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Keywords = multi-wavelength fiber laser

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18 pages, 1807 KiB  
Article
3DVT: Hyperspectral Image Classification Using 3D Dilated Convolution and Mean Transformer
by Xinling Su and Jingbo Shao
Photonics 2025, 12(2), 146; https://doi.org/10.3390/photonics12020146 - 11 Feb 2025
Viewed by 410
Abstract
Hyperspectral imaging and laser technology both rely on different wavelengths of light to analyze the characteristics of materials, revealing their composition, state, or structure through precise spectral data. In hyperspectral image (HSI) classification tasks, the limited number of labeled samples and the lack [...] Read more.
Hyperspectral imaging and laser technology both rely on different wavelengths of light to analyze the characteristics of materials, revealing their composition, state, or structure through precise spectral data. In hyperspectral image (HSI) classification tasks, the limited number of labeled samples and the lack of feature extraction diversity often lead to suboptimal classification performance. Furthermore, traditional convolutional neural networks (CNNs) primarily focus on local features in hyperspectral data, neglecting long-range dependencies and global context. To address these challenges, this paper proposes a novel model that combines CNNs with an average pooling Vision Transformer (ViT) for hyperspectral image classification. The model utilizes three-dimensional dilated convolution and two-dimensional convolution to extract multi-scale spatial–spectral features, while ViT was employed to capture global features and long-range dependencies in the hyperspectral data. Unlike the traditional ViT encoder, which uses linear projection, our model replaces it with average pooling projection. This change enhances the extraction of local features and compensates for the ViT encoder’s limitations in local feature extraction. This hybrid approach effectively combines the local feature extraction strengths of CNNs with the long-range dependency handling capabilities of Transformers, significantly improving overall performance in hyperspectral image classification tasks. Additionally, the proposed method holds promise for the classification of fiber laser spectra, where high precision and spectral analysis are crucial for distinguishing between different fiber laser characteristics. Experimental results demonstrate that the CNN-Transformer model substantially improves classification accuracy on three benchmark hyperspectral datasets. The overall accuracies achieved on the three public datasets—IP, PU, and SV—were 99.35%, 99.31%, and 99.66%, respectively. These advancements offer potential benefits for a wide range of applications, including high-performance optical fiber sensing, laser medicine, and environmental monitoring, where accurate spectral classification is essential for the development of advanced systems in fields such as laser medicine and optical fiber technology. Full article
(This article belongs to the Special Issue Advanced Fiber Laser Technology and Its Application)
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<p>Overall framework of the 3DVT network model.</p>
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<p>ViT encoder with average pooling projection.</p>
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16 pages, 10770 KiB  
Article
A Tunable and Switchable Multi-Wavelength Erbium-Doped Fiber Laser Based on a Curvature Mach–Zehnder Interferometer Filter Using Thin-Core Fiber
by Christian Perezcampos-Mayoral, Jaime Gutiérrez-Gutiérrez, José Luis Cano-Pérez, Marciano Vargas-Treviño, Lorenzo Tepech-Carrillo, Erick Israel Guerra-Hernández, Itandehui Belem Gallegos-Velasco, Pedro Antonio Hernández-Cruz, Eeduardo Pérez-Campos-Mayoral, Victor Hugo Ojeda-Meixueiro, Julián Moisés Estudillo-Ayala, Juan Manuel Sierra-Hernandez and Roberto Rojas-Laguna
Appl. Sci. 2024, 14(24), 11578; https://doi.org/10.3390/app142411578 - 11 Dec 2024
Viewed by 771
Abstract
We propose and demonstrate a tunable and switchable multi-wavelength fiber ring laser configuration based on a Mach–Zehnder interferometer (MZI) filter. The MZI was fabricated using a core-offset splicing technique, with a 2 cm piece of thin-core erbium-doped fiber (TCEDF), with a core diameter [...] Read more.
We propose and demonstrate a tunable and switchable multi-wavelength fiber ring laser configuration based on a Mach–Zehnder interferometer (MZI) filter. The MZI was fabricated using a core-offset splicing technique, with a 2 cm piece of thin-core erbium-doped fiber (TCEDF), with a core diameter of 2.90 µm, coupled in the central region of the MZI between two segments of single-mode fiber (SMF). By applying curvature to the MZI filter, we generated lasing single-, double-, triple-, and quadruple-emission lines with a curvature range from 2.3452 m−1 to 6.0495 m−1. A single-emission lasing line can be tuned from 1556.63 nm to 1564.25 nm with a tuning span of 7.62 nm and an SMSR of 49.80 dB. The laser emission can be switched to quadruple- and triple-emission lasing signals, with SMSR values of 39.96 dB and 36.83 dB, respectively. The dual-narrow emission lasing signal can be tuned from 1564.56 nm to 1561.34 nm, with an SMSR of 40.46 dB. Another lasing dual-emission signal can be tuned from 1585.69 nm to 1576.89 nm, producing an 8.8 nm tuning range, and from 1572.53 nm to 1563.66 nm, producing an 8.87 nm range, with the best SMSR of 42.35 dB. Full article
(This article belongs to the Special Issue Recent Trends in Fiber Optic Sensor: Technology and Applications)
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Figure 1
<p>Fiber clamping for SMF/TCEDF/SMF splices. (<b>a</b>) This demonstrates how to adhere the fiber to the metric rod with the masking tape and (<b>b</b>) illustrates how splicing is accomplished with the fusion splicer.</p>
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<p>Core-offset splice SMF/TCEDF/SMF design. (<b>a</b>) Illustrates the splicing between fibers, (<b>b</b>) shows the TCEDF cut, (<b>c</b>) U-shape of the MZI filter, (<b>d</b>) exhibits the z-side view of the MZI.</p>
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<p>(<b>a</b>) Interference spectra generated in the optical cavity of each MZI filter, (<b>b</b>) spatial frequency of the transmission spectrum generated by every filter.</p>
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<p>Diagram of the MTEFL ring array: (<b>a</b>) illustrates the configuration scheme, and (<b>b</b>) depicts the process for inducing curvature in the MZI filter to generate wavelength-switchable tunable emission lines.</p>
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<p>MTEFL emission tuning and switching cases generated for single (state-a), quadruple (state-b), triple (state-c), narrow-double (state-d), and double (state-e) lasing signals.</p>
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<p>(State-a) single-emission signal. (<b>a</b>) Tuning lines, (<b>b</b>) emission samples of curvature and SNR, (<b>c</b>) SMSR and SNR of the most significant peaks and their comparison, (<b>d</b>) the polynomial fit between the curvature data and its wavelength shift.</p>
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<p>Switch with quad-emission line. (<b>a</b>) SMSR on each peak, (<b>b</b>) power difference between the peaks and their separation.</p>
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<p>(State-c) double switch of triple-emission signals: (<b>a</b>) SMSR on the first switch, (<b>b</b>) separation and power of peaks, (<b>c</b>) SMSR of the second switch, (<b>d</b>) separation and the power of peaks.</p>
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<p>(State-c) double switch of triple-emission signals: (<b>a</b>) SMSR on the first switch, (<b>b</b>) separation and power of peaks, (<b>c</b>) SMSR of the second switch, (<b>d</b>) separation and the power of peaks.</p>
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<p>Narrow-dual-emission signals (state-d). (<b>a</b>) Tuning and the potential difference between peaks and their wavelength comparisons, (<b>b</b>) most significative peaks and power comparison, (<b>c</b>) sensitivity compared to the dispersion of curvature samples.</p>
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<p>Double-emission signal (state-e). (<b>a</b>) Tuning and most significant power peaks, (<b>b</b>) separation comparison, (<b>c</b>) peaks power comparison, (<b>d</b>) sensitivity generated with the curvature/wavelength samples.</p>
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<p>Double-emission signal (state-e). (<b>a</b>) Tuning and most significant power peaks, (<b>b</b>) separation comparison, (<b>c</b>) peaks power comparison, (<b>d</b>) sensitivity generated with the curvature/wavelength samples.</p>
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<p>(<b>a</b>) Stability test of the single initial and final emission, (<b>b</b>) power variation, (<b>c</b>) wavelength variation.</p>
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<p>First and last emissions signals of the dual-narrow lasing lines. (<b>a</b>) Stability test, (<b>b</b>) power fluctuation, (<b>c</b>) wavelength stability.</p>
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<p>Stability tests of the dual lasing lines. (<b>a</b>) Stability test on the first emission, (<b>b</b>) power fluctuation, (<b>c</b>) wavelength stability, (<b>a’</b>) stability test on the last emission, (<b>b’</b>) power fluctuation, (<b>c’</b>) wavelength stability.</p>
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<p>(<b>a</b>) Stability tests of the quad-emission line, (<b>b</b>) power variation, (<b>c</b>) wavelength variation.</p>
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<p>Stability tests of the triple emissions. (<b>a</b>) On the first switch, (<b>b</b>) power variation, (<b>c</b>) wavelength variation, (<b>a’</b>) test on the second switch, (<b>b’</b>) power variation, (<b>c’</b>) wavelength variation.</p>
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16 pages, 16410 KiB  
Article
A Tunable and Switchable Multi-Wavelength Erbium-Doped Fiber Ring Laser Enabled by Adjusting the Spectral Fringe Visibility of a Mach-Zehnder Fiber Interferometer
by Romeo Emmanuel Nuñez Gomez, Gilberto Anzueto Sánchez, Alejando Martínez Ríos, Ariel Fong González, Alfredo Olarte Paredes, Areli Marlen Salgado Delgado, Jesús Castrellón Uribe and René Salgado Delgado
Appl. Sci. 2024, 14(21), 9846; https://doi.org/10.3390/app14219846 - 28 Oct 2024
Viewed by 1413
Abstract
This paper presents a tunable, switchable multi-wavelength emission from an erbium-doped fiber ring laser, enabled by adjusting the spectral fringe visibility of a fiber interferometer filter. The filter is formed with specially designed concatenated tapered fibers to configure a Mach-Zehnder fiber interferometer (MZFI). [...] Read more.
This paper presents a tunable, switchable multi-wavelength emission from an erbium-doped fiber ring laser, enabled by adjusting the spectral fringe visibility of a fiber interferometer filter. The filter is formed with specially designed concatenated tapered fibers to configure a Mach-Zehnder fiber interferometer (MZFI). The laser emission is highly flexible and reconfigurable, allowing for tuning between single- and dual-wavelength operation. The laser can switch sequentially from one up to six wavelengths by fixing the curvature and adjusting the polarization state. The lasing emission is generated over a stable wavelength range between 1559.59 nm and 1563.54 nm, exhibiting an optical signal-to-noise ratio (OSNR) exceeding ~35 dB. The performance of amplitude and wavelength fluctuations were evaluated, indicating an appropriate stability of ~3 dB and a shift less than 0.1 nm within a 45 min period at room temperature. A detailed comparison with the literature is given. Full article
(This article belongs to the Special Issue Recent Trends in Fiber Optic Sensor: Technology and Applications)
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Figure 1
<p>Experimental erbium-doped fiber ring laser cavity setup for tunable and multi-wavelength emission.</p>
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<p>(<b>a</b>) MZFI structure formed with a pair of tapered sections fabricated on SMF-28, (<b>b</b>) displacement mechanism to used induce curvature in the MZFI.</p>
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<p>ASE spectrum as the light source from the EDF (black line) and the modified spectrum after passing through the MZFI (red line). The laser oscillation at 1563.07 nm is shown by the blue line.</p>
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<p>(<b>a</b>) The progressive modification of ASE spectrum with increasing curvature applied to the MZFI, (<b>b</b>) an inset in the range of 1541 to 1560 nm demonstrates an FSR of 5 nm.</p>
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<p>The wavelength shifts as a function of curvature (0 m<sup>−1</sup> to 2.93 m<sup>−1</sup>) and the variation of the measured fringe visibility.</p>
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<p>Tunable single laser wavelength between 1563.705 nm to 1558.05 nm for the curvatures from 0 m<sup>−1</sup> to 2.79 m<sup>−1</sup>.</p>
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<p>(<b>a</b>). Switchable dual-wavelength emissions generated at curvatures of 1.53 m<sup>−1</sup> with 1559.07 nm and 1563.66 nm, (<b>b</b>) 2.33 m<sup>−1</sup> with 1543.21 nm and 1549.287 nm, (<b>c</b>) 2.5 m<sup>−1</sup> with 1554.61 nm and 1559.667 nm, (<b>d</b>) 2.75 m<sup>−1</sup> with 1556.8 nm and 1561.877 nm.</p>
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<p>(<b>a</b>) Single-wavelength oscillation at 1562.22 nm, (<b>b</b>) dual-wavelength oscillation (1562.22–1562.875 nm), (<b>c</b>) triple-wavelength oscillation (1560.175–1562.22–1562.88 nm).</p>
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<p>(<b>a</b>) Quadruple-wavelength emission (1560.85–1561.51–1562.26–1562.86 nm), (<b>b</b>) quintuple-wavelength emission (1559.59–1560.91–1561.58–1562.93–1563.61 nm), and (<b>c</b>) sextuple-wavelength emission (1560.25–1560.97–1561.63–1562.29–1562.98–1563.64 nm).</p>
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<p>(<b>a</b>) Spectral distribution stability of a single laser oscillation at 1562.22 nm, with high-intensity uniformity across the spectrum, (<b>b</b>) a maximum wavelength shift of 0.01 nm, and (<b>c</b>) output power fluctuations of less than 0.12 dB.</p>
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<p>(<b>a</b>). Stability of the dual-wavelength laser oscillation at 1562.22–1562.785 nm with uniform intensity, (<b>b</b>) a maximum wavelength shift of 0.07 nm, and (<b>c</b>) output power fluctuations of less than 0.25 dB.</p>
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<p>(<b>a</b>) Power stability of the triple-wavelength laser system, (<b>b</b>) maximum wavelength shift of 0.07 nm, and (<b>c</b>) maximum amplitude fluctuation of 0.51dB for the 1562.88 nm line.</p>
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<p>(<b>a</b>) Power stability of the quadruple-wavelength laser system, (<b>b</b>) maximum wavelength shift of 0.22 nm, and (<b>c</b>) maximum amplitude fluctuation of 3 dB for the 1562.83 nm line.</p>
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<p>(<b>a</b>) Power stability of the quintuple-wavelength laser system, (<b>b</b>) maximum wavelength shift of 0.07 nm, and (<b>c</b>) maximum amplitude fluctuation of 1.7 dB for the 1561.58 nm line.</p>
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<p>(<b>a</b>) Power stability of the sextuple-wavelength laser system, (<b>b</b>) negligible wavelength shift, and (<b>c</b>) maximum amplitude fluctuation of 2.71 dB for the 1562.98 nm line.</p>
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13 pages, 4106 KiB  
Article
A Multi-Format, Multi-Wavelength Erbium-Doped Fiber Ring Laser Using a Tunable Delay Line Interferometer
by Cheng-Kai Yao, Amare Mulatie Dehnaw and Peng-Chun Peng
Appl. Sci. 2024, 14(16), 6933; https://doi.org/10.3390/app14166933 - 8 Aug 2024
Cited by 2 | Viewed by 1223
Abstract
This work demonstrates the use of an erbium-doped fiber amplifier (EDFA), a tunable bandpass filter (TBF), and a tunable delay line interferometer (TDLI) to form a ring laser that produces multi-format, multi-wavelength laser beams. The TDLI serves as the core of the proposed [...] Read more.
