5.
6.
7.
8.
9.
PROCEDURE:
Prepare a paste of weighed quantity of cement (300 grams) with a weighed
quantity of potable or distilled water, starting with 26% water of 300g of cement.
Take care that the time of gauging is not less than 3 minutes, not more than 5
minutes and the gauging shall be completed before setting occurs.
The gauging time shall be counted from the time of adding the water to the dry
cement until commencing to fill the mould.
Fill the vicat mould with this paste, the mould resting upon a non porous plate.
After completely filling the mould, trim off the surface of the paste, making it in level
with the top of the mould. The mould may slightly be shaken to expel the air.
Place the test block with the mould, together with the non-porous resting plate, under
the rod bearing the plunger (10mm diameter), lower the plunger gently to touch the surface
of the test block and quickly release, allowing it to penetrate into the paste.
This operation shall be carried out immediately after filling the mould.
Prepare trial pastes with varying percentages of water and test as described
above until the amount of water necessary for making the standard consistency as
defined above is obtained.
Express the amount of water as a percentage by weight of the dry cement.
PRECAUTIONS: Clean appliances shall be used for gauging. In filling the mould the operator
hands and the blade of the gauging trowel shall alone be used. The temperature of cement,
water and that of test room, at the time when the above operations are being performed, shall
be 27 + 2 C. For each repetition of the experiment fresh cement is to be taken.
OBSERVATIONS:
Weight of cement Weight of water Plunger
S. No taken in gms
taken in gms
penetration
(a)
(b)
(mm)
Time
Taken
Consistency of
cement in % by
weight b/a * 100
1.
2.
3.
4.
5.
PROCEDURE:
Preparation of Test Block:
Prepare a neat cement paste by gauging 300 grams of cement with 0.85 times
the water required to give a paste of standard consistency.
Potable or distilled water shall be used in preparing the paste.
The paste shall be gauged in the manner and under the conditions prescribed in
determination of consistency of standard cement paste.
Start a stop-watch at the instant when water is added to the cement.
Fill the mould with the cement paste gauged as above the mould resting on a
nonporous plate.
6. Fill the mould completely and smooth off the surface of the paste making it level with
the top of the mould. The cement block thus prepared in the mould is the test block.
DETERMINATION OF INITIAL SETTING TIME:
1.
Place the test blocks confined in the mould and rest it on the non-porous plate, under the
rod bearing initial setting needle, lower the needle gently in contact with the surface of the test
block and quickly release, allowing it to penetrate into the test block.
2.
3.
In the beginning, the needle will completely pierce the test block.
Repeat this procedure until the needle, when brought in contact with the test
block and released as described above, fails to pierce the block to a point 5 to 7 mm
measured from the bottom of the mould shall be the initial setting time.
PRECAUTIONS: Clean appliances shall be used for gauging. All the apparatus shall be
free from vibration during the test. The temperature of water and that of the test room, at the
time of gauging shall be 27 0C + 20 C. Care shall be taken to keep the needle straight.
OBSERVATIONS:
Time in minutes :
Height in mm fails to penetrate
RESULT: Initial setting time for the given sample of cement =
Final setting time for the given sample of cement =
COMMENTS:
NOTE
(I) Duplicate determination of specific gravity should agree within 0.01.
(II) To get more accurate result, the flask should be held in a constant temperature
before each reading is taken.
RESULT
Specific gravity of a sample of cement =
SOUNDNESS OF CEMENT
(IS 269-1989 AND IS 4031-1988 PART 3)
AIM: To determine the soundness of the given sample of cement by "Le Chatelier" Method.
3.
While this operation is being performed cover the mould with another piece of glass
sheet, place a small weight on this covering glass sheet and immediately submerge the whole
assembly in water at a temperature of 27 0 - 20 C and keep there for 24 hours.
4.
9.
The difference between these two measurements represents the expansion of the cement.
For good quality cement this expansion should not be more than 10mm.
OBSERVATIONS:
Initial distance between the indicator points in
mm = Final distance between the indicator
points in mm = Expansion in mm = final length initial length = RESULT: Expansion in mm
PROCEDURE:
Coarse aggregate:
1. Take 5Kgs of coarse aggregate (nominal size 20mm) from the sample by quartering.
2. Carry out sieving by hand, shake each sieve in order 75mm ,40mm, 20mm,
10mm, and No's 480, 240, 120, 60, 30, & 15 over a clean dry tray for a period of
not less than 2 minutes.
3. The shaking is done with a varied motion backward and forward, left to right,
circular, clockwise and anticlockwise and with frequent jarring.
4. So
that material is kept moving over the sieve surface in frequently changing directions.
the sieves in order of No. 480, 240, 120, 60, 30 and 15 keeping sieve 480 at top
and 15 at bottom.
3. Fix them in the sieve shaking machine with the pan at the bottom and cover at the top.
4. Keep the sand in the top sieve no 480, carry out the sieving in the set of sieves
and arranged before for not less than 10 minutes.
