CN113907193A - Composition of ester catechin and vitamin C palmitate for breeding pigeons and preparation method thereof - Google Patents
Composition of ester catechin and vitamin C palmitate for breeding pigeons and preparation method thereof Download PDFInfo
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- CN113907193A CN113907193A CN202111057430.3A CN202111057430A CN113907193A CN 113907193 A CN113907193 A CN 113907193A CN 202111057430 A CN202111057430 A CN 202111057430A CN 113907193 A CN113907193 A CN 113907193A
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- composition
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- palmitate
- catechin
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- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 title claims abstract description 74
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 title claims abstract description 74
- 235000005487 catechin Nutrition 0.000 title claims abstract description 74
- 229950001002 cianidanol Drugs 0.000 title claims abstract description 74
- 239000000203 mixture Substances 0.000 title claims abstract description 72
- 241000272201 Columbiformes Species 0.000 title claims abstract description 51
- QAQJMLQRFWZOBN-LAUBAEHRSA-N L-ascorbyl-6-palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](O)[C@H]1OC(=O)C(O)=C1O QAQJMLQRFWZOBN-LAUBAEHRSA-N 0.000 title claims abstract description 44
- 235000000072 L-ascorbyl-6-palmitate Nutrition 0.000 title claims abstract description 44
- 239000011786 L-ascorbyl-6-palmitate Substances 0.000 title claims abstract description 44
- 150000002148 esters Chemical group 0.000 title claims abstract description 39
- 238000009395 breeding Methods 0.000 title claims abstract description 26
- 230000001488 breeding effect Effects 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000843 powder Substances 0.000 claims abstract description 34
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 25
- 239000002131 composite material Substances 0.000 claims abstract description 24
- WMBWREPUVVBILR-WIYYLYMNSA-N (-)-Epigallocatechin-3-o-gallate Chemical compound O([C@@H]1CC2=C(O)C=C(C=C2O[C@@H]1C=1C=C(O)C(O)=C(O)C=1)O)C(=O)C1=CC(O)=C(O)C(O)=C1 WMBWREPUVVBILR-WIYYLYMNSA-N 0.000 claims abstract description 19
- WMBWREPUVVBILR-UHFFFAOYSA-N GCG Natural products C=1C(O)=C(O)C(O)=CC=1C1OC2=CC(O)=CC(O)=C2CC1OC(=O)C1=CC(O)=C(O)C(O)=C1 WMBWREPUVVBILR-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000000463 material Substances 0.000 claims abstract description 14
- 239000000287 crude extract Substances 0.000 claims abstract description 12
- 238000011049 filling Methods 0.000 claims abstract description 12
- 239000006185 dispersion Substances 0.000 claims abstract description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 24
- 238000003756 stirring Methods 0.000 claims description 20
- 238000002156 mixing Methods 0.000 claims description 17
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 239000011248 coating agent Substances 0.000 claims description 10
- 238000000576 coating method Methods 0.000 claims description 10
- 150000001875 compounds Chemical class 0.000 claims description 9
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 150000005846 sugar alcohols Polymers 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
- 239000000284 extract Substances 0.000 claims description 5
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 4
- 239000005995 Aluminium silicate Substances 0.000 claims description 4
- 240000008042 Zea mays Species 0.000 claims description 4
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 4
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 4
- 235000012211 aluminium silicate Nutrition 0.000 claims description 4
- 235000005822 corn Nutrition 0.000 claims description 4
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims description 4
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 4
- 229910052901 montmorillonite Inorganic materials 0.000 claims description 4
- -1 polyoxyethylene Polymers 0.000 claims description 4
- 239000004575 stone Substances 0.000 claims description 4
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 3
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 3
- 239000004359 castor oil Substances 0.000 claims description 3
- 235000019438 castor oil Nutrition 0.000 claims description 3
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 3
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 3
- 229920000053 polysorbate 80 Polymers 0.000 claims description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 3
- 235000011152 sodium sulphate Nutrition 0.000 claims description 3
- 235000013312 flour Nutrition 0.000 claims description 2
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 2
- 239000007964 self emulsifier Substances 0.000 claims description 2
- 238000004321 preservation Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 10
- 239000003674 animal food additive Substances 0.000 abstract description 7
- 230000036039 immunity Effects 0.000 abstract description 6
- 230000003647 oxidation Effects 0.000 abstract description 6
- 238000007254 oxidation reaction Methods 0.000 abstract description 6
- 239000002994 raw material Substances 0.000 abstract description 6
- 239000000126 substance Substances 0.000 abstract description 3
- 230000002195 synergetic effect Effects 0.000 abstract description 3
- 238000005538 encapsulation Methods 0.000 abstract description 2
- 239000013538 functional additive Substances 0.000 abstract description 2
- 229940030275 epigallocatechin gallate Drugs 0.000 description 14
- 239000000654 additive Substances 0.000 description 6
- 235000013601 eggs Nutrition 0.000 description 6