This work demonstrates the use of an erbium-doped fiber amplifier (EDFA), a tunable bandpass filter (TBF), and a tunable delay line interferometer (TDLI) to form a ring laser that produces multi-format, multi-wavelength laser beams. The TDLI serves as the core of the proposed laser generation system. TDLI harnesses the weak Fabry–Pérot (FP) interferences generated by its built-in 50/50 beamsplitter (BS) with unalterable filtering characteristics and the interferences with free spectral range (FSR) adjustable from each of its two outputs with nearly complementary phases to superpose and generate a variable interference standing wave. The interferometric standing wave and weak FP interferences are used to form a spatial-hole burning to promote the excitation of multi-format and multi-wavelength lasers. The proposed system enables dual-wavelength spacing ranging from 0.3 nm to 3.35 nm, with a switchable wavelength position at approximately 1527 nm to 1535 nm, providing flexible tunability. Full article
(This article belongs to the Special Issue Advanced Optical-Fiber-Related Technologies)
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<p>An experimental framework involves a multi-wavelength erbium-doped fiber ring laser with a delayed line interferometer (internal structure enlargement) as the primary component. (TDLI: tunable delay line interferometer; EDFA: erbium-doped fiber amplifier; TBF: tunable bandpass filter; OSA: optical spectral analyzer).</p>
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<p>(<b>a</b>) The spectrum shows multiple FP interferences resulting from the combination of two BS and the primary interference caused by TDLI with different FSRs by virtue of reflections from the end face of the fiber head. The EDFA emits light from port 1 into the TDLI, which is then reflected by port 3 and the BS into port 2 for observation by the OSA. (<b>b</b>) Transmission spectra of two-phase complementary interferences formed by TDLI and spectral characteristics of a multi-wavelength laser capable of output in the <a href="#applsci-14-06933-f001" class="html-fig">Figure 1</a> framework. The EDFA emits light, which passes from ports 3 to 2 and 1, respectively, and then yellow and blue line interferograms can be obtained with the OSA, respectively.</p>
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<p>(<b>a</b>) Dual-wavelength laser with variable spacing and consistent center position of dual wavelengths. (<b>b</b>) Dual-wavelength laser with intertwined wavelength positions. (<b>c</b>,<b>d</b>) Dual-wav-length laser with regular positional tuning and similar wavelength spacing (the subplot is a superimposed drawing of the spectrum that does not correspond to the power scale of the vertical axis).</p>
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<p>(<b>a</b>,<b>b</b>) The same dual-wavelength laser with different interferences and the spectral observation at different times.</p>
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<p>(<b>a</b>) Dual-wavelength laser with the narrowest wavelength spacing. (<b>b</b>) Dual-wavelength laser with several interfering lobes between the lasing wavelengths.</p>
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<p>(<b>a</b>,<b>b</b>) The wavelength position and the power corresponding to the peak of the lasing wavelength per minute are obtained from <a href="#applsci-14-06933-f004" class="html-fig">Figure 4</a>a,b, respectively. (<b>c</b>,<b>d</b>) The wavelength position and the power corresponding to the peak of the lasing wavelength per minute are obtained from <a href="#applsci-14-06933-f005" class="html-fig">Figure 5</a>a,b, respectively. (The yellow lines with circle signs represent the shorter wavelength; the pink lines with square signs represent the longer wavelength; the blue signs correspond to wavelength positions; and the dark signs correspond to power values).</p>
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<p>(<b>a</b>) A record of triple-wavelength lasers with the same wavelength spacing every ten minutes. (<b>b</b>) The wavelength position and the power corresponding to the peak of the lasing wavelength per ten minutes are obtained from (<b>a</b>). (The yellow line is at 1530.1 nm, the bright red line is at 1531.22 nm, and the coffee line is at 1532.34 nm; the dark signs correspond to wavelength positions, and the blue signs correspond to power values).</p>
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12 pages, 2898 KiB  
Communication
Polarization Influence on Er3+-Doped Multi-Wavelength Brillouin Fiber Laser Based on Fiber Loop Mirror
by Yunqi Hao, Miao Miao, Weitong Liao and Kun Yang
Photonics 2024, 11(7), 659; https://doi.org/10.3390/photonics11070659 - 13 Jul 2024
Viewed by 833
Abstract
Polarization influences on the performance of multi-wavelength Brillouin Er3+-doped fiber laser are investigated by adjusting the polarization controller (PC) in the fiber loop mirror (FLM), where the linear laser cavity is composed of a fiber-tailed mirror and an FLM, and the [...] Read more.
Polarization influences on the performance of multi-wavelength Brillouin Er3+-doped fiber laser are investigated by adjusting the polarization controller (PC) in the fiber loop mirror (FLM), where the linear laser cavity is composed of a fiber-tailed mirror and an FLM, and the stimulated Brillouin scattering (SBS) and the Er3+-doped fiber amplification (EDFA) simultaneously serve as the cavity gain. We realized 1–7 Brillouin laser lines by increasing the 980 nm pump power. For the first-order Brillouin laser, the signal–noise ratio (SNR) and optical intensity present a sinusoidal envelope; the conversion efficiency changes significantly from 0.56465 dBm/mw to 0.44975 dBm/mw by adjusting the ring’s angle in the PC; the first-order SBS thresholds are 20.4 mw, 36.1 mw and 28.5 mw at different angles θ2 = 36°, 276° and 300°, respectively; flatness between the two Brillouin lasers change obviously from 2.863 dB to 41.801 dB with different ring angles; the second-order Brillouin laser is suppressed and disappears finally at Δθ2 = −64° to −84° and 106°~136° angle variation. For the fifth-order Brillouin laser, the highest-order Brillouin laser line is seriously suppressed until it disappears at some angle variations similarly. The powers and wavelength stabilities for one-, three- and seven-wavelength Brillouin fiber lasers were measured in 1 h, and the obtained Er3+-doped multi-wavelength Brillouin fiber laser (MWBFL) worked stably during that time, but the stabilities become worse with higher SBS orders. Full article
(This article belongs to the Section Lasers, Light Sources and Sensors)
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<p>The scheme of multi-wavelength Brillouin Er<sup>3+</sup>-doped fiber laser.</p>
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<p>(<b>a</b>) The output spectra and (<b>b</b>) the number distribution of the Brillouin laser with different 980 nm power.</p>
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<p>First Brillouin wavelength: (<b>a</b>) spectra, (<b>b</b>) OSNR and (<b>c</b>) optical intensity with θ<sub>2</sub> variation.</p>
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<p>The conversion efficiencies for different θ<sub>2</sub>.</p>
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<p>(<b>a</b>) The laser bandwidth measurement setup; (<b>b</b>) the measurement of BFL linewidth by the homodyne spectrum method.</p>
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<p>The dual Brillouin wavelengths with EDFA.</p>
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<p>The flatness between two Brillouin wavelengths changing with angle θ<sub>2</sub>: (<b>a</b>) the optical spectra; (<b>b</b>) the flatness analysis.</p>
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<p>(<b>a</b>) Fifth-order Brillouin laser spectra with EDFA; (<b>b</b>) peak-values distribution of the 5th-Brillouin laser.</p>
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<p>(<b>a</b>) Five-wavelength Brillouin laser spectra with θ<sub>2</sub> variation; (<b>b</b>) the flatness distribution at different θ<sub>2</sub>.</p>
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<p>Stability of 1-wavelength Brillouin laser line in an hour: (<b>a</b>) the optical intensities (<b>b</b>) the central wavelengths.</p>
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<p>Stabilities of 3-wavelength BFL in an hour: (<b>a</b>) the optical intensities (<b>b</b>) the central wavelengths.</p>
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<p>Stabilities of 7-wavelength BFL in an hour: (<b>a</b>) the optical intensities (<b>b</b>) the central wavelengths.</p>
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13 pages, 8711 KiB  
Communication
Demonstration of Power-over-Fiber with Watts of Output Power Capabilities over Kilometers or at Cryogenic Temperatures
by Simon Fafard and Denis Masson
Photonics 2024, 11(7), 596; https://doi.org/10.3390/photonics11070596 - 26 Jun 2024
Cited by 2 | Viewed by 2262
Abstract
We demonstrate the use of laser diodes and multijunction photovoltaic power converters to efficiently deliver watts of electrical power for long-distance or cryogenic applications. Transmission through single-mode and multi-mode fibers at the wavelengths of 808 nm and 1470/1550 nm are studied. An electrical [...] Read more.
We demonstrate the use of laser diodes and multijunction photovoltaic power converters to efficiently deliver watts of electrical power for long-distance or cryogenic applications. Transmission through single-mode and multi-mode fibers at the wavelengths of 808 nm and 1470/1550 nm are studied. An electrical output power of ~0.1 W is obtained after a 5 km transmission through a standard single-mode SMF28 fiber fed with 0.25 W of optical power. An electrical output power of ~1 W is demonstrated after a 5 km transmission with a standard OM1 multi-mode fiber fed with ~2.5 W. Photovoltaic conversion efficiencies reaching Eff ~49% are obtained with an output voltage of ~5 V using commercial multijunction laser power converters. For low-temperature applications, an ultra-sensitive silicon photomultiplier (SiPM) is used to detect the residual light leaked from fibers as the temperature is decreased. Our study demonstrates that specific fiber types enable low-loss transmission compatible with cryogenic requirements and without light leakage triggering of the SiPM. A cryogenic power-over-fiber system at ~1470 nm is demonstrated with ~2 W of electrical power converted over a 10 m distance having a conversion efficiency of Eff > 65% at 77 K. Full article
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Figure 1
<p>Transmission losses’ dependence on the optical fiber length measured for standard single-mode (green curve) and multi-mode fibers (blue curve). The slopes give the dB/km loss parameters, while the intercepts represent the coupling losses from the lasers/patchcords/connectors used. The single-mode fiber is a Corning SMF28-Ultra with a core diameter of 8.2 μm, cladding of 125 μm, and NA ~0.14, which is fed from a pigtailed single-mode 1550 nm laser diode. The multi-mode fiber is a standard graded-index Corning InfiniCor OM1 fiber with a core diameter of 62.5 μm, cladding of 125 μm, and NA ~0.275 coupled from a pigtailed multi-mode 1470 nm laser diode having a 105 μm core and an NA ~0.22. A lens-coupler was used to minimize the coupling losses between the multi-mode laser and the OM1 fiber (OzOptics’ part #AA-300-33-1550-M-SP1) [<a href="#B44-photonics-11-00596" class="html-bibr">44</a>,<a href="#B45-photonics-11-00596" class="html-bibr">45</a>,<a href="#B46-photonics-11-00596" class="html-bibr">46</a>,<a href="#B47-photonics-11-00596" class="html-bibr">47</a>,<a href="#B48-photonics-11-00596" class="html-bibr">48</a>].</p>
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<p>Measured electrical output from Broadcom’s AFBR-POC205A9 multijunction PT10-InGaAs/InP laser power converter for single-mode transmission distances of 1 km (blue crosses) and 5 km (green X) with different optical input powers at 1550 nm. The transmitted optical power on the horizontal axis refers to the output power exiting the output end of the fiber.</p>
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<p>Measured electrical output from Broadcom’s AFBR-POC205A8 multijunction PT10-InGaAs/InP laser power converter for multi-mode transmission distances of 1 km (purple circles at 1550 nm) and 5 km (green circles at 1470 nm) for different optical input powers. The single-mode data of <a href="#photonics-11-00596-f002" class="html-fig">Figure 2</a> are also included for comparison.</p>
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<p>Picture of pigtailed multi-mode 808 nm laser diode in operation at 20 °C, revealing faint light leakage and some slightly brighter spots along the fiber length (<b>top</b>). The picture was taken from a smart-phone camera, which responded to the 808 nm light. Bottom: Another similar 808 nm laser diode in operation (powered with a DC/DC power supply) with room illumination to better view the laser pigtail (<b>bottom left</b>); and corresponding infrared smart-phone view, which highlights the laser light leakage (<b>bottom right</b>). The pigtail at the bottom was set up with a 30 mm diameter loop, which induced additional light leakage.</p>
Full article ">Figure 4 Cont.
<p>Picture of pigtailed multi-mode 808 nm laser diode in operation at 20 °C, revealing faint light leakage and some slightly brighter spots along the fiber length (<b>top</b>). The picture was taken from a smart-phone camera, which responded to the 808 nm light. Bottom: Another similar 808 nm laser diode in operation (powered with a DC/DC power supply) with room illumination to better view the laser pigtail (<b>bottom left</b>); and corresponding infrared smart-phone view, which highlights the laser light leakage (<b>bottom right</b>). The pigtail at the bottom was set up with a 30 mm diameter loop, which induced additional light leakage.</p>
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<p>The −40 V dark-current of a silicon photomultiplier (Broadcom’s AFBR-S4xx SiPM) was used to evaluate, with the highest possible sensitivity, the residual light emanating from various multi-mode optical fiber configurations as a function of the ambient temperature. The “common fibers” (blue and purple curves) are step-index fiber types with a 400 μm core and protected with a furcation tubing jacket, as shown in <a href="#photonics-11-00596-f004" class="html-fig">Figure 4</a>. The “polyimide fiber” (green curve) is a bare polyimide fiber (no tubing jacket) from Thorlabs’ FG400LEP multi-mode fiber with a 400 μm core and an NA ~0.22. Compared to the SiPM current in the dark (black curve: “No light”), obtained in complete darkness, the polyimide fiber exhibited no measurable light leakage over the temperature range studied.</p>
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<p>Measured electrical output at 77 K for different optical input powers at 1466 nm transmitted through 10 m of bare polyimide multi-mode fiber, converted using Broadcom’s AFBR-POC205A8 multijunction PT10-InGaAs/InP laser power converter.</p>
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<p>Measured output power as a function of temperature for an AFBR-POC205A9 LPC with 1.5 W of optical input at about 1470 nm. Fiber light leakage can parasitically reduce the measured LPC output power at lower temperatures when fiber types other than bare polyimide fibers are used.</p>
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12 pages, 4682 KiB  
Article
Numerical Modeling of Mid-IR Lasers Based on Tb-Doped Chalcogenide Multicore Fibers
by Nikolay I. Salnikov, Alexey V. Andrianov and Elena A. Anashkina
Fibers 2024, 12(3), 25; https://doi.org/10.3390/fib12030025 - 11 Mar 2024
Viewed by 1860
Abstract
Mid-IR fiber lasers operating at wavelengths near 5 μm are of great interest for many fundamental and industrial applications, but only a few experimental samples based on active chalcogenide fibers have been demonstrated so far. One of the limitations of the power of [...] Read more.
Mid-IR fiber lasers operating at wavelengths near 5 μm are of great interest for many fundamental and industrial applications, but only a few experimental samples based on active chalcogenide fibers have been demonstrated so far. One of the limitations of the power of such lasers may be a fairly low fiber damage threshold. To solve this problem, we developed and numerically investigated in detail a mid-IR fiber laser at 5.3 µm with multi-W output power pumped into the cladding at a wavelength of 2 µm. We proposed using a Tb-doped chalcogenide multicore fiber with 25 single-mode cores arranged in a 5 × 5 square lattice as an active medium. The proposed laser design surpasses the power limit of single-core chalcogenide fibers. When simulating lasers, we specified realistic parameters of Tb-doped chalcogenide glass based on published experimental data. We performed a comprehensive theoretical analysis, studied the influence of various factors on the characteristics of generation, and found optimal system parameters and expected generation parameters. Full article
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Graphical abstract

Graphical abstract
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<p>(<b>a</b>) Simplified scheme of the energy levels of Tb<sup>3+</sup> ions. (<b>b</b>) Emission and absorption cross-sections of <sup>7</sup>F<sub>5</sub> → <sup>7</sup>F<sub>6</sub> laser transition.</p>
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<p>(<b>a</b>) Cross-section of chalcogenide multicore fiber with Tb-doped cores arranged in a 5 × 5 square lattice. Modeled electric fields of in-phase (<b>b</b>) and out-of-phase (<b>c</b>) supermodes. Intensity distributions of the laser beam before (<b>d</b>), after one (<b>e</b>), and after two (<b>f</b>) steps of CBC, calculated in the far field after propagating a path of 5 cm.</p>
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<p>(<b>a</b>) Scheme of Tb-doped chalcogenide glass fiber laser. CBC is the system for coherent beam combining by summing out-of-phase supermode with two beamsplitters. Evolution of intracavity powers at pump wavelength (<b>b</b>) and at signal wavelength (<b>c</b>) modeled for <span class="html-italic">P<sub>pump</sub></span> = 30 W, <span class="html-italic">L</span> = 150 cm, and <span class="html-italic">R</span><sub>2</sub> = 0.19.</p>
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<p>Output laser power vs. fiber cavity length <span class="html-italic">L</span> and reflection coefficient <span class="html-italic">R</span><sub>2</sub> for <span class="html-italic">P<sub>pump</sub></span> = 30 W. The dashed curve shows the optimal fiber length that maximizes output laser power for certain <span class="html-italic">R</span><sub>2</sub>.</p>
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<p>Output laser power vs. pump power <span class="html-italic">P<sub>pump</sub></span> and reflection coefficient <span class="html-italic">R</span><sub>2</sub> for <span class="html-italic">L</span> = 150 cm.</p>
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<p>Output laser power vs. pump power, modeled for <span class="html-italic">L</span> = 100 cm (<b>a</b>) and <span class="html-italic">L</span> = 150 cm (<b>b</b>) and varied <span class="html-italic">R</span><sub>2</sub>.</p>
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<p>Output laser power vs. fiber cavity length <span class="html-italic">L</span> and pump power <span class="html-italic">P<sub>pump</sub></span> for <span class="html-italic">R</span><sub>2</sub> = 0.19. The dashed curve shows the optimal fiber length that maximizes output laser power for certain <span class="html-italic">P<sub>pump</sub></span>.</p>
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<p>Output laser power vs. fiber intracavity length modeled for <span class="html-italic">P<sub>pump</sub></span> = 10 W (<b>a</b>); <span class="html-italic">P<sub>pump</sub></span> = 20 W (<b>b</b>); and <span class="html-italic">P<sub>pump</sub></span> = 30 W (<b>c</b>) for varied <span class="html-italic">R</span><sub>2</sub>.</p>
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<p>Output laser power vs. pump power, modeled for <span class="html-italic">L</span> = 150 cm, <span class="html-italic">R</span><sub>2</sub> = 0.19, and varied fiber background losses.</p>
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<p>Output laser power vs. fiber intracavity length, modeled for <span class="html-italic">P<sub>pump</sub></span> = 30 W (<b>a</b>); <span class="html-italic">P<sub>pump</sub></span> = 100 W (<b>b</b>), <span class="html-italic">R</span><sub>2</sub> = 0.19, and varied fiber background losses.</p>
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18 pages, 2605 KiB  
Review
Brief Review of Recent Developments in Fiber Lasers
by Galina Nemova
Appl. Sci. 2024, 14(6), 2323; https://doi.org/10.3390/app14062323 - 10 Mar 2024
Cited by 9 | Viewed by 3981
Abstract
This review covers the recent achievements in high-power rare earth (RE)-doped fiber lasers, Raman fiber lasers, and Brillouin fiber lasers. RE-doped fiber lasers have many applications such as laser cutting, laser welding, laser cleaning, and laser precision processing. They operate in several wavelength [...] Read more.