5. Find the weight retained in each sieve.
OBSERVATIONS:
Coarse aggregate: Wt. of coarse aggregate taken: Kgs.
S.No
1.
2.
3.
Sieve size
75 mm
40 mm
20 mm
Weight
retained
% Weight
retained
% weight
passing
Cumulative
% Weights
retained
4.
10 mm
5. 4800 microns
6. 2400 microns
7. 1200 microns
8. 600 microns
9. 300 microns
10. 150 microns
Sieve size
1
2
3
4
5
6
4800 microns
2400 microns
1200 microns
600 microns
300 microns
150 microns
Weight
retained
% Weight
retained
% weight
passing
6.9
7.5
8.0
8.5
Cumulative
% Weights
retained
3. Percentage of voids or porosity is the ratio of volume of voids to the total volume of a
sample of an aggregate.
4. Bulk density or unit weight is the weight of material per unit volume.
PROCEDURE: Coarse aggregate
1. Find the weight of the empty container W1.
2. Take coarse aggregate in the container up to approximately half of the container and
find out the weight W2.
3. Fill the container with water upto the level of the coarse aggregates so that all void
space inside the aggregate is filled with water. Find its weight W3.
4. Fill the container with water after emptying it from mix of coarse aggregate and water.
5. Water should be upto the mark, upto which coarse aggregate is filled. Find its weight W4
6. Repeat the same process for another trail by taking the aggregate upto the full of the
container and by filling the water up to same point.
OBSERVATIONS:
S.No
1)
2)
3)
4)
Trail 1
Weight of empty container
Weight of container with material
Weight of container + material + water
Weight of container + water
W1
W2
W3
W4
Trail 2
W3 - W1 / ((W4 - W1)-(W3-W2))
ii) Porosity = Vol. of Voids / Total Vol. of aggregate
*100 W3 - W2 / (W4 - W1) * 100
iii) Specific gravity = W2 - W1 / ((W4 - W1) - (W3 - W2))
iv) Bulk density = W2 - W1 / (W4 - W1)
Fine aggregate: Void Ratio and porosity
1. Take 150 ml of dry sand (v1 ml) in clean measuring jar of 1000 ml capacity.
2. Add a measured quantity of 100 ml clean water to the above sample (v2 ml) i.e. v2=100 ml
3. Shake the jar thoroughly till all air bubbles are expelled.
4. Now note the readings against the top surface of water in the jar (V3 ml)
Void ratio = v1 + v2 - v3 / v3 - v2
Porosity = v1 + v2 - v3 / v1
Specific gravity of fine aggregates:
1. Weigh the empty measuring jar of 1000 ml capacity = W1
2. Take the weight of empty measuring jar with 150 ml of sand
Empty jar + sand
=W2
3. Take the weight of empty measuring jar with 150 ml of sand and 100 ml of water
Empty jar + sand + water
= W3
4. Remove the mix of sand and water from bottle and fill it with water up to volume V3 then
weigh it.
Empty jar + water
= W4
Specific gravity = Weight of solids / Volume of Solids
W2 - W1 / ((W4 - W1) - (W3 - W2))
PRECAUTIONS: While filling the container with water in determining void ratio and
porosity of coarse aggregate care should be taken that water should not be in excess of
the level of course aggregate.
RESULT:
1) Specific gravity of course aggregate.
2) Void ratio of course aggregate.
3) Porosity of coarse aggregate.
4) Bulk density of course aggregate.
5) Specific gravity of fine aggregate.
6) Void ratio of the given fine aggregate.
7) Porosity of the given time aggregate.
COMMENTS:
.
BULKING OF SAND
AIM: To ascertain the bulking phenomena of given sample of sand.
APPARATUS: 1000ml measuring jar, brush.
INTRODUCTION: Increase in volume of sand due to presence of moisture is known as bulking
of sand. Bulking is due to the formation of thin film of water around the sand grains and the
interlocking of air in between the sand grains and the film of water. When more water is added
sand particles get submerged and volume again becomes equal to dry volume of sand. To
compensate the bulking effect extra sand is added in the concrete so that the ratio of coarse to
fine aggregate will not change from the specified value. Maximum increase in volume may be
20 % to 40 % when moisture content is 5 % to 10 % by weight. Fine sands show greater
percentage of bulking than coarse sands with equal percentage of moisture.
PROCEDURE:
1) Take 1000ml measuring jar.
2) Fill it with loose dry sand upto 500ml without tamping at any stage of filling.
3) Then pour that sand on a pan and mix it thoroughly with water whose volume is equal to
2% of that of dry loose sand.
4) Fill the wet loose sand in the container and find the volume of the sand which is in
excess of the dry volume of the sand.
5) Repeat the procedure for moisture content of 4%, 6%, 8%, etc. and note down the readings.
6) Continue the procedure till the sand gets completely saturated i.e till it reaches the
original volume of 500ml.
OBSERVATIONS:
S.No
Volume of dry
loose sand V1
1.
500 ml
2.