- 230000000996 additive effect Effects 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 238000009472 formulation Methods 0.000 description 4
- 210000002966 serum Anatomy 0.000 description 4
- 238000007873 sieving Methods 0.000 description 4
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 3
- 239000003963 antioxidant agent Substances 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 235000006708 antioxidants Nutrition 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 241000411851 herbal medicine Species 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000011718 vitamin C Substances 0.000 description 3
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 2
- 102000002322 Egg Proteins Human genes 0.000 description 2
- 108010000912 Egg Proteins Proteins 0.000 description 2
- 108060003951 Immunoglobulin Proteins 0.000 description 2
- 229930003268 Vitamin C Natural products 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 230000004071 biological effect Effects 0.000 description 2
- 125000004403 catechin group Chemical group 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 235000005911 diet Nutrition 0.000 description 2
- 230000037213 diet Effects 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 125000003976 glyceryl group Chemical group [H]C([*])([H])C(O[H])([H])C(O[H])([H])[H] 0.000 description 2
- 102000018358 immunoglobulin Human genes 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 235000013824 polyphenols Nutrition 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 235000019154 vitamin C Nutrition 0.000 description 2
- XMOCLSLCDHWDHP-SWLSCSKDSA-N (+)-Epigallocatechin Natural products C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC(O)=C(O)C(O)=C1 XMOCLSLCDHWDHP-SWLSCSKDSA-N 0.000 description 1
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- XMOCLSLCDHWDHP-UHFFFAOYSA-N L-Epigallocatechin Natural products OC1CC2=C(O)C=C(O)C=C2OC1C1=CC(O)=C(O)C(O)=C1 XMOCLSLCDHWDHP-UHFFFAOYSA-N 0.000 description 1
- 208000002720 Malnutrition Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 235000004458 antinutrient Nutrition 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 235000014103 egg white Nutrition 0.000 description 1
- 210000000969 egg white Anatomy 0.000 description 1
- 210000002969 egg yolk Anatomy 0.000 description 1
- 235000013345 egg yolk Nutrition 0.000 description 1
- XMOCLSLCDHWDHP-IUODEOHRSA-N epi-Gallocatechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@H]2O)=CC(O)=C(O)C(O)=C1 XMOCLSLCDHWDHP-IUODEOHRSA-N 0.000 description 1
- DZYNKLUGCOSVKS-UHFFFAOYSA-N epigallocatechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3cc(O)c(O)c(O)c3 DZYNKLUGCOSVKS-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- 238000010579 first pass effect Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 235000004213 low-fat Nutrition 0.000 description 1
- 230000001926 lymphatic effect Effects 0.000 description 1
- 230000001071 malnutrition Effects 0.000 description 1
- 235000000824 malnutrition Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 208000015380 nutritional deficiency disease Diseases 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 238000012858 packaging process Methods 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 235000021404 traditional food Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/116—Heterocyclic compounds
- A23K20/121—Heterocyclic compounds containing oxygen or sulfur as hetero atom
- A23K20/126—Lactones
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/116—Heterocyclic compounds
- A23K20/121—Heterocyclic compounds containing oxygen or sulfur as hetero atom
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/22—Compounds of alkali metals
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/24—Compounds of alkaline earth metals, e.g. magnesium
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/28—Silicates, e.g. perlites, zeolites or bentonites
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Zoology (AREA)
- Animal Husbandry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Molecular Biology (AREA)
- Mycology (AREA)
- Physiology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention belongs to the technical field of feed additives, and particularly relates to a composition of ester catechin and vitamin C palmitate for pigeons and a preparation method thereof. The composition comprises: catechin crude extract containing EGCG, vitamin C palmitate, composite self-emulsifying agent, solidified dispersion powder and filling auxiliary material; in the preparation of the composition, the encapsulation effect formed by the vitamin C palmitate and the composite self-emulsifying agent is utilized, so that the stability and the absorptivity of catechin can be effectively ensured, the composition also has a high-efficiency synergistic effect, the bioavailability of ECGC is remarkably improved, the instability problem of conventional catechin is overcome, the biological efficacy of the composition is remarkably improved, and the composition is lower in usage amount, so that the composition has better biological safety; the raw materials used by the composition are food-grade or feed-grade raw materials, and no other chemical preparation is added, so that the composition can be used as a functional additive for substitute resistance to improve the oxidation resistance and immunity of a pigeon breeding organism and improve the egg quality.
Description
Technical Field
The invention belongs to the technical field of feed additives, and particularly relates to a composition of ester catechin and vitamin C palmitate for pigeons and a preparation method thereof.