This review covers the recent achievements in high-power rare earth (RE)-doped fiber lasers, Raman fiber lasers, and Brillouin fiber lasers. RE-doped fiber lasers have many applications such as laser cutting, laser welding, laser cleaning, and laser precision processing. They operate in several wavelength ranges including 1050–1120 nm (ytterbium-doped fiber lasers), 1530–1590 nm (erbium- and erbium–ytterbium-doped fiber lasers), and 1900–2100 nm (thulium- and holmium-doped fiber lasers). White spaces in the wavelength spectrum, where no RE-doped fiber lasers are available, can be covered by Raman lasers. The heat power generated inside the laser active medium due to the quantum defect degrades the performance of the laser causing, for example, transverse-mode instability and thermal lensing. It can even cause catastrophic fiber damage. Different approaches permitting the mitigation of the heat generation process are considered in this review. Brillouin fiber lasers, especially multiwavelength Brillouin fiber lasers, have several important applications including optical communication, microwave generation, and temperature sensing. Recent progress in Brillouin fiber lasers is considered in this review. Full article
(This article belongs to the Special Issue Advanced Optical-Fiber-Related Technologies)
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Figure 1
<p>Diagrams of energy levels and transitions for some Yb<sup>3+</sup>, Er<sup>3+</sup>, Tm<sup>3+</sup>, and Ho<sup>3+</sup> ions.</p>
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<p>Energy diagrams of a traditional four-level laser (<b>a</b>) and a radiation-balanced laser (<b>b</b>). <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>λ</mi> </mrow> <mrow> <mi>P</mi> </mrow> </msub> </mrow> </semantics></math> and <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>λ</mi> </mrow> <mrow> <mi>L</mi> </mrow> </msub> <mtext> </mtext> </mrow> </semantics></math>are the pump and laser frequencies, respectively. <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>λ</mi> </mrow> <mrow> <mi>F</mi> </mrow> </msub> </mrow> </semantics></math> is the mean fluorescence frequency. Solid and dushed arrows illustrate photon and phonon transitions, respectively.</p>
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<p>Power evolution of all-fiber laser oscillators operating at ~1000 nm [<a href="#B37-applsci-14-02323" class="html-bibr">37</a>,<a href="#B38-applsci-14-02323" class="html-bibr">38</a>,<a href="#B39-applsci-14-02323" class="html-bibr">39</a>,<a href="#B40-applsci-14-02323" class="html-bibr">40</a>,<a href="#B41-applsci-14-02323" class="html-bibr">41</a>,<a href="#B42-applsci-14-02323" class="html-bibr">42</a>,<a href="#B43-applsci-14-02323" class="html-bibr">43</a>,<a href="#B44-applsci-14-02323" class="html-bibr">44</a>,<a href="#B45-applsci-14-02323" class="html-bibr">45</a>,<a href="#B46-applsci-14-02323" class="html-bibr">46</a>,<a href="#B47-applsci-14-02323" class="html-bibr">47</a>,<a href="#B48-applsci-14-02323" class="html-bibr">48</a>].</p>
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<p>Power evolution of Er<sup>3+</sup>-doped and Er<sup>3+</sup>-Yb<sup>3+</sup> co-doped fiber lasers operating at ~1.5 μm [<a href="#B50-applsci-14-02323" class="html-bibr">50</a>,<a href="#B51-applsci-14-02323" class="html-bibr">51</a>,<a href="#B52-applsci-14-02323" class="html-bibr">52</a>,<a href="#B53-applsci-14-02323" class="html-bibr">53</a>,<a href="#B54-applsci-14-02323" class="html-bibr">54</a>,<a href="#B55-applsci-14-02323" class="html-bibr">55</a>,<a href="#B56-applsci-14-02323" class="html-bibr">56</a>,<a href="#B57-applsci-14-02323" class="html-bibr">57</a>,<a href="#B58-applsci-14-02323" class="html-bibr">58</a>,<a href="#B59-applsci-14-02323" class="html-bibr">59</a>,<a href="#B60-applsci-14-02323" class="html-bibr">60</a>,<a href="#B61-applsci-14-02323" class="html-bibr">61</a>].</p>
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<p>Power evolution of Tm<sup>3+</sup>-doped and Tm<sup>3+</sup>-Ho<sup>3+</sup> co-doped fiber lasers operating at ~2 μm [<a href="#B62-applsci-14-02323" class="html-bibr">62</a>,<a href="#B63-applsci-14-02323" class="html-bibr">63</a>,<a href="#B64-applsci-14-02323" class="html-bibr">64</a>,<a href="#B65-applsci-14-02323" class="html-bibr">65</a>,<a href="#B66-applsci-14-02323" class="html-bibr">66</a>,<a href="#B67-applsci-14-02323" class="html-bibr">67</a>,<a href="#B68-applsci-14-02323" class="html-bibr">68</a>,<a href="#B69-applsci-14-02323" class="html-bibr">69</a>,<a href="#B70-applsci-14-02323" class="html-bibr">70</a>,<a href="#B71-applsci-14-02323" class="html-bibr">71</a>].</p>
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<p>Processes that take place in a Raman laser: (<b>a</b>) stimulated Stokes Raman scattering (SSRS), (<b>b</b>) stimulated anti-Stokes Raman scattering (SARS), (<b>c</b>) coherent anti-Stokes Raman scattering (CARS) when it converts a Stokes photon and a pump photon to an anti-Stokes photon and a pump photon, annihilating two phonons, and (<b>d</b>) CARS when it converts an anti-Stokes photon and a pump photon to a Stokes photon and a pump photon, creating two phonons. <math display="inline"><semantics> <mrow> <msub> <mrow> <mtext> </mtext> <mi>ω</mi> </mrow> <mrow> <mi>P</mi> </mrow> </msub> </mrow> </semantics></math>, <math display="inline"><semantics> <mrow> <msub> <mrow> <mtext> </mtext> <mi>ω</mi> </mrow> <mrow> <mi>S</mi> </mrow> </msub> </mrow> </semantics></math>, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>ω</mi> </mrow> <mrow> <mi>a</mi> <mi>S</mi> </mrow> </msub> </mrow> </semantics></math>, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>Ω</mi> </mrow> <mrow> <mi>o</mi> <mi>p</mi> </mrow> </msub> </mrow> </semantics></math> are the pump, Stokes, anti-Stokes, and optical phonon frequencies, respectively.</p>
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<p>The energy level diagram of Brillouin scattering. (<b>a</b>) Brillouin Stokes scattering; (<b>b</b>) Brillouin anti-Stokes scattering. <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>ω</mi> </mrow> <mrow> <mi>P</mi> </mrow> </msub> </mrow> </semantics></math>, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>ω</mi> </mrow> <mrow> <mi>S</mi> </mrow> </msub> </mrow> </semantics></math>, <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>ω</mi> </mrow> <mrow> <mi>a</mi> <mi>S</mi> </mrow> </msub> </mrow> </semantics></math>, and <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>Ω</mi> </mrow> <mrow> <mi>a</mi> <mi>p</mi> </mrow> </msub> </mrow> </semantics></math> are the pump, Stokes, anti-Stokes, and acoustic phonon frequencies, respectively.</p>
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<p>Illustration of the cascaded SBS process. It occurs via the interplay of SBS and four-wave mixing.</p>
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114 pages, 85007 KiB  
Review
Advancements in Additive Manufacturing for Copper-Based Alloys and Composites: A Comprehensive Review
by Alireza Vahedi Nemani, Mahya Ghaffari, Kazem Sabet Bokati, Nima Valizade, Elham Afshari and Ali Nasiri
J. Manuf. Mater. Process. 2024, 8(2), 54; https://doi.org/10.3390/jmmp8020054 - 2 Mar 2024
Cited by 8 | Viewed by 4628
Abstract
Copper-based materials have long been used for their outstanding thermal and electrical conductivities in various applications, such as heat exchangers, induction heat coils, cooling channels, radiators, and electronic connectors. The development of advanced copper alloys has broadened their utilization to include structural applications [...] Read more.
Copper-based materials have long been used for their outstanding thermal and electrical conductivities in various applications, such as heat exchangers, induction heat coils, cooling channels, radiators, and electronic connectors. The development of advanced copper alloys has broadened their utilization to include structural applications in harsh service conditions found in industries like oil and gas, marine, power plants, and water treatment, where good corrosion resistance and a combination of high strength, wear, and fatigue tolerance are critical. These advanced multi-component structures often have complex designs and intricate geometries, requiring extensive metallurgical processing routes and the joining of the individual components into a final structure. Additive manufacturing (AM) has revolutionized the way complex structures are designed and manufactured. It has reduced the processing steps, assemblies, and tooling while also eliminating the need for joining processes. However, the high thermal conductivity of copper and its high reflectivity to near-infrared radiation present challenges in the production of copper alloys using fusion-based AM processes, especially with Yb-fiber laser-based techniques. To overcome these difficulties, various solutions have been proposed, such as the use of high-power, low-wavelength laser sources, preheating the build chamber, employing low thermal conductivity building platforms, and adding alloying elements or composite particles to the feedstock material. This article systematically reviews different aspects of AM processing of common industrial copper alloys and composites, including copper-chrome, copper-nickel, tin-bronze, nickel-aluminum bronze, copper-carbon composites, copper-ceramic composites, and copper-metal composites. It focuses on the state-of-the-art AM techniques employed for processing different copper-based materials and the associated technological and metallurgical challenges, optimized processing variables, the impact of post-printing heat treatments, the resulting microstructural features, physical properties, mechanical performance, and corrosion response of the AM-fabricated parts. Where applicable, a comprehensive comparison of the results with those of their conventionally fabricated counterparts is provided. Full article
(This article belongs to the Special Issue High-Performance Metal Additive Manufacturing)
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Figure 1
<p>Different types of defects in WAAM, laser AM, and arc welding processes (Reprinted with permission from [<a href="#B40-jmmp-08-00054" class="html-bibr">40</a>]).</p>
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<p>Effect of laser wavelength on the absorption rate of various metals (Reprinted with permission from [<a href="#B26-jmmp-08-00054" class="html-bibr">26</a>]).</p>
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<p>An example of unsuccessful L-PBF-processed copper using laser powers less than 200 W, resulting in highly porous parts (Reprinted with permission from [<a href="#B53-jmmp-08-00054" class="html-bibr">53</a>]).</p>
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<p>Breakage in the optical mirror of the laser source due to laser back reflection during the L-PBF processing of copper (Reprinted with permission from [<a href="#B56-jmmp-08-00054" class="html-bibr">56</a>]).</p>
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<p>The effect of preheating temperature on the density of L-PBF-fabricated copper parts; (<b>a</b>–<b>c</b>) preheating temperature of 200 °C, and (<b>d</b>–<b>f</b>) preheating temperature of 400 °C (Reprinted with permission from [<a href="#B3-jmmp-08-00054" class="html-bibr">3</a>]).</p>
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<p>(<b>a</b>) Effect of laser wavelength on the laser absorptivity of pure copper [<a href="#B55-jmmp-08-00054" class="html-bibr">55</a>], (<b>b</b>) comparison between the optical absorption of pure copper powders, tin-coated powders of R1 (1.36 wt.%) and R2 (0.28 wt.%), and pre-alloyed CuSn0.3 powders (Reprinted with permission from [<a href="#B59-jmmp-08-00054" class="html-bibr">59</a>]).</p>
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<p>(<b>a</b>,<b>b</b>) Optical micrographs, (<b>c</b>,<b>d</b>) SEM images, (<b>e</b>,<b>f</b>) bright-field TEM micrographs, and (<b>g</b>,<b>h</b>) HR-TEM images taken from the L-PBF-fabricated Cu-0.5Cr alloy (Reprinted with permission from [<a href="#B60-jmmp-08-00054" class="html-bibr">60</a>]).</p>
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<p>The top view of L-PBF-fabricated CuCr1 parts using (<b>a</b>) virgin and (<b>b</b>) nitrided powders. The corresponding side views of samples fabricated with (<b>c</b>) virgin and (<b>d</b>) nitrided powders (Reprinted with permission from [<a href="#B64-jmmp-08-00054" class="html-bibr">64</a>]).</p>
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<p>Optical microscopy images showing the porosity level in L-PBF-fabricated CuCr1 samples using (<b>a</b>) carbon-mixed and (<b>b</b>) carburized powders (Reprinted with permission from [<a href="#B65-jmmp-08-00054" class="html-bibr">65</a>]).</p>
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<p>SEM images showing the improvement in the density level of L-PBF-fabricated Cu-0.8Cr alloy manufactured by (<b>a</b>) virgin Cu-0.8Cr powders and (<b>b</b>) Cu-0.8Cr + 0.2 wt.% TiC powders (Reprinted with permission from [<a href="#B66-jmmp-08-00054" class="html-bibr">66</a>]).</p>
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<p>Microstructure of the L-PBF-fabricated Cu-Cr alloys using (<b>a</b>) nitrided CuCr powders (Reprinted with permission from [<a href="#B64-jmmp-08-00054" class="html-bibr">64</a>]), (<b>b</b>) carburized CuCr powders (Reprinted with permission from [<a href="#B65-jmmp-08-00054" class="html-bibr">65</a>]), and (<b>c</b>) carbon-mixed CuCr powders (Reprinted with permission from [<a href="#B63-jmmp-08-00054" class="html-bibr">63</a>]).</p>
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<p>SEM images of the L-PBF Cu-Cr0.5 samples solution-treated at (<b>a</b>) 920 °C, (<b>b</b>) 940 °C, (<b>c</b>) 960 °C, (<b>d</b>) 980 °C, (<b>e</b>) 1000 °C, and (<b>f</b>) 1020 °C (Reprinted with permission from [<a href="#B61-jmmp-08-00054" class="html-bibr">61</a>]).</p>