3.
4.
5.
6.
% moisture
content added
2%
4%
6%
8%
Volume of wet
loose sand V2
% Bulking V2
V1 / V1
GRAPH: Draw a graph between percentage moisture content on X-axis and percentage bulking
on Y-axis. The points on the graph should be added as a smooth curve. Then from the graph,
determine maximum percentage of bulking and the corresponding moisture content.
PRECAUTIONS:
1) While mixing water with sand grains, mixing should be thorough and uniform.
2) The sample should not be compressed while being filled in jar.
3) The sample must be slowly and gradually poured into measuring jar from its top.
4) Increase in volume of sand due to bulking should be measured accurately.
RESULT: The maximum bulking of the given sand is -----------at -----------% of moisture
content.
COMMENTS:
Place the mixed concrete in the cleaned slump cone in 4 layers each approximately
1/4 in height of the mould. Tamp each layer 25 times with tamping rod.
4) Remove the cone immediately, rising it slowly and carefully in the vertical direction.
5) As soon as the concrete settlement comes to a stop, measure the subsistence of the
concrete in cms, which gives the slump.
Note: Slump test is adopted in the Laboratory or during the progress of the work in the field
for determining consistency of concrete where nominal max., size of aggregates does not
exceed 40 mm. Any slump specimen which collapses or shears off laterally gives incorrect
results and at this juncture the test is repeated only true slump should be measured.
OBSERVATIONS:
S.No
1
2
3
4
W/c Ratio
0.5
0.6
0.7
|0.8
Slump in mm
PRECAUTIONS:
1) The strokes are to be uniformly applied through the entire area of the concrete section.
2) The cone should be removed very slowly by lifting it upwards without disturbing the
concrete.
3) During filling the mould must be firmly pressed against the base.
4)
Vibrations from nearly machinery might also increase subsidence; hence test
should be made beyond the range of ground vibrations.
COMMENTS: This test is not a true guide to workability. For example, a harsh coarse
mix cannot be said to have same workability as one with a large portion of sand even
though they have the same slump.
Recommended slumps of concrete mix of various works
S.No
1
2
3
4
Description of work
Road work
Ordinary beams to slabs|
Columns thin vertical section & retaining Walls etc
Mass concrete(Runway, |Pavements)
THEORY: This test is adopted to determine workability of concrete where nominal size
of aggregate does not exceed 40 mm. It is based on the definition, that workability is that
property of concrete, which determines the amount of work required to produce full
compaction. The test consists essentially of applying a standard amount of work to
standard quantity of concrete and measuring the resulting compaction.
The compaction factor is defined as the ratio of the weight of partially compacted concrete to the
weight of fully compacted concrete. It shall be stated to the nearest second decimal place.
PROCEDURE: Conduct test for W/c ratio 0.5, 0.6, 0.7, and 0.8, for each mix take 10 kg
of coarse aggregate 5kg of fine aggregate and 2.5 Kg of cement.
1. Grease the inner surface of the hoppers and the cylinder.
2. Fasten the hopper doors.
3. Weigh the empty cylinder accurately (Wt. Kgs).
4. Fix the cylinder on the base with fly nuts and bolts
5. Mix coarse and fine aggregates and cement dry until the mixture is uniform in colour
and then with water until concrete appears to be homogeneous.
6. Fill the freshly mixed concrete in upper hopper gently with trowel without compacting.
7. Release the trap door of the upper hopper and allow the concrete of fall into the lower
hopper bringing the concrete into standard compaction.
8. Immediately after the concrete comes to rest, open the trap door of the lower hopper and allow
the concrete to fall into the cylinder, bringing the concrete into standard compaction.
9. Remove the excess concrete above the top of the cylinder by a trowel.
10. Find the weight of cylinder i.e cylinder filled with partially compacted concrete (W2 kgs)
11.
Refill the cylinder with same sample of concrete in approx. 4 layers, tamping each
layer with tamping for 25 times in order to obtain full compaction of concrete.
12. Level the mix and weigh the cylinder filled with fully compacted concrete (W3 Kg)
13. Repeat the procedure for different for different a trowel.
OBSERVATIONS AND CALCULATIONS:
Weight of cylinder = W1 Kgs.
S.No
W/c ration
1
2
3
4
0.5
0.6
0.7
0.8
Wt.
With
partially
compaction
W2
(Kgs)
Compaction
factor
(W1- W2)/
(W3- W1)
PRECAUTIONS:
1. The top hopper must be filled gently.
2. The mix should not be pressed or compacted in the hopper.
3.
If the concrete in the hopper does not fall through when the trap door is released, it should
be freed by passing a metal rod. A single steady penetration will usually affect release.
COMMENTS: It is more sensitive, precise than slump test and is particularly useful to
concrete mixes of low workability.
Placing condition
Degree of
Values of
workability
workability
0.75 to 0.80
vibration
2
Low
0.8 to 0.85
Medium
0.85 to 0.92
reinforce
d
High
0.92 to above