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<p>TEM images taken from the L-PBF CuCr0.5 sample (<b>a</b>) before and (<b>b</b>) after solution treatment at 1020 °C, confirming the reduction in dislocation density during the heat treatment (Reprinted with permission from [<a href="#B61-jmmp-08-00054" class="html-bibr">61</a>]).</p>
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<p>Microstructure of the L-PBF-fabricated Cu-0.5Cr alloy after (<b>a</b>) direct aging at 480 °C and (<b>b</b>) solutioning at 1020 °C + aging at 480 °C (Reprinted with permission from [<a href="#B61-jmmp-08-00054" class="html-bibr">61</a>]).</p>
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<p>(<b>a</b>) Low-magnification image showing the distribution of Cr in the Cu matrix of a L-PBF processed CuCr20 alloy, and (<b>b</b>) higher magnification of the box shown in image (<b>a</b>). (<b>c</b>,<b>d</b>) Higher magnification images showing the distribution of Cr in the Cu matrix (Reprinted with permission from [<a href="#B67-jmmp-08-00054" class="html-bibr">67</a>]).</p>
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<p>(<b>a</b>) Effect of heat treatment temperature and time on the electrical conductivity of L-PBF-fabricated CuCr20 and CuCr25 alloys (Reprinted with permission from [<a href="#B67-jmmp-08-00054" class="html-bibr">67</a>]) and (<b>b</b>) effect of annealing temperature on the electrical conductivity of L-PBF-fabricated Cu-1.3Cr and Cu-2.5Cr alloys (Reprinted with permission from [<a href="#B62-jmmp-08-00054" class="html-bibr">62</a>]).</p>
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<p>(<b>a</b>) Effect of post-printing aging time and temperature on the Vickers hardness of L-PBF-fabricated CuCr20 and CuCr25 alloys (Reprinted with permission from [<a href="#B67-jmmp-08-00054" class="html-bibr">67</a>]) and (<b>b</b>) effect of annealing temperature on the hardness of L-PBF-fabricated 1.3Cr and 2.5Cr alloys (Reprinted with permission from [<a href="#B62-jmmp-08-00054" class="html-bibr">62</a>]).</p>
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<p>(<b>a</b>) Elongation, (<b>b</b>) yield strength, and (<b>c</b>) tensile strength of traditionally and L-PBF-fabricated Cu-0.5Cr alloy (the applied heat treatment cycles for the L-PBF sample: direct aging at 480 °C, solutioning at 1020 °C, and solutioning at 1020 °C + aging at 480 °C) [<a href="#B60-jmmp-08-00054" class="html-bibr">60</a>,<a href="#B61-jmmp-08-00054" class="html-bibr">61</a>].</p>
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<p>Effect of annealing temperature on the tensile strength and breaking elongation of L-PBF (<b>a</b>) Cu-1.3Cr and (<b>b</b>) Cu-2.5Cr alloys fabricated in parallel (0°) and perpendicular (90°) to the stacking directions, and SEM images taken from the fractured surfaces of the L-PBF Cu-1.3Cr alloy fabricated in (<b>c</b>) parallel (0°) and (<b>d</b>) perpendicular (90°) directions schematically shown in (<b>e</b>), and (<b>f</b>) a vertical cross-section image showing the crack propagation in the as-printed Cu-1.3Cr L-PBF sample (Reprinted with permission from [<a href="#B62-jmmp-08-00054" class="html-bibr">62</a>]).</p>
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<p>(<b>a</b>,<b>b</b>) Elongation, (<b>c</b>,<b>d</b>) yield strength, and (<b>e</b>,<b>f</b>) tensile strength of L-PBF Cu-Cr alloys manufactured by CuCr0.3 [<a href="#B63-jmmp-08-00054" class="html-bibr">63</a>], CuCr0.3 mixed with 0.05 wt.% carbon nano-particle [<a href="#B63-jmmp-08-00054" class="html-bibr">63</a>], carburized CuCr1 [<a href="#B65-jmmp-08-00054" class="html-bibr">65</a>], and nitrided CuCr1 [<a href="#B64-jmmp-08-00054" class="html-bibr">64</a>] before and after different heat treatments. (Note: AB, S+A, and DA stand for as-built, solutionized+aged, and directly aged, respectively.).</p>
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<p>(<b>a</b>) Relative density of Cu-0.8Cr + 0.2 wt.% TiC and virgin Cu-0.8Cr samples manufactured by L-PBF process with laser power of 320 W and various scan speeds of 500 mm/s, 600 mm/s, 700 mm/s, 800 mm/s, and 1000 mm/s; (<b>b</b>) UTS, Rp0.2, and elongation of L-PBF samples fabricated by laser power of 320 W and scan speed of 600 mm/s. Fracture morphologies of (<b>c</b>,<b>d</b>) Cu-0.8Cr and (<b>e</b>,<b>f</b>) Cu-0.8Cr + 0.2 wt.% TiC tensile samples (Reprinted with permission from [<a href="#B66-jmmp-08-00054" class="html-bibr">66</a>]).</p>
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<p>(<b>a</b>) Corrosion potential (E<sub>corr</sub>) and (<b>b</b>) corrosion current density (i<sub>corr</sub>) of the L-PBF Cu-0.5Cr samples before and after different heat treatments in 3.5 wt.% NaCl solution (applied heat treatments: direct aging at 480 °C, solutioning at 1020 °C, and solutioning at 1020 °C + aging at 480 °C) [<a href="#B61-jmmp-08-00054" class="html-bibr">61</a>].</p>
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<p>Microstructure of L-DED CuCr30 samples (<b>a</b>) before and (<b>b</b>) after the extrusion process, along with the corresponding EBSD analysis (<b>c</b>) before and (<b>d</b>) after the extrusion process. (<b>e</b>,<b>f</b>) Bright field TEM images taken from the L-DED CuCr30 alloy after the extrusion process indicate the formation of twins (Reprinted with permission from [<a href="#B80-jmmp-08-00054" class="html-bibr">80</a>]).</p>
Full article ">Figure 24
<p>(<b>a</b>) Electrical conductivity, (<b>b</b>) density, and (<b>c</b>) tensile strength of vacuum casted, as-printed L-DED, and L-DED +extruded CuCr30 alloy [<a href="#B80-jmmp-08-00054" class="html-bibr">80</a>,<a href="#B81-jmmp-08-00054" class="html-bibr">81</a>].</p>
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<p>(<b>a</b>) Low-magnification SEM image taken from the EBM-fabricated Cu-25Cr alloy. (<b>b</b>,<b>c</b>) EDS elemental analysis taken from areas A and B. (<b>d</b>) A high-resolution FIB-SEM image taken from an EBM-fabricated Cu-25Cr alloy (Reprinted with permission from [<a href="#B84-jmmp-08-00054" class="html-bibr">84</a>]).</p>
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<p>Typical microstructure of Cu-Cr alloys fabricated using different AM methods (Reprinted with minor edits with permission from [<a href="#B60-jmmp-08-00054" class="html-bibr">60</a>,<a href="#B67-jmmp-08-00054" class="html-bibr">67</a>,<a href="#B80-jmmp-08-00054" class="html-bibr">80</a>,<a href="#B84-jmmp-08-00054" class="html-bibr">84</a>]).</p>
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<p>Effect of pre/post-printing processes on the electrical conductivities and tensile strengths of different Cu-Cr alloys fabricated by traditional manufacturing and AM methods.</p>
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<p>Microstructure of the L-PBF-fabricated Cu81-Ni19 alloy (labeled as a 3D model) and the substrate in the annealed state (labeled as a monolith) (Reprinted with permission from [<a href="#B88-jmmp-08-00054" class="html-bibr">88</a>]).</p>
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<p>SEM images of L-PBF Cu-Ni alloy (Cu76-Ni14.8-Sn7-Pb1.6) with laser scan speeds of (<b>a</b>) 100 mm/s, (<b>b</b>) 200 mm/s, and (<b>c</b>) 300 mm/s (layer thickness: 20 μm) [<a href="#B86-jmmp-08-00054" class="html-bibr">86</a>].</p>
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<p>Thickness and mass density of L-PBF Cu-Ni monolayers (Cu71-Ni22.8-Sn4.7-Pb1.43) fabricated at (<b>a</b>,<b>b</b>) laser power of 190 W with different scan speeds of 25, 50, and 80 mm/s, and (<b>c</b>,<b>d</b>) at different laser powers of 190 and 260 W with the scan speed of 80 mm/s [<a href="#B89-jmmp-08-00054" class="html-bibr">89</a>].</p>
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<p>After-corrosion (in NaCl) topography of the L-PBF-fabricated Cu76-Ni14.8-Sn7-Pb1.6 alloy with a layer thickness of (<b>a</b>–<b>c</b>) 20 μm and different laser scan speeds of (<b>a</b>) 100 mm/s, (<b>b</b>) 200 mm/s, and (<b>c</b>) 300 mm/s, and a layer thickness of 60 μm and different laser scan speeds of (<b>d</b>) 100 mm/s, (<b>e</b>) 200 mm/s, and (<b>f</b>) 300 mm/s (Reprinted with permission from [<a href="#B86-jmmp-08-00054" class="html-bibr">86</a>]).</p>
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<p>Tensile strength of L-PBF Cu-Ni (Cu71-Ni22.8-Sn4.7-Pb1.43) monolayers fabricated at (<b>a</b>) laser power of 190 W with different scan speeds and (<b>b</b>) different laser powers with a scan speed of 80 mm/s (Reprinted with permission from [<a href="#B89-jmmp-08-00054" class="html-bibr">89</a>]).</p>
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<p>(<b>a</b>) The order of the deposition and (<b>b</b>) a photographic view of the as-built structure of the graded Cu-Ni alloy fabricated by the L-DED process (Reprinted with permission from [<a href="#B33-jmmp-08-00054" class="html-bibr">33</a>]).</p>
Full article ">Figure 34
<p>Surface morphology of L-DED-fabricated (<b>a</b>) pure Ni and (<b>b</b>) Cu-Ni alloy. The porosity distribution at the interface of (<b>c</b>) Ni-CuNi75, (<b>d</b>) CuNi75-CuNi50, and (<b>e</b>) CuNi50-CuNi25. (<b>f</b>) The XRD patterns of a L-DED-deposited graded Cu-Ni alloy (Reprinted with permission from [<a href="#B33-jmmp-08-00054" class="html-bibr">33</a>]).</p>
Full article ">Figure 35
<p>Microstructure of the L-DED-deposited graded Cu-Ni alloy at different locations of (<b>a</b>) the bottom layer, (<b>b</b>,<b>c</b>) the middle layers, and (<b>d</b>) the top layer (Reprinted with permission from [<a href="#B33-jmmp-08-00054" class="html-bibr">33</a>]).</p>
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<p>(<b>a</b>–<b>h</b>) EBSD data and (<b>i</b>–<b>l</b>) TEM analysis of WAAM-fabricated Cu-Ni alloy (the composition of filler: Cu-Si(0.082), Mn(0.89), S(0.01), P(0.04), Fe(0.64), Ti(0.25), and Ni(30.13) (wt.%)) (Reprinted with permission from [<a href="#B85-jmmp-08-00054" class="html-bibr">85</a>]).</p>
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<p>As-deposited microstructures of the L-DED-fabricated copper-nickel alloy using different elemental powder blends of (<b>a</b>) blend 1, (<b>b</b>) blend 2, (<b>c</b>) blend 3, and (<b>d</b>) blend 4, which are listed in <a href="#jmmp-08-00054-t004" class="html-table">Table 4</a> (Reprinted with permission from [<a href="#B92-jmmp-08-00054" class="html-bibr">92</a>]).</p>
Full article ">Figure 38
<p>Optical micrographs of the as-deposited microstructure of the L-DED-fabricated copper-nickel alloys using different sets of powder blends of pure copper and Delero-22 alloy, including (<b>a</b>) blend 1, (<b>b</b>) blend 2, (<b>c</b>) blend 3, (<b>d</b>) blend 4, and (<b>e</b>) blend 5, which are listed in <a href="#jmmp-08-00054-t005" class="html-table">Table 5</a> (Reprinted with permission from [<a href="#B92-jmmp-08-00054" class="html-bibr">92</a>]).</p>
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<p>(<b>a</b>) L-DED nozzle used for mixing and melting Cu-Ni powders to produce samples shown in (<b>b</b>). (<b>c</b>) The SEM-EDS of an area from the B1S1 sample (see <a href="#jmmp-08-00054-t006" class="html-table">Table 6</a>) (Reprinted with permission from [<a href="#B94-jmmp-08-00054" class="html-bibr">94</a>]).</p>
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<p>Microhardness variations along the building direction for two samples of L-DED-graded Cu-Ni alloy and pure Ni-Cu joint (Reprinted with permission from [<a href="#B33-jmmp-08-00054" class="html-bibr">33</a>]).</p>
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<p>Mechanical properties of Cu–Ni alloy fabricated by the WAAM process (the composition of filler: Cu-Si(0.082), Mn(0.89), S(0.01), P(0.04), Fe(0.64), Ti(0.25), and Ni(30.13) (wt.%)) [<a href="#B85-jmmp-08-00054" class="html-bibr">85</a>].</p>
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<p>Mechanical properties of miniature tensile Cu-Ni alloy samples manufactured by the L-DED process using various blends of copper-nickel powders listed in <a href="#jmmp-08-00054-t005" class="html-table">Table 5</a> (Reprinted with permission from [<a href="#B92-jmmp-08-00054" class="html-bibr">92</a>]).</p>
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<p>Variation in Vickers hardness values (HV<sub>0.2</sub>) along the height of the L-DED-deposited copper-nickel-graded material. (<b>a</b>,<b>c</b>,<b>e</b>): Hardness plots on set 1, set 2, and set 3 deposits of 100/0 (Ni/Cu) on 30/70 (Ni/Cu), respectively. (<b>b</b>,<b>d</b>,<b>f</b>): Hardness plots of set 1, set 2, and set 3 deposits of 30/70 (Ni/Cu) on 100/0 (Ni/Cu) (solid circles are the spot measurement, and the red dotted line is the moving average trend line with four measurements as the period) (Reprinted with permission from [<a href="#B93-jmmp-08-00054" class="html-bibr">93</a>]).</p>
Full article ">Figure 44
<p>(<b>a</b>) It represents 0.2% offset yield strength, (<b>b</b>) ultimate tensile strength, and (<b>c</b>) strain to break for the miniature tensile Cu-Ni alloy samples manufactured by L-DED using different sets of power and duty cycles (Reprinted with permission from [<a href="#B93-jmmp-08-00054" class="html-bibr">93</a>]).</p>
Full article ">Figure 45
<p>Resistivity and thermal conductivity along (<b>a</b>,<b>b</b>) x, y (in-plane), and z (cross-plane) directions from the same block of the L-DED-fabricated Cu-Ni sample (B1S2 in <a href="#jmmp-08-00054-t006" class="html-table">Table 6</a>), and (<b>c</b>,<b>d</b>) in the cross-plane direction measured for different blocks of the L-DED samples listed in <a href="#jmmp-08-00054-t006" class="html-table">Table 6</a> (Reprinted with permission from [<a href="#B94-jmmp-08-00054" class="html-bibr">94</a>]).</p>
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<p>(<b>a</b>) PDP and (<b>b</b>,<b>c</b>) EIS results for the Cu–Ni alloy fabricated by WAAM process (Reprinted with permission from [<a href="#B85-jmmp-08-00054" class="html-bibr">85</a>]).</p>
Full article ">Figure 47
<p>(<b>a</b>) XRD patterns of L-PBF and cast Cu–10Sn alloy, along with the corresponding SEM images taken from the microstructure of (<b>b</b>–<b>d</b>) L-PBF and (<b>e</b>) cast Cu–10Sn alloy, and (<b>f</b>) the corresponding stress–strain curves (Reprinted with permission from [<a href="#B104-jmmp-08-00054" class="html-bibr">104</a>]).</p>
Full article ">Figure 48
<p>(<b>a</b>,<b>b</b>) Bright-field TEM images, (<b>c</b>) higher resolution TEM image, and (<b>d</b>,<b>e</b>) EDS elemental maps taken from L-PBF-fabricated Cu-13Sn alloy. (<b>f</b>) A comparison between the mechanical properties of the L-PBF Cu-13Sn alloy (denoted as the present study) and other tin-bronzes fabricated by L-PBF or other fabrication methods (Reprinted with permission from [<a href="#B110-jmmp-08-00054" class="html-bibr">110</a>]).</p>
Full article ">Figure 49
<p>Effect of laser energy density on the (<b>a</b>) hardness and relative density, (<b>b</b>) yield strength, (<b>c</b>) tensile strength, and (<b>d</b>) ductility of L-PBF Cu-10Sn alloy, along with (<b>e</b>) the corresponding stress–strain curves. Microstructure of L-PBF Cu-10Sn parts fabricated at energy densities of (<b>f</b>) 210, (<b>g</b>) 220, and (<b>h</b>) 230 J/mm<sup>2</sup> (Reprinted with permission from [<a href="#B115-jmmp-08-00054" class="html-bibr">115</a>]).</p>
Full article ">Figure 50
<p>(<b>a</b>) Effect of laser energy density at different laser powers on the relative density of the L-PBF Cu-15Ni-8Sn alloy. SEM images at different magnifications taken from the microstructure of the L-PBF Cu-15Ni-8Sn alloy fabricated with a laser power of 340 W and energy densities of (<b>b</b>,<b>e</b>) 142 J/mm<sup>3</sup>, (<b>c</b>,<b>f</b>) 70 J/mm<sup>3</sup>, and (<b>d</b>,<b>g</b>) 142 J/mm<sup>3</sup> (Reprinted with permission from [<a href="#B117-jmmp-08-00054" class="html-bibr">117</a>]).</p>
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<p>Schematic illustration from the formation sequence of the L-PBF-fabricated Cu-15Sn alloy: (<b>a</b>) the initial deposited track in each layer, (<b>b</b>) the adjacent deposited track in the same layer, (<b>c</b>) the first deposited track in the subsequent layer, and (<b>d</b>) the effect of temperature gradient on the supercooling [<a href="#B8-jmmp-08-00054" class="html-bibr">8</a>]. SEM images showing the microstructure of an L-PBF fabricated Cu-10Sn alloy at (<b>e</b>) low-magnification side view and high-magnification images from (<b>f</b>) region 1, (<b>g</b>) region 2, and (<b>h</b>) region 3 (Reprinted with permission from [<a href="#B118-jmmp-08-00054" class="html-bibr">118</a>]).</p>
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<p>XRD patterns of the raw Cu-10Sn pre-alloyed powders, L-PBF part in the as-fabricated (AF) condition, and annealed samples at 600 and 800 °C in horizontal and vertical directions (Reprinted with permission from [<a href="#B118-jmmp-08-00054" class="html-bibr">118</a>]).</p>
Full article ">Figure 53
<p>(<b>a</b>) XRD patterns of the raw Cu-15Sn pre-alloyed powders, the L-PBF-fabricated part, and the annealed sample at 600 °C for 4 h, along with the (<b>b</b>–<b>e</b>) microstructure of the as-printed and (<b>f</b>,<b>g</b>) annealed L-PBF Cu-15Sn samples (Reprinted with permission from [<a href="#B8-jmmp-08-00054" class="html-bibr">8</a>]).</p>
Full article ">Figure 54
<p>EBSD-IPF maps of L-PBF Cu-10Sn samples: (<b>a</b>) as-printed-horizontal, (<b>b</b>) as-printed-vertical, (<b>c</b>) annealed at 600 °C-horizontal, (<b>d</b>) annealed at 600 °C-vertical, (<b>e</b>) annealed at 800 °C-horizontal, and (<b>f</b>) annealed at 800 °C-vertical (Reprinted with permission from [<a href="#B118-jmmp-08-00054" class="html-bibr">118</a>]).</p>
Full article ">Figure 55
<p>(<b>a</b>) Stress–strain curves of the conventionally fabricated QSn15-1-1 bar, as-printed, and annealed L-PBF Cu-15Sn samples at 500, 600, and 700 °C, along with the fractured surfaces of (<b>b</b>,<b>c</b>) as-printed and (<b>d</b>,<b>e</b>) annealed L-PBF Cu-15Sn samples at 600 °C for 4 h (Reprinted with permission from [<a href="#B8-jmmp-08-00054" class="html-bibr">8</a>]).</p>
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<p>Summary of the mechanical properties of various tin-bronzes, produced through different conventional and AM methods.</p>
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<p>(<b>a</b>) Thermal conductivity of the L-PBF Cu-10Sn alloy in the as-fabricated (AF) and annealed samples at 600 and 800 °C. (<b>b</b>) Effect of Sn content on the thermal conductivity of tin-bronzes and (<b>c</b>) effect of δ phase percentage on the Sn content in the α phase and thermal conductivity of tin-bronzes (Reprinted with permission from [<a href="#B118-jmmp-08-00054" class="html-bibr">118</a>]).</p>
Full article ">Figure 58
<p>(<b>a</b>) Weight loss versus immersion time curves of AF and annealed L-PBF Cu-10Sn samples at 600 and 800 °C, and (<b>b</b>) XRD results of the corroded surfaces after 11 days of immersion in a 3.5 wt.% NaCl water solution. The results of (<b>c</b>) OCP and (<b>d</b>) PDP tests of the AF and annealed L-PBF Cu-10Sn samples at 600 and 800 °C. SEM images taken from the corroded surfaces of the L-PBF Cu-10Sn alloy after immersion testing of (<b>e</b>) the sample annealed at 800 °C and (<b>f</b>,<b>g</b>) the AF sample (Reprinted with permission from [<a href="#B118-jmmp-08-00054" class="html-bibr">118</a>]).</p>
Full article ">Figure 59
<p>The pros and cons of different AM methods employed in bimetallic material fabrication [<a href="#B39-jmmp-08-00054" class="html-bibr">39</a>,<a href="#B128-jmmp-08-00054" class="html-bibr">128</a>,<a href="#B129-jmmp-08-00054" class="html-bibr">129</a>,<a href="#B130-jmmp-08-00054" class="html-bibr">130</a>,<a href="#B131-jmmp-08-00054" class="html-bibr">131</a>,<a href="#B132-jmmp-08-00054" class="html-bibr">132</a>,<a href="#B133-jmmp-08-00054" class="html-bibr">133</a>].</p>
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<p>(<b>a</b>–<b>c</b>) Schematic illustration of the L-PBF Cu10Sn-Ti6Al4V bimetallic structure with different interface processing strategies. Cross-section of L-PBF Cu10Sn-Ti6Al4V bimetallic structure fabricated using (<b>a1</b>,<b>a2</b>) direct boding strategy, (<b>b1</b>,<b>b2</b>) remelting method, and (<b>c1</b>,<b>c2</b>) FGM strategy (Reprinted with permission from [<a href="#B139-jmmp-08-00054" class="html-bibr">139</a>]).</p>
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<p>(<b>a1</b>–<b>e3</b>) Microstructural features of the interface between Cu10Sn and Ti6Al4V sides of the bimetallic structure fabricated by L-PBF with direct bonding strategy, remelting method, and FGM techniques (Reprinted with permission from [<a href="#B139-jmmp-08-00054" class="html-bibr">139</a>]).</p>
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<p>(<b>a</b>) L-PBF bimetallic 316L/CuSn10 structure and (<b>b</b>) the schematic illustrations of the interlayer staggered scanning strategy (<b>left</b>) and island scanning strategy (<b>right</b>). (<b>c</b>) The entire interfacial microstructure of L-PBF bimetallic 316L/CuSn10, (<b>d</b>) magnified area A of (<b>c</b>), (<b>e</b>) magnified area B of (<b>c</b>), (<b>f</b>) magnified area C of (<b>c</b>), (<b>g</b>) magnified area D of (<b>e</b>), and (<b>h</b>) a schematic illustration of the nucleation site and propagation direction of the cracks (Reprinted with permission from [<a href="#B145-jmmp-08-00054" class="html-bibr">145</a>]).</p>
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<p>XRD patterns taken from the L-PBF bimetallic 316L/CuSn10 structure in different regions, including the 316L side, CuSn10 side, and interface region (Reprinted with permission from [<a href="#B145-jmmp-08-00054" class="html-bibr">145</a>]).</p>
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<p>Stress–strain curves of single parts of (<b>a</b>) 316L SS, (<b>b</b>) CuSn10, and (<b>c</b>) horizontally combined and (<b>d</b>) vertically combined 316L/CuSn10 bimetallic materials fabricated by L-PBF (Reprinted with permission from [<a href="#B145-jmmp-08-00054" class="html-bibr">145</a>]).</p>
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<p>A schematic illustration showing the FDM process (Reprinted with permission from [<a href="#B150-jmmp-08-00054" class="html-bibr">150</a>]).</p>
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<p>Optical microscopy images showing the porosity distribution in FDM-fabricated Cu-10Sn bronze sintered at temperatures of (<b>a</b>) 850 °C, (<b>b</b>) 875 °C, and (<b>c</b>) 900 °C. (<b>d</b>) Stress–strain curves of the FDM-produced Cu-10Sn bronze sintered at temperatures of 850 °C, 875 °C, and 900 °C (Reprinted with permission from [<a href="#B150-jmmp-08-00054" class="html-bibr">150</a>]).</p>
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<p>A summary of microstructural features observed in NAB alloys fabricated using different conventional and AM methods [<a href="#B19-jmmp-08-00054" class="html-bibr">19</a>,<a href="#B155-jmmp-08-00054" class="html-bibr">155</a>,<a href="#B165-jmmp-08-00054" class="html-bibr">165</a>,<a href="#B167-jmmp-08-00054" class="html-bibr">167</a>,<a href="#B171-jmmp-08-00054" class="html-bibr">171</a>].</p>
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<p>An overview of the mechanical properties exhibited by NAB alloys fabricated by diverse conventional and AM methods.</p>
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<p>Microstructure of the cast NAB using (<b>a</b>) optical and (<b>b</b>) SEM images. TEM images taken from the microstructure of WAAM-fabricated NAB alloy: (<b>c</b>) low-magnification image showing the general microstructure, and (<b>d</b>,<b>e</b>) high-magnification images showing the intermetallic phases (Reprinted with permission from [<a href="#B152-jmmp-08-00054" class="html-bibr">152</a>]).</p>
Full article ">Figure 70
<p>Bright-field TEM images indicating (<b>a</b>) Cu matrix along with the corresponding SAED pattern confirming the presence of α phase and κ<sub>IV</sub> intermetallic, (<b>b</b>) globular κ<sub>II</sub> phases characterized as Fe<sub>3</sub>Al, and (<b>c</b>) lamellar κ<sub>III</sub> phases characterized as NiAl (Reprinted with permission from [<a href="#B152-jmmp-08-00054" class="html-bibr">152</a>]).</p>
Full article ">Figure 71
<p>Microstructure of heat-treated WAAM-produced NAB in three different conditions: (<b>a</b>,<b>b</b>) 350 °C for 2 h (HT-1), (<b>c</b>,<b>d</b>) 550 °C for 4 h (HT-2), and (<b>e</b>,<b>f</b>) 675 °C for 6 h (HT-3) (Reprinted with permission from [<a href="#B154-jmmp-08-00054" class="html-bibr">154</a>]).</p>
Full article ">Figure 72
<p>(<b>a</b>) Macrostructure of WAAM-fabricated NAB alloy (Cu-8Al-2Ni-2Fe-2Mn), microstructural features at (<b>b</b>) the bottom area of the first deposited layer, (<b>c</b>) transition from dendritic structure to cellular grains in the first deposited layer, (<b>d</b>,<b>e</b>) low- and high-magnification micrographs taken from the first interlayer band area, and (<b>f</b>,<b>g</b>) low- and high-magnification micrographs taken from the second interlayer band area (Reprinted with permission from [<a href="#B156-jmmp-08-00054" class="html-bibr">156</a>]).</p>
Full article ">Figure 73
<p>Top view of the microstructure of WAAM-fabricated NAB alloy (Cu-8Al-2Ni-2Fe-2Mn) taken from different locations of (<b>a</b>–<b>c</b>) bottom area, (<b>d</b>,<b>e</b>) top area, and (<b>f</b>) the very last deposited layer, confirming the microstructural coarsening from the bottom to the top regions (Reprinted with permission from [<a href="#B156-jmmp-08-00054" class="html-bibr">156</a>]).</p>
Full article ">Figure 74
<p>Effect of ultrasonic vibration on the columnar structure of WAAM NAB, (<b>a</b>) without ultrasonic vibration and (<b>b</b>) with ultrasonic vibration (Reprinted with permission from [<a href="#B157-jmmp-08-00054" class="html-bibr">157</a>]).</p>
Full article ">Figure 75
<p>CMT Twin torch along with the first deposited layer of NAB using a CMT Twin torch (Reprinted with permission from [<a href="#B158-jmmp-08-00054" class="html-bibr">158</a>]).</p>
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<p>(<b>a</b>) Engineering stress–strain curves of the cast and WAAM-NABs (Reprinted with permission from [<a href="#B152-jmmp-08-00054" class="html-bibr">152</a>]). (<b>b</b>) Stress–strain curves of the WAAM NAB in as-built and heat-treated conditions of HT-1 (350 °C for 2 h), HT-2 (550 °C for 4 h), and HT-3 (675 °C for 6 h) (Reprinted with permission from [<a href="#B154-jmmp-08-00054" class="html-bibr">154</a>]).</p>
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<p>(<b>a</b>) Wear depth and (<b>b</b>) weight loss of the WAAM and cast NABs during wear testing. (<b>c</b>) Microhardness profile showing the transition from the cast substrate to WAAM-fabricated NAB (Reprinted with permission from [<a href="#B22-jmmp-08-00054" class="html-bibr">22</a>]).</p>
Full article ">Figure 78
<p>Stress–strain curves of the cast NAB counterpart (C95220 alloys), and the WAAM NAB samples under different conditions (U2 and U3 are with ultrasonic vibration, and C3 is without ultrasonic vibration) (Reprinted with permission from [<a href="#B157-jmmp-08-00054" class="html-bibr">157</a>]).</p>
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<p>Mechanical properties of a WAAM-fabricated NAB alloy, including (<b>a</b>) tensile strength, (<b>b</b>) yield strength, (<b>c</b>) elongation, and (<b>d</b>) the standard deviation of tensile strength values. (Note: QT = quenching and tempering, and AF = as-fabricated.) (Reprinted with permission from [<a href="#B153-jmmp-08-00054" class="html-bibr">153</a>]).</p>
Full article ">Figure 80
<p>PFs of the WAAM-fabricated NAB alloy in different conditions of As-fabricated (AF), quenched (Q), quenched and tempered (QT), and directly tempered (T) (Reprinted with permission from [<a href="#B159-jmmp-08-00054" class="html-bibr">159</a>]).</p>
Full article ">Figure 81
<p>Microstructure of the (<b>a</b>) cast, (<b>b</b>) wrought, and (<b>c</b>,<b>d</b>) L-PBF-fabricated NAB counterparts (Reprinted with permission from [<a href="#B165-jmmp-08-00054" class="html-bibr">165</a>]).</p>
Full article ">Figure 82
<p>Microstructure of the L-PBF-fabricated NAB samples after different post-printing heat treatment cycles, including (<b>a</b>,<b>b</b>) 600 °C for 1 hour, (<b>c</b>,<b>d</b>) 700 °C for 1 hour, (<b>e</b>,<b>f</b>) 800 °C for 1 h, (<b>g</b>,<b>h</b>) 900 °C for 1 h (Reprinted with permission from [<a href="#B165-jmmp-08-00054" class="html-bibr">165</a>]).</p>
Full article ">Figure 83
<p>(<b>a</b>) Stress–strain curves of the as-printed and heat-treated L-PBF NAB samples, and (<b>b</b>) a comparison with the mechanical properties of cast and wrought counterparts. (<b>c</b>) Mass loss measurements after seawater exposure for 3 and 6 months in the as-printed and heat-treated L-PBF NAB alloy compared with the cast and wrought counterparts (Reprinted with permission from [<a href="#B165-jmmp-08-00054" class="html-bibr">165</a>]).</p>
Full article ">Figure 84
<p>Microstructure of as-built and heat-treated L-PBF NAB alloys using different feedstocks, including (<b>a</b>,<b>b</b>) C63000 and (<b>c</b>,<b>d</b>) C95800. (<b>e</b>) Stress–strain curves of L-PBF-fabricated NAB alloys using two feedstocks of C63000 and C95800 in the as-built and heat-treated conditions, respectively, along with the cast and forged counterparts (Reprinted with permission from [<a href="#B163-jmmp-08-00054" class="html-bibr">163</a>]).</p>
Full article ">Figure 85
<p>PDP curves of the as-built and heat-treated L-PBF NAB alloys, using different feedstocks of (<b>a</b>,<b>b</b>) C63000 and (<b>c</b>,<b>d</b>) C95800 (Reprinted with permission from [<a href="#B163-jmmp-08-00054" class="html-bibr">163</a>]).</p>
Full article ">Figure 86
<p>(<b>a</b>) As-fabricated EBM NAB cylindrical parts with a diameter of 25 mm, (<b>b</b>) IPF map of the as-fabricated sample, (<b>c</b>) the corresponding grain boundary map, (<b>d</b>) SEM image showing uniform distribution of precipitates, (<b>e</b>) the IPF map taken from the white square selected areas showing the formation of precipitates on both intergranular and intragranular areas, and (<b>f</b>–<b>i</b>) the corresponding EDS elemental maps of Cu, Al, Ni, and Fe (Reprinted with permission from [<a href="#B166-jmmp-08-00054" class="html-bibr">166</a>]).</p>
Full article ">Figure 87
<p>(<b>a</b>–<b>c</b>) TEM images at different magnifications and the corresponding SAED patterns taken from the melt pool center of the L-DED NAB part; (<b>d</b>–<b>g</b>) the corresponding EDS elemental maps of Cu, Al, Fe, and Ni’ (<b>h</b>,<b>i</b>) TEM images and the corresponding SAED patterns of α and β* taken from the melt pool boundary; (<b>j</b>) HRTEM image taken from α; (<b>k</b>) HRTEM image taken from β*; and (<b>l</b>–<b>o</b>) EDS elemental maps taken from the inset in (<b>h</b>) (Reprinted with permission from [<a href="#B171-jmmp-08-00054" class="html-bibr">171</a>]).</p>
Full article ">Figure 88
<p>(<b>a</b>) Stress–strain curve of the L-DED NAB part fabricated with different process parameters (S1–S8) and (<b>b</b>) summary of the obtained mechanical properties. (<b>c</b>) A comparison between the mechanical properties of the L-DED NAB part and the counterparts fabricated by other manufacturing processes, including WAAM, L-PBF, and cast before and after heat treatment (Reprinted with permission from [<a href="#B171-jmmp-08-00054" class="html-bibr">171</a>]).</p>
Full article ">Figure 89
<p>(<b>a</b>) SEM image taken from the interface between WAAM NAB and the 316L SS substrate, showing the formation of cracks in the HAZ of the SS side, and (<b>b</b>) higher magnification SEM image, showing the penetration of liquid NAB into the intergranular regions of the SS side (Reprinted with permission from [<a href="#B160-jmmp-08-00054" class="html-bibr">160</a>]).</p>
Full article ">Figure 90
<p>(<b>a</b>) Interface of the WAAM-fabricated NAB/316L bimetal, and (<b>b</b>–<b>d</b>) the corresponding EDS elemental analysis (Reprinted with permission from [<a href="#B161-jmmp-08-00054" class="html-bibr">161</a>]).</p>
Full article ">Figure 91
<p>Microstructural features of (<b>a</b>,<b>b</b>) interfacial region of the L-DED-fabricated CuNi2SiCr/NAB bimetal part, (<b>c</b>) NAB substrate, (<b>d</b>) CuNi2SiCr-deposited layers, (<b>e</b>) HAZ region, and (<b>f</b>) diluted region (Reprinted with permission from [<a href="#B169-jmmp-08-00054" class="html-bibr">169</a>]).</p>
Full article ">Figure 92
<p>After-immersion surface morphology of the (<b>a</b>–<b>d</b>) NAB substrate and (<b>e</b>–<b>h</b>) deposited layers at different immersion times: (<b>a</b>,<b>e</b>) 1 day, (<b>b</b>,<b>f</b>) 5 days, (<b>c</b>,<b>g</b>) 14 days, and (<b>d</b>,<b>h</b>) 28 days (Reprinted with permission from [<a href="#B170-jmmp-08-00054" class="html-bibr">170</a>]).</p>
Full article ">Figure 93
<p>(<b>a</b>) Schematic illustration showing the L-DED fabrication process of NAB/15-5 PH bimetal samples; (<b>b</b>) a representative of the as-fabricated part showing the tensile sample preparation; (<b>c</b>) a prototype of a bimetal NAB/15-5 PH part; (<b>d</b>) low-magnification confocal image, covering the last layer of 15-5 PH side, interface, and the first layer of NAB side; (<b>e</b>–<b>g</b>) higher magnification images taken from zones 1, 2, and 3 of (<b>d</b>), respectively; and (<b>h</b>) EDS elemental line scan covering NAB side, interface, and 15-5 PH side (Reprinted with permission from [<a href="#B168-jmmp-08-00054" class="html-bibr">168</a>]).</p>
Full article ">Figure 94
<p>Schematic illustration of stress concentration at the tips of Fe<sub>x</sub>Al dendrites during tensile loading in (<b>a</b>) longitudinal and (<b>b</b>) transverse directions in the L-DED-fabricated NAB/15-5 PH bimetal part (Reprinted with permission from [<a href="#B168-jmmp-08-00054" class="html-bibr">168</a>]).</p>
Full article ">Figure 95
<p>Corrosion properties of the L-DED bimetal NAB/15-5 PH part: (<b>a</b>) PDP curves, and (<b>b</b>) Nyquist plots resulted from EIS testing. Surface profiles of (<b>c</b>) NAB and (<b>d</b>) 15-5 PH after 72 h of immersion. SEM images taken from the corroded surfaces of (<b>e</b>) NAB and (<b>f</b>) 15-5 PH after 72 h of immersion. (<b>g</b>) The depth of the corrosion pits in the NAB and 15-5 PH (Reprinted with permission from [<a href="#B168-jmmp-08-00054" class="html-bibr">168</a>]).</p>
Full article ">Figure 96
<p>(<b>a</b>) TiO<sub>2</sub>-TiC-coated diamond particles produced by the molten salt method, (<b>b</b>) Raman spectra of TiO<sub>2</sub>-TiC powder taken from the selected area of interest, (<b>c</b>) schematic illustration showing the L-DED process, and (<b>d</b>) SEM image of the copper/diamond powder mixture (Reprinted with permission from [<a href="#B175-jmmp-08-00054" class="html-bibr">175</a>]).</p>
Full article ">Figure 97
<p>(<b>a</b>–<b>c</b>) SEM images taken from the surface of L-DED-fabricated copper-diamond composites with different energy densities, (<b>d</b>) effect of process parameters on the quality of the printed parts, (<b>e</b>) effect of laser energy density on the density of the printed parts, (<b>f</b>) schematic illustration showing the process of particle ejection during the deposition process, and (<b>g</b>) effect of interphase on the thermal conductivity (TC) of copper-diamond composites when using no interphase (black bar), only TiC interphase (red bar), and TiO<sub>2</sub>-TiC interphase (green bar) (Reprinted with permission from [<a href="#B175-jmmp-08-00054" class="html-bibr">175</a>]).</p>
Full article ">Figure 98
<p>(<b>a</b>,<b>b</b>) SEM images of the L-DED-fabricated copper-diamond surface, (<b>c</b>) cross-sectional view of copper-(TiO<sub>2</sub>-TiC)-diamond, (<b>d</b>) copper/TiO<sub>2</sub> interface, (<b>e</b>) TiO<sub>2</sub>/TiC interface, and (<b>f</b>–<b>h</b>) HR-TEM micrographs of copper, TiO<sub>2</sub>, and TiC, respectively (Reprinted with permission from [<a href="#B175-jmmp-08-00054" class="html-bibr">175</a>]).</p>
Full article ">Figure 99
<p>SEM images taken from (<b>a</b>) the original diamond particle, (<b>b</b>) the TiO<sub>2</sub>-TiC-coated diamond particle before L-DED printing, and (<b>c</b>) after L-DED printing. (<b>d</b>) The corresponding Raman spectra from the powders at different states and (<b>e</b>) full width at half maximum (FWHM) and the diamond peak’ position in different states of the powders (Reprinted with permission from [<a href="#B175-jmmp-08-00054" class="html-bibr">175</a>]).</p>
Full article ">Figure 100
<p>(<b>a</b>) XRD results of a BJT-fabricated copper-diamond composite in the (a<sub>1</sub>) green state, (a<sub>2</sub>) after sintering at 800 °C, and (a<sub>3</sub>) after sintering at 900 °C, along with the (<b>b</b>) relative density of the samples fabricated with different volume fractions of diamond and different sintering temperatures (Reprinted with permission from [<a href="#B182-jmmp-08-00054" class="html-bibr">182</a>]).</p>
Full article ">Figure 101
<p>(<b>a</b>) An schematic illustration showing the effect of sintering temperature on the BJT-fabricated copper-diamond composite sample, along with the fracture surfaces of the samples sintered at (<b>b</b>) 800 °C and (<b>c</b>) 900 °C (Reprinted with permission from [<a href="#B182-jmmp-08-00054" class="html-bibr">182</a>]).</p>
Full article ">Figure 102
<p>SEM images taken from (<b>a</b>) mixed composite powder before the L-PBF process and (<b>b</b>) surface of the L-PBF-fabricated Cu-GO composite specimen, along with the (<b>c</b>) stress–strain curves of as-printed samples in vertical and horizontal directions (Reprinted with permission from [<a href="#B23-jmmp-08-00054" class="html-bibr">23</a>]).</p>
Full article ">Figure 103
<p>(<b>a</b>,<b>b</b>) Unpolished top view of the L-PBF-fabricated copper-carbon composite, (<b>c</b>,<b>d</b>) the corresponding polished (unetched) samples, and (<b>e</b>,<b>f</b>) the corresponding etched samples (Reprinted with permission from [<a href="#B177-jmmp-08-00054" class="html-bibr">177</a>]).</p>
Full article ">Figure 104
<p>(<b>a</b>,<b>b</b>) Virgin CuCr0.3 alloy powder, (<b>c</b>,<b>d</b>) mixed CuCr0.3 powder and carbon nano-particles, along with the SEM images taken from the top view of the L-PBF-fabricated (<b>e</b>) CuCr0.3 alloy, and (<b>f</b>) carbon-mixed CuCr0.3 composite used for L-PBF fabrication of copper-carbon composite (Reprinted with permission from [<a href="#B63-jmmp-08-00054" class="html-bibr">63</a>]).</p>
Full article ">Figure 105
<p>SEM image taken from the powder mixture used for the L-DED fabrication of the copper-ZrB<sub>2</sub> in-situ composite (Reprinted with permission from [<a href="#B178-jmmp-08-00054" class="html-bibr">178</a>]).</p>
Full article ">Figure 106
<p>(<b>a</b>) Microstructure and elemental distribution maps of Zr, Cu, and Ni taken from the L-DED-fabricated copper-ZrB<sub>2</sub> in-situ composite and (<b>b</b>) the corresponding XRD results (Reprinted with permission from [<a href="#B178-jmmp-08-00054" class="html-bibr">178</a>]).</p>
Full article ">Figure 107
<p>(<b>a</b>) XRD analysis and (<b>b</b>) SEM images taken from the SLS processed copper-ceramic composite using ZrB<sub>2</sub> reinforcing particles (Reprinted with permission from [<a href="#B179-jmmp-08-00054" class="html-bibr">179</a>]).</p>
Full article ">Figure 108
<p>(<b>a</b>) An overview of the ODS-Cu powder used for SEBM-fabrication of copper-alumina composite, (<b>b</b>) a low-magnification cross-sectional view, and (<b>c</b>) a high-magnification SEM image showing the uniform dispersion of Al<sub>2</sub>O<sub>3</sub> with an approximate size of 35 nm (Reprinted with permission from [<a href="#B180-jmmp-08-00054" class="html-bibr">180</a>]).</p>
Full article ">Figure 109
<p>Longitudinal cross-sectional overview of SEBM-fabricated copper-alumina composite showing a porous structure in (<b>a</b>–<b>c</b>) all different sets of process parameters, along with (<b>d</b>–<b>f</b>) higher magnification SEM images showing the occurrence of phase separation in the microstructure of the as-printed specimens, that is, region (1) consists of pure copper, region (2) reveals copper/alumina structure, and region (3) contains alumina (Reprinted with permission from [<a href="#B180-jmmp-08-00054" class="html-bibr">180</a>]).</p>
Full article ">Figure 110
<p>Different feedstock powders used for SLS fabrication of Cu-tin alloy, including (<b>a</b>) virgin Cu powders, (<b>b</b>) mechanically mixed Cu and Sn powders, and (<b>c</b>,<b>d</b>) cross-section and surface of composite Cu-Sn powders, respectively (Reprinted with permission from [<a href="#B181-jmmp-08-00054" class="html-bibr">181</a>]).</p>
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<p>SEM images at different magnifications taken from the SLS-fabricated Cu-based sample using (<b>a</b>,<b>b</b>) mechanically mixed Cu and Sn powders, (<b>c</b>,<b>d</b>) composite Cu-Sn powders, along with (<b>e</b>,<b>f</b>) a detailed microstructural feature showing the necking between two Cu particles in the presence of a Sn-rich interparticle layer (Reprinted with permission from [<a href="#B181-jmmp-08-00054" class="html-bibr">181</a>]).</p>
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18 pages, 5728 KiB  
Article
Simultaneous Two- and Three-Photon Deep Imaging of Autofluorescence in Bacterial Communities
by Alma Fernández, Anton Classen, Nityakalyani Josyula, James T. Florence, Alexei V. Sokolov, Marlan O. Scully, Paul Straight and Aart J. Verhoef
Sensors 2024, 24(2), 667; https://doi.org/10.3390/s24020667 - 20 Jan 2024
Cited by 2 | Viewed by 2072
Abstract
The intrinsic fluorescence of bacterial samples has a proven potential for label-free bacterial characterization, monitoring bacterial metabolic functions, and as a mechanism for tracking the transport of relevant components through vesicles. The reduced scattering and axial confinement of the excitation offered by multiphoton [...] Read more.
The intrinsic fluorescence of bacterial samples has a proven potential for label-free bacterial characterization, monitoring bacterial metabolic functions, and as a mechanism for tracking the transport of relevant components through vesicles. The reduced scattering and axial confinement of the excitation offered by multiphoton imaging can be used to overcome some of the limitations of single-photon excitation (e.g., scattering and out-of-plane photobleaching) to the imaging of bacterial communities. In this work, we demonstrate in vivo multi-photon microscopy imaging of Streptomyces bacterial communities, based on the excitation of blue endogenous fluorophores, using an ultrafast Yb-fiber laser amplifier. Its parameters, such as the pulse energy, duration, wavelength, and repetition rate, enable in vivo multicolor imaging with a single source through the simultaneous two- and three-photon excitation of different fluorophores. Three-photon excitation at 1040 nm allows fluorophores with blue and green emission spectra to be addressed (and their corresponding ultraviolet and blue single-photon excitation wavelengths, respectively), and two-photon excitation at the same wavelength allows fluorophores with yellow, orange, or red emission spectra to be addressed (and their corresponding green, yellow, and orange single-photon excitation wavelengths). We demonstrate that three-photon excitation allows imaging over a depth range of more than 6 effective attenuation lengths to take place, corresponding to an 800 micrometer depth of imaging, in samples with a high density of fluorescent structures. Full article
(This article belongs to the Special Issue Recent Advances in Biophotonics Sensors)
Show Figures

Figure 1

Figure 1
<p>Example excitation spectra and emission spectra for fluorophores in a multicolor, multiphoton imaging experiment. On the x-axes, we show (from top to bottom) the wavelength corresponding to single-photon excitation and emission, 2-photon excitation, and 3-photon excitation, respectively.</p>
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<p>(<b>a</b>) Brightfield and (<b>b</b>) widefield epifluorescence images (composite of 405/440 (blue), 488/520 (green), and 560/605 (red) (excitation/emission filter central wavelength)) of a thin <span class="html-italic">S. aizunensis</span> sample (~3 µL of sample sandwiched between a microscope slide and cover slip), showing the filaments formed in the cultures. The strong scattering from this sample causes a significant blur, even when the focal plane is directly below the cover slip. Scale bars: 100 µm.</p>
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<p>Schematic of our laser and microscope system. The repetition rate of the laser was controlled by choosing an appropriate divisor to the oscillator pulse train with the timing electronics. The detection electronics’ sampling rate was set with the oscillator pulse train, and then synchronized to the amplifier output pulses.</p>
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<p>Characterization of the output beam from our femtosecond fiber laser. The pulses were characterized using second-harmonic frequency-resolved optical gating (<b>a</b>,<b>b</b>), showing a pulse duration of 180 fs with minimal satellite pulses. (<b>c</b>) The far-field beam profile, measured with a beam profiler camera. The profile is nearly perfectly Gaussian, owing to only the fundamental mode being launched in the large-mode area final amplifier stage.</p>
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<p>Three-dimensional measurement of the 2P and 3P PSF. (<b>a</b>,<b>b</b>) Projections of the 3D measurement along the <span class="html-italic">z</span>-axis of the orange (2P) and blue (3P) fluorescence, respectively, from a 500 nm bead. (<b>d</b>,<b>e</b>) Projections along the <span class="html-italic">y</span>-axis of the orange and blue fluorescence, respectively, of the same 500 nm bead, to visualize the <span class="html-italic">z</span>-profiles of the PSFs. (<b>c</b>) Linear lateral cross-sections of the 2P and 3P PSFs. The solid lines represent the <span class="html-italic">x</span> cross-sections and the dashed lines show the <span class="html-italic">y</span> cross-sections of the 3P (blue) and 2P (red) PSFs. The magenta and cyan lines show the lateral cross-sections of the calculated 2P and 3P PSFs, convoluted with a 500 nm sphere, respectively. (<b>f</b>) Linear axial cross-sections of the measured 2P (red line) and 3P (blue line) PSFs. The magenta and cyan lines show the axial cross-section of the calculated 2P and 3P PSF convoluted with a 500 nm sphere, respectively.</p>
Full article ">Figure 6
<p>Simulated signal-to-background ratio vs. scattering length and imaging depth for (<b>a</b>) 2P excited fluorescence and (<b>b</b>) 3P fluorescence. Contour lines (iso-values for signal-to-background ratio) and color coding are the same for both panels. Contour lines are labeled where possible. Beyond a signal-to-background ratio of 1:20, contour lines are drawn at 1:50 and 1:100. Obviously, those last contours represent situations where image quality is so gravely compromised that imaging is practically impossible.</p>
Full article ">Figure 7
<p>Characterization of the nonlinearity of the fluorescence in different detection spectral windows. Panel (<b>a</b>) shows a composite image (76 µm × 76 µm) of the measurements in all 3 detection channels at the highest laser power shown in panel (<b>b</b>). Scale bars: 10 µm. A region where the no sample movement was detected between all measurements was chosen to extract the signal vs. background. Panel (<b>b</b>) shows the power dependence of the fluorescence signal in the red (570–640 nm), green (490–560 nm), and blue (400–480 nm) detection channels.</p>
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<p>Measurement of 2P and 3P fluorescence vs. depth (76 µm × 76 µm × 570 µm) in a Streptomyces sample. (<b>a</b>) Red (570–640 nm), green (490–560 nm), and blue (400–480 nm) fluorescence channels (top row—<span class="html-italic">xy</span> slice 90 µm below top surface; middle row—central <span class="html-italic">xz</span> cut; bottom row—<span class="html-italic">xy</span> slice 390 µm below top surface; horizontal (<span class="html-italic">xy</span>) scale bar: 10 µm; vertical (<span class="html-italic">z</span>) scale bar: 30 µm). (<b>b</b>) Signal minus background vs. depth normalized to maximum value (solid dots and solid lines) and, accordingly, scaled background vs. depth (dashed lines) for the red, green, and blue channels. (<b>c</b>) Signal-to-background ratio vs. depth for the red, green, and blue detection channels.</p>
Full article ">Figure 9
<p>Measurement of 2P and 3P fluorescence vs. depth (76 µm × 76 µm × 270 µm) in a dense <span class="html-italic">Streptomyces</span> bacterial community sample. (<b>a</b>) Red (570–640 nm), green (490–560 nm), and blue (400–480 nm) fluorescence channels (Top row—<span class="html-italic">xy</span> slice 10 µm below top surface. Middle row—<span class="html-italic">xz</span> slide 160 µm below top surface. Bottom row—<span class="html-italic">xy</span> slice 270 µm below top surface. Scale bar: 10 µm.). (<b>b</b>) Center <span class="html-italic">xz</span> cut; scale bar: 10 µm.</p>
Full article ">Figure 10
<p>(<b>a</b>) Signal minus background vs. depth corresponding to the stack shown in <a href="#sensors-24-00667-f007" class="html-fig">Figure 7</a>, normalized to maximum value (close to 150 µm depth; solid dots and lines) and, accordingly, scaled background vs. depth (dashed lines) for the red, green, and blue channels. (<b>b</b>) Signal-to-background ratio vs. depth for the red, green, and blue detection channels.</p>
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<p>Images (76 µm × 76 µm) obtained at 780 µm below the sample surface in a medium-dense sample (with 120 µm effective attenuation length), i.e., at 6.5 scattering lengths below the surface; (<b>a</b>) 3P excited fluorescence signal detected in the 400–480 nm spectral window; (<b>b</b>) 2P excited fluorescence signal detected in the 570–640 nm spectral window. <span class="html-italic">Streptomyces</span> filaments are clearly recognized in the 3P image but cannot be resolved in the 2P image due to the overwhelming background. Scale bars: 10 µm.</p>
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11 pages, 2597 KiB  
Article
Multiwavelength Fluorescence and Diffuse Reflectance Spectroscopy for an In Situ Analysis of Kidney Stones
by Polina S. Tseregorodtseva, Gleb S. Budylin, Nadezhda V. Zlobina, Zare A. Gevorkyan, Daria A. Filatova, Daria A. Tsigura, Artashes G. Armaganov, Andrey A. Strigunov, Olga Y. Nesterova, David M. Kamalov, Elizaveta V. Afanasyevskaya, Elena A. Mershina, Nikolay I. Sorokin, Valentin E. Sinitsyn, Armais A. Kamalov and Evgeny A. Shirshin
Photonics 2023, 10(12), 1353; https://doi.org/10.3390/photonics10121353 - 8 Dec 2023
Cited by 1 | Viewed by 1950
Abstract
This study explores the use of diffuse reflectance spectroscopy (DRS) and multiwavelength fluorescence spectroscopy for real-time kidney stone identification during laser lithotripsy. Traditional methods are not suitable for in situ analysis, so the research focuses on optical techniques that can be integrated with [...] Read more.
This study explores the use of diffuse reflectance spectroscopy (DRS) and multiwavelength fluorescence spectroscopy for real-time kidney stone identification during laser lithotripsy. Traditional methods are not suitable for in situ analysis, so the research focuses on optical techniques that can be integrated with lithotripsy fibers. Experiments were conducted ex vivo, using DRS and multiwavelength fluorescence spectroscopy (emission–excitation matrix (EEM)) to distinguish between 48 urinary stones of three types: urate, oxalate and hydroxyapatite, with infrared spectroscopy as a reference. A classification model was developed based on EEM and DRS data. Initial classification relying solely on EEM data achieved an f1-score of 87%, which increased to 92% when DRS data were included. The findings suggest that optical spectroscopy can effectively determine stone composition during laser lithotripsy, potentially enhancing surgical outcomes via the real-time automatic optimization of laser radiation parameters. Full article
(This article belongs to the Special Issue Optical Spectroscopy and Applications)
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Figure 1

Figure 1
<p>(<b>A</b>) Experimental setup for measuring the fluorescence excitation–emission matrices of calculi; (<b>B</b>) experimental setup for recording the diffuse light reflection spectra of calculi.</p>
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<p>FTIR spectra for different types of stones. The dotted lines represent the band characteristics of each type (chemical composition) of calculus.</p>
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<p>(<b>A</b>–<b>C</b>) The normalized average fluorescence emission spectra for the three types of stones at excitation wavelengths of 340, 380 and 420 nm, respectively. The translucent areas depict the magnitude of the standard deviation. (<b>D</b>–<b>F</b>) The characteristic EEMs of the three types of stones.</p>
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<p>(<b>A</b>) The normalized fluorescence spectrum of averaged over five measurement points from a single calculi. (<b>B</b>) The normalized fluorescence spectrum of all the calculi. The translucent areas depict the magnitude of the standard deviation. The excitation wavelength was 380 nm.</p>
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<p>(<b>A</b>) Average optical density (OD) spectra of three types of stones with OD subtracted at 600 nm. Translucent areas indicate the magnitude of the standard deviation. (<b>B</b>) Box plots of the slope of the OD spectra for the three types of stones. The rhombus depicts the outlying OD spectrum detected from one of the oxalate stones. (<b>C</b>) Characteristic appearance of a urate calculus, oxalates and hydroxyapatites from top to bottom, respectively.</p>
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<p>The confusion matrix (<b>A</b>) of the train subset for the classifier using EEM data (<b>B</b>) of the test subset for the classifier also using solely EEM data; (<b>C</b>) of the train subset for the classifier that uses both EEM and DRS data; and (<b>D</b>) of the test subset for a classifier that uses both EEM and DRS data.</p>
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23 pages, 6863 KiB  
Review
Advances in Ultrafast Fiber Lasers for Multiphoton Microscopy in Neuroscience
by Thulasi Srinivasan and Murat Yildirim
Photonics 2023, 10(12), 1307; https://doi.org/10.3390/photonics10121307 - 26 Nov 2023
Cited by 5 | Viewed by 4061
Abstract
Multiphoton microscopy (MPM) has emerged as a vital tool in neuroscience, enabling deeper imaging with a broader field of view, as well as faster and sub-cellular resolution. Recent innovations in ultrafast fiber laser technology have revolutionized MPM applications in living brains, offering advantages [...] Read more.
Multiphoton microscopy (MPM) has emerged as a vital tool in neuroscience, enabling deeper imaging with a broader field of view, as well as faster and sub-cellular resolution. Recent innovations in ultrafast fiber laser technology have revolutionized MPM applications in living brains, offering advantages like cost-effectiveness and user-friendliness. In this review, we explore the progress in ultrafast fiber laser technology, focusing on its integration into MPM for neuroscience research. We also examine the utility of femtosecond fiber lasers in fluorescence and label-free two- and three-photon microscopy applications within the field. Furthermore, we delve into future possibilities, including next-generation fiber laser designs, novel laser characteristics, and their potential for achieving high spatial and temporal resolution imaging. We also discuss the integration of fiber lasers with implanted microscopes, opening doors for clinical and fundamental neuroscience investigations. Full article
(This article belongs to the Special Issue Recent Advances in Multiphoton Microscopy)
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<p>Fundamentals and types of multiphoton microscopy (MPM). (<b>a</b>) A femtosecond laser generates ultrashort pulses, which are sent to galvanometric (xy) scanning mirrors to scan the beam on the back aperture of the objective with the help of scan and tube lenses. The dichroic mirror helps to transmit the excitation wavelength and reflects the emitted light from the mouse brain. Since the beam fills most of the back aperture of the objective lens, the beam is focused to a micrometer level beam size on the focal plane of the objective. The emitted light is directed to the highly sensitive photon multiplier tubes (PMTs) by using two dichroic mirrors and two band-pass filters depending on the type of MPM. (<b>b</b>) Energy-level diagrams of different kinds of MPMs, such as 2PEF, SHG, 3PEF, and THG. <math display="inline"><semantics> <mrow> <mi>h</mi> <mi>ω</mi> </mrow> </semantics></math> is the excitation photon energy, <math display="inline"><semantics> <mi>λ</mi> </semantics></math> denotes wavelength.</p>
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<p>The recent developments in the field of ultra-fast fiber lasers. (<b>a</b>) Ring laser cavity design. Insets: Longitudinal modes in a simple laser cavity: gain medium of the laser, cavity longitudinal modes are equally spaced by <math display="inline"><semantics> <mfrac> <mi>c</mi> <mrow> <mn>2</mn> <mi>L</mi> </mrow> </mfrac> </semantics></math>, the modes whose corresponding frequencies fall within the gain bandwidth of the laser will be amplified and lased out. (<b>b</b>) Pulse shaping regimes of the mode-locked fiber lasers. (<b>c</b>) Different categories of saturable absorbers: Optical phenomena-based, and material-based. (<b>d</b>) Tunable repetition rate and wavelength source for MPM imaging.</p>
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<p>Various configurations of ultrafast lasers. (<b>a</b>) Schematic representation of the mode-locked Yb-doped fiber laser ring cavity. The total cavity length is 4.8 m. A polarizing beam splitter (PBS) is used to split the fast and slow axis light and helps to measure the pulsed output. Half-wave and quarter-wave plates are used to varying the polarization state of the light which helps to obtain the phase and mode-locking. The use of the birefringent filter plate (BRF) allows for control of the spectral bandwidth in the cavity. Col.1 and Col.2 indicate the collimators [<a href="#B26-photonics-10-01307" class="html-bibr">26</a>]. (<b>b</b>) Experimental configuration of circularly polarized solitons generation: QWP, quarter-wave plate; L, lens; LPF, long-pass filter [<a href="#B50-photonics-10-01307" class="html-bibr">50</a>]. (<b>c</b>) Experimental view of Cr:F laser setup. FC: fiber collimator; PL: pump lens; CM: Concave mirror; DCM: double-chirped mirror; PL: pump lens; OC: output coupler; BD: beam dump [<a href="#B51-photonics-10-01307" class="html-bibr">51</a>]. (<b>d</b>) Schematic of the 1.8 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m femtosecond fiber laser system, Stage 1: Er-doped amplifier, Stage 2: Tm:ZBLAN pre-amplifier and power amplifier [<a href="#B16-photonics-10-01307" class="html-bibr">16</a>].</p>
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<p>Different configurations of fiber amplifiers. (<b>a</b>) System diagram for a basic CPA system (<b>b</b>) different building blocks of the MOPA system, (<b>c</b>) schematic representation of GMNA.</p>
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<p>All−fiber mode−locked oscillator output characteristics. (<b>a</b>) Wavelength spectrum of the laser. (<b>b</b>) Mode−locked laser pulse train. (<b>c</b>) Measured RF spectrum repetition rate centered at 21.35 MHz. (<b>d</b>) Oscillator output before and after compression. Adapted from [<a href="#B52-photonics-10-01307" class="html-bibr">52</a>].</p>
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<p>Characteristics of different stage amplifier output. (<b>a</b>) Optical spectrum of pre−amplifier. (<b>b</b>) Optical spectrum of the power−amplifier. (<b>c</b>) The power amplifier ASE spectrum. (<b>d</b>) The relationship between input and output power. Adapted from [<a href="#B52-photonics-10-01307" class="html-bibr">52</a>].</p>
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<p>Two-photon functional mouse brain imaging with fiber lasers. (<b>a</b>) Dual color neuronal (jRGECO1a) and axonal (jYCaMP1s) imaging at 1040 nm wavelength with 31.25 MHz repetition rate. (<b>Top left</b>) The average image of both colors, (<b>top right</b>) pixel-wise covariance of response amplitudes in each color. (<b>Bottom</b>) jYCaMP (yellow) and jRGECO (red) recordings from the button site. Gray lines represent the visual stimulus onsets. Adapted from [<a href="#B27-photonics-10-01307" class="html-bibr">27</a>]. (<b>b</b>) Comparison of spontaneous activity of neurons at a 680 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m depth with or without AES by two-photon microscopy. (<b>Top left</b>) Structural image of neurons without AES. (<b>Top right</b>) structural image of neurons with AES. (<b>Bottom left</b>) Spontaneous activity traces acquired without AES. (<b>Bottom right</b>) Spontaneous activity traces acquired with AES. Adapted from [<a href="#B59-photonics-10-01307" class="html-bibr">59</a>].</p>
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<p>Two-photon fluorescence structural mouse brain imaging with fiber lasers. (<b>a</b>) Dual color neuronal (green, YFP mice) and microvasculature (red, Texas Red dye) imaging at 1060 nm wavelength with 40 MHz repetition rate up to a 750 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m depth. (<b>left</b>) Microvasculature imaging with Texas-red dye, (<b>right</b>) neuronal imaging with YFP transgenic mice. Adapted from [<a href="#B26-photonics-10-01307" class="html-bibr">26</a>]. (<b>b</b>) Neuronal and brain vasculature imaging by exciting the mouse brain with a Yb amplifier-based fiber laser and a Raman laser simultaneously. (<b>Top</b>) Maximum intensity projections ranging from the surface to a 750 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m depth for neurons (<b>left</b>, tdTomato, 1060 nm excitation), vasculature (<b>right</b>, Alexafluor 647, 1250 nm excitation), and overlaid to each other (<b>middle</b>). (<b>Bottom</b>) Side view for the same stacks from neurons (<b>left</b>), vasculature (<b>right</b>), and overlaid to each other (<b>middle</b>) Adapted from [<a href="#B60-photonics-10-01307" class="html-bibr">60</a>]. (<b>c</b>) (<b>Left</b>) 3D reconstruction of 2-photon fluorescence image stack of mouse brain vasculature labeled with ICG (red), and third-harmonic generation images of myelinated axons (green) delineating the white matter. (<b>Right</b>) Representative 2D two-photon fluorescence images at the depth from the brain surface, as indicated. Adapted from [<a href="#B50-photonics-10-01307" class="html-bibr">50</a>].</p>
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<p>Three-photon fluorescence functional mouse and Drosophila brain imaging with fiber lasers. (<b>a</b>) Video-rate imaging of neural activity in Kenyon cells labeled with GCaMP7f during electric shocks. The blue and orange lines show single Kenyon cell activity under rest and electric shock, respectively. Red shade areas represent the periods of electric shocks. Inset: a single Kenyon cell. Scale bar is 80 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m. Adapted from [<a href="#B51-photonics-10-01307" class="html-bibr">51</a>]. (<b>b</b>) (<b>Top</b>) Structural images of neurons without AES (<b>left</b>), and with AES (<b>right</b>). (<b>Bottom</b>) Spontaneous activity of neurons without AES (<b>left</b>), and with AES (<b>right</b>). With AES, the spontaneous traces have higher SNR than those without AES. Reproduced with permission from [<a href="#B59-photonics-10-01307" class="html-bibr">59</a>].</p>
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<p>Examples of three-photon structural brain imaging. (<b>a</b>) Schematic illustration of in vivo imaging of neurons expressing TurboFP635. TurboFP635 was expressed in cortical neurons of a mouse (C57BL/6N) and was excited by 3-photon excitation at 1.8 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m (<b>left</b>), 3D reconstruction of 700 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m z-stack (<b>right</b>). Reproduced with permission from Ref. [<a href="#B16-photonics-10-01307" class="html-bibr">16</a>]. (<b>b</b>) Comparison of 3P and 2P excitation for imaging mouse brain tissue (<b>left</b>); 3PEF (<b>top</b>) and 2PEF (<b>bottom</b>) imaging of a tdTomato-labeled fixed mouse brain cortex at depths of 200 and 600 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m. (<b>right</b>) Dual-color 3PEF imaging for several combinations of green–red fluorescent proteins in HEK cells (<b>top</b>) and mouse brain tissue at a depth of 500 <math display="inline"><semantics> <mi mathvariant="sans-serif">μ</mi> </semantics></math>m (<b>bottom</b>). Reproduced with permission from Ref. [<a href="#B49-photonics-10-01307" class="html-bibr">49</a>].</p>
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<p>Simultaneous three-photon fluorescence (3PEF) and third-harmonic generation (THG) imaging of fixed Rainbow-3 mouse brain cortex and brain stem. (<b>a</b>–<b>c</b>) Simultaneous THG (<b>a</b>) and 3PEF (<b>b</b>) imaging of a fixed mouse brain cortex. (<b>c</b>) In the cortex, THG imaging provides contrast similar to that of brain vasculature, as confirmed by overlaying the 3PEF signal acquired through tdTomato. (<b>d</b>–<b>f</b>) Simultaneous THG (<b>d</b>) and 3PEF (<b>e</b>) imaging of a fixed mouse brain stem; (<b>f</b>) 3PEF highlights the brain vasculature and THG highlights myelinated axons and cell bodies so that the overlapping of these two signals is minimal. Reproduced with permission from [<a href="#B63-photonics-10-01307" class="html-bibr">63</a>].</p>
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<p>Several fiber laser advancement prospects as well as potential future innovations.</p>
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22 pages, 8382 KiB  
Review
Research Progress in Tunable Fiber Lasers Based on Multimode Interference Filters
by Liqiang Zhang, Kexin Zhu, Yicun Yao, Xiuying Tian, Hailong Xu and Zhaogang Nie
Micromachines 2023, 14(11), 2026; https://doi.org/10.3390/mi14112026 - 30 Oct 2023
Viewed by 1782
Abstract
Tunable fiber lasers have the advantages of good beam quality, high integration, and adjustable output wavelength, and they are widely used in fields such as optical fiber communication and optical fiber sensing. The fiber filter is one of the key components of tunable [...] Read more.
Tunable fiber lasers have the advantages of good beam quality, high integration, and adjustable output wavelength, and they are widely used in fields such as optical fiber communication and optical fiber sensing. The fiber filter is one of the key components of tunable fiber lasers. Among the various filters currently used, multimode interference filters have the advantages of simple structure, convenient implementation, flexible tuning methods, and convenient spectral range design. The structures of multimode interference filters based on multimode fibers, no-core fibers, multi-core fibers, tapered fibers, and other special fibers are introduced in this paper. The working principles and tuning methods are analyzed and the research progress of tunable fiber lasers based on these filters is summarized. Finally, the development trend of tunable fiber lasers based on multimode interference filters is discussed. The rapid development and applications of multimode interference filters can help improve the performance of continuous and pulse lasers as well as promote the practicality of tunable fiber lasers. Full article
(This article belongs to the Special Issue High Power Fiber Laser Technology)
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<p>Structure of SMF-MMF-SMF filter [<a href="#B8-micromachines-14-02026" class="html-bibr">8</a>].</p>
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<p>(<b>a</b>) Tunable Yb-doped fiber laser based on SMF-MMF-SMF filter; (<b>b</b>) Tunable results of the dissipative soliton fiber laser [<a href="#B10-micromachines-14-02026" class="html-bibr">10</a>].</p>
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<p>(<b>a</b>) Tuning principle of SMF-MMF-SMF filter by bending; (<b>b</b>) Experimental setup diagram of the tunable fiber laser; (<b>c</b>) Output spectra of the interval-adjustable dual-wavelength fiber laser; (<b>d</b>) Output spectra of the tunable single-wavelength fiber laser [<a href="#B20-micromachines-14-02026" class="html-bibr">20</a>].</p>
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<p>(<b>a</b>) Experimental setup diagram of the tunable mode-locked fiber laser; (<b>b</b>) Output spectra of the tunable mode-locked fiber laser [<a href="#B24-micromachines-14-02026" class="html-bibr">24</a>].</p>
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<p>(<b>a</b>) Experimental setup diagram of the Tm-doped fiber laser; (<b>b</b>) Measured spectra of the single-wavelength laser by adjusting the PC and rotating the MMF [<a href="#B26-micromachines-14-02026" class="html-bibr">26</a>].</p>
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<p>Structure of the SMF-NCF-SMF filter [<a href="#B29-micromachines-14-02026" class="html-bibr">29</a>].</p>
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<p>(<b>a</b>) Structure of the tunable SMF-NCF-SMF filter; (<b>b</b>) Experimental setup diagram of the tunable Tm-doped fiber laser; (<b>c</b>) Tuning results of the Tm-doped fiber laser [<a href="#B31-micromachines-14-02026" class="html-bibr">31</a>].</p>
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<p>(<b>a</b>) Structure of the SMF-NCF-SMF filter based on index-matching liquid; (<b>b</b>) Experimental setup diagram of the tunable erbium-doped fiber laser; (<b>c</b>) Tuning results [<a href="#B32-micromachines-14-02026" class="html-bibr">32</a>].</p>
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<p>(<b>a</b>) Cross-section of the two-core fiber [<a href="#B33-micromachines-14-02026" class="html-bibr">33</a>]; (<b>b</b>) The structure of the interference filter based on two-core fiber [<a href="#B33-micromachines-14-02026" class="html-bibr">33</a>]; (<b>c</b>) Structure of the interference filter based on tapered seven-core fiber [<a href="#B35-micromachines-14-02026" class="html-bibr">35</a>].</p>
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<p>(<b>a</b>) The field distribution and normalized power in a tapered seven-core fiber simulated by Rsoft software; (<b>b</b>) Transmission spectra of tapered seven-core fiber simulated by Rsoft software [<a href="#B35-micromachines-14-02026" class="html-bibr">35</a>].</p>
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<p>(<b>a</b>) Cross-section of the seven-core fiber; (<b>b</b>) Working principle of the interference filter based on seven-core fiber [<a href="#B39-micromachines-14-02026" class="html-bibr">39</a>].</p>
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<p>(<b>a</b>) Experimental setup diagram of the tunable erbium-doped fiber laser based on tapered seven-core fiber filter; (<b>b</b>) Spectra of the tunable fiber laser [<a href="#B35-micromachines-14-02026" class="html-bibr">35</a>].</p>
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<p>Power transfer number versus FSR measured (blue circles) and simulated (red stars) at λ<sub>0</sub> = 1.55 μm for tapers assuming different elongations. Inset shows an experimental example of normalized transfer power versus taper elongation [<a href="#B42-micromachines-14-02026" class="html-bibr">42</a>].</p>
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<p>(<b>a</b>) Schematic diagram of the tapered fiber filter; (<b>b</b>) Tunable fiber laser based on tapered fiber filter; (<b>c</b>) Tuning results of the fiber laser [<a href="#B44-micromachines-14-02026" class="html-bibr">44</a>].</p>
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<p>Schematic diagram of the double-cone MZI filter [<a href="#B50-micromachines-14-02026" class="html-bibr">50</a>].</p>
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<p>(<b>a</b>) Experimental setup diagram of the tunable fiber laser based on a double-cone MZI filter; (<b>b</b>) Tuning results after annealing [<a href="#B50-micromachines-14-02026" class="html-bibr">50</a>].</p>
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<p>(<b>a</b>) The cross-section of the FLCSCF; (<b>b</b>) Schematic diagram of the FLCSCF filter; (<b>c</b>) Experimental setup of the fiber laser based on FLCSCF filter; (<b>d</b>) Tunable single-wavelength lasing output [<a href="#B59-micromachines-14-02026" class="html-bibr">59</a>].</p>
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<p>Diagram of two cascaded up-taper joints structure [<a href="#B60-micromachines-14-02026" class="html-bibr">60</a>].</p>
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<p>(<b>a</b>) The cross-section of the PCF; (<b>b</b>) Schematic diagram of the SMF-PCF-SMF filter [<a href="#B55-micromachines-14-02026" class="html-bibr">55</a>]; (<b>c</b>) Experimental setup of the tunable fiber laser; (<b>d</b>) Tuning results of the single-wavelength output spectrum [<a href="#B63-micromachines-14-02026" class="html-bibr">63</a>].</p>
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<p>(<b>a</b>) Schematic diagram of the core-offset structure filter; (<b>b</b>) Experimental setup of the tunable fiber laser; (<b>c</b>) Spectral response against temperature [<a href="#B62-micromachines-14-02026" class="html-bibr">62</a>].</p>
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<p>(<b>a</b>) Experimental setup diagram of the tunable mode-locked fiber laser based on tapered seven-core fiber filter; (<b>b</b>) Spectra of the tunable dissipative soliton fiber laser; (<b>c</b>) Spectra of the tunable amplifier similariton fiber laser [<a href="#B41-micromachines-14-02026" class="html-bibr">41</a>].</p>
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21 pages, 5732 KiB  
Article
A Distance-Weighted Dynamic Bandwidth Allocation Algorithm for Improved Performance in Long-Reach Passive Optical Networks for Next Generation Networks
by Adebanjo Haastrup, Mohammad Zehri, David Rincón, José Ramón Piney and Ali Bazzi
Photonics 2023, 10(8), 923; https://doi.org/10.3390/photonics10080923 - 11 Aug 2023
Cited by 2 | Viewed by 1705
Abstract
In recent years, there has been an increasing trend towards extending the coverage of passive optical networks (PONs) over large geographical areas. Long-reach PONs (LRPONs) are capable of extending the distance covered by PONs from 20 km to 100 km, leading to cost [...] Read more.
In recent years, there has been an increasing trend towards extending the coverage of passive optical networks (PONs) over large geographical areas. Long-reach PONs (LRPONs) are capable of extending the distance covered by PONs from 20 km to 100 km, leading to cost savings in the network operation by reducing the number of central offices. They have become widely deployed due to their ability to provide high-speed, long-distance data transmission over optical fibers. In addition, the next generation of optical access networks are expected to provide high-capacity mobile and wireless backhauling over a wide coverage area. However, this extended reach also requires the design of efficient dynamic bandwidth allocation (DBA) schemes to address the performance degradation caused by the increased propagation delay in LRPONs. The DBA schemes commonly used for upstream traffic transmission in traditional PONs are not well-suited for use in LRPONs due to their inefficiency in bandwidth utilization due to the increased round-trip time (RTT) between the optical line terminal (OLT) and the optical network unit (ONU). In this study, we present an efficient DBA algorithm, the Distance-Weighted Bandwidth Allocation DWDBA Algorithm, specifically enhanced for multi-wavelength LRPONs. Our DBA algorithm utilizes a scheduling policy that assigns weight vectors to Optical Network Units (ONUs) based on their distance from the Optical Line Terminal (OLT), sorting them accordingly without penalizing any ONU due to their distance. The DWDBA takes the laser tuning time into consideration. We conducted extensive simulations to evaluate the performance of the proposed algorithm under various scenarios and compared it to the IPACT algorithm. The results of the simulations show that the proposed algorithm outperformed the IPACT algorithm in terms of bandwidth utilization and queue delay. Full article
(This article belongs to the Special Issue Optical Technologies Supporting 5G/6G Mobile Networks)
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<p>Evolution of LRPON (based on Figure 1 from [<a href="#B19-photonics-10-00923" class="html-bibr">19</a>]).</p>
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<p>OLT and ONUs discovery and communication protocol. The contention zone is the period where multiple ONUs engage in competition to register with the OLT, ensuring collision avoidance.</p>
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<p>Flowchart of the DWDBA algorithm.</p>
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<p>DWDBA Algorithm Sequence Diagram.</p>
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<p>Throughput for scenario 1 where the ONUs are placed between 50 km and 75 km from OLT for DWDBA (<b>left</b>) and IPACT (<b>right</b>).</p>
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<p>Throughput for scenario 2 where the ONUs are placed between 70 km and 100 km from OLT for DWDBA (<b>left</b>) and IPACT (<b>right</b>).</p>
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<p>Throughput for scenario 3 where the ONUs are placed between 17 km and 100 km from OLT for DWDBA (<b>left</b>) and IPACT (<b>right</b>).</p>
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<p>Throughput for scenario 4 where the ONUs are placed between 50 km and 100 km from OLT for DWDBA (<b>left</b>) and IPACT (<b>right</b>).</p>
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<p>Queue delay for scenario 1 where the ONUs are placed between 50 km and 75 km from OLT for DWDBA (<b>left</b>) and IPACT (<b>right</b>).</p>
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<p>Queue delay for scenario 2 where the ONUs are placed between 70 km and 100 km from OLT for DWDBA (<b>left</b>) and IPACT (<b>right</b>).</p>
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<p>Queue delay for scenario 3 where the ONUs are placed between 17 km and 100 km from OLT for DWDBA (<b>left</b>) and IPACT (<b>right</b>).</p>
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<p>Queue delay for ONUs placed between 50 km and 100 km from OLT for DWDBA (<b>left</b>) and IPACT (<b>right</b>).</p>
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6 pages, 3452 KiB  
Article
Tunable Multiwavelength SOA-Based Fiber Laser
by Hani J. Kbashi, Vishal Sharma and Sergey V. Sergeyev
Electronics 2023, 12(15), 3277; https://doi.org/10.3390/electronics12153277 - 30 Jul 2023
Cited by 2 | Viewed by 1612
Abstract
Tunable multiwavelength fiber lasers based on semiconductor optical amplifiers (SOA) have received attracting interest due to their wide prospective applications in dense division multiplexing (DWDM) systems and optical sensing. Using an SOA in a nonlinear optical loop mirror (NOLM), we demonstrate up to [...] Read more.
Tunable multiwavelength fiber lasers based on semiconductor optical amplifiers (SOA) have received attracting interest due to their wide prospective applications in dense division multiplexing (DWDM) systems and optical sensing. Using an SOA in a nonlinear optical loop mirror (NOLM), we demonstrate up to 13 lasing peaks by controlling the pump current and the polarization controller. At maximum pump current (450 mA), the emitted multiwavelength is between 1550 nm and 1572 nm with a wavelength spacing of 1.87 nm and 3 dB output linewidth of 0.8 nm with an output power of −7 dBm and 27 dB optical signal-to-noise ratio (OSNR). The multiwavelength output power and multiwavelength peak stability are investigated, and it was found that the power fluctuation of each multiwavelength line is less than 0.2 dB. In addition, by adjusting the polarization controllers (PCs) and SOA temperature, we obtained a tunable multiwavelength emission. The proposed fiber laser offers advantages such as simple structure, low loss, and long-time stable and multiwavelength emission. Full article
(This article belongs to the Special Issue Advances in Optical Fibers for Fiber Sensors)
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<p>The experimental setup of the multiwavelength SOA fiber laser.</p>
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<p>Multiwavelength emission from SOA fiber laser at different pump currents.</p>
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<p>The emitted wavelength peaks vs. the pump current.</p>
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<p>The multiwavelength SOA fiber laser outputs optical power.</p>
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<p>The multiwavelength SOA fiber laser tunability operating regimes at different SOA temperatures.</p>
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<p>Output optical power stability over 6 h.</p>
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<p>The multiwavelength peaks stability at pump current of 300 mA over 3 h.</p>
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