Background
The pigeon as a traditional food material has extremely high nutritive value, is not only a famous and precious delicious dish, but also a high-grade nourishing product, and is vegetatively named as 'one pigeon Shengjiu chicken'. With the development of economy and improvement of living standard in China, the problem of three highs caused by the traditional high-fat high-cholesterol diet is more and more emphasized, healthy, low-fat and low-cholesterol diet is favored, and consumption diversification is added, so that the pigeon raising industry is greatly developed, and foods of various special pigeons are put on the daily family members. However, with the enlargement of the industrial scale of the pigeon industry, the popularization of commercial feeds, the shortening of the breeding cycle and the like, some problems restricting the pigeon industry are gradually highlighted, such as the problems of complication and multi-pathogenicity of pigeon epidemic diseases, the abuse problem of various drugs of pigeons, the flavor reduction problem of pigeon meat products caused by commercial breeding and the like, so that how to ensure the quality of the pigeon products on the premise of improving the supply quantity of the pigeon products is one of the current popular research projects.
The current commonly used additive solutions include a Chinese herbal medicine additive solution, a plant essential oil or extract additive solution, an antioxidant solution and the like. Patent CN202011067831.2 discloses components, a preparation method and application of a feed additive capable of increasing the feed intake of a pigeon, reducing the diarrhea rate of the pigeon and improving the immunity of the pigeon; patent CN201910225323.3 discloses an antiviral feed additive for young meat pigeons and a preparation method thereof; the patent with Chinese herbal medicines as main components has certain formula complexity and obvious time dependence and dosage dependence on effectiveness, needs large dosage for long-time application to achieve the effect, and the field use cost of the patent technology particularly forms great economic pressure for the poultry industry along with the continuous improvement of the purchase price of the Chinese herbal medicines at present.
Also related patent CN201911279534.1 discloses a gallocatechin and its application in preparing intestinal pathogenic bacteria medicine and feed additive; patent CN201510314609.0 discloses the application of epigallocatechin gallate (EGCG) in preparing pig feed additive and pig feed prepared by the same, the above patent technologies for catechin type feed additives are mostly directly added after simple treatment, neglect the limiting factors which restrict the maximum bioavailability of catechin, namely, catechin is polyphenol substance, which has the problems of poor self-stability and easy oxidation failure, ester catechin such as EGCG has better stability than the conventional non-ester catechin, a considerable loss of effectiveness still occurs, and the effect can only be guaranteed by using an increase in the dosage, meanwhile, considering that the phenolic hydroxyl of catechin is easy to react with various active groups on protein to generate precipitate, the reactant has the effect of anti-nutrient absorption, therefore, when a large amount of catechin additives are added, the loss of nutrients in the feed or the side effects such as malnutrition are often caused.
Disclosure of Invention
In view of the above problems, the present invention aims to provide a composition of ester catechin for breeding pigeons and vitamin C palmitate and a preparation method thereof, and provides a composition of ester catechin for breeding pigeons and vitamin C palmitate, which has characteristics of high stability, high biological activity and no biological toxicity, and a preparation method thereof, wherein the composition can significantly improve oxidation resistance and immunity of the pigeons, and can improve egg quality.
The technical content of the invention is as follows:
the invention provides a composition of ester catechin for pigeons and vitamin C palmitate, which comprises the following components: catechin crude extract containing EGCG, vitamin C palmitate, composite self-emulsifying agent, solidified dispersion powder and filling auxiliary material;
according to the weight parts, 20-40 parts of a catechin crude extract containing EGCG, 10-20 parts of vitamin C palmitate, 10-20 parts of a composite self-emulsifying agent, 10-20 parts of solidified dispersion powder and 20-40 parts of a filling auxiliary material;
the crude catechin extract contains 5% of EGCG;
the composite self-emulsifying agent is a composition of polyhydric alcohol and an emulsifying agent in a weight part ratio of 1: 5-1: 9, wherein the polyhydric alcohol comprises one or two of propylene glycol and glycerol;
the emulsifier comprises one or more of glycerol, tween-80, polyoxyethylene castor oil oxide and glyceryl monostearate;
the polyalcohol and the emulsifier in the composite self-emulsifier are mixed;
the solidified dispersing powder comprises one or more than one of active carbon, calcium carbonate, corncob powder, bran powder and puffed corn powder;
the filling auxiliary materials comprise one or more than one of medical stone powder, montmorillonite powder, kaolin powder and anhydrous sodium sulphate.
The invention also provides a preparation method of the composition of ester catechin and vitamin C palmitate for the breeding pigeons, which comprises the following steps:
1) mixing vitamin C palmitate and a composite self-emulsifying agent, heating to fully melt, then preserving heat at the temperature of 100-110 ℃, adding a catechin crude extract containing EGCG, and continuously stirring to form a compound type wrapping liquid of ester type catechin;
2) slowly adding the compound coating solution into the preheated solidified dispersion powder, continuously stirring, fully mixing, cooling to room temperature, adding the filling auxiliary materials, uniformly stirring, crushing the finally obtained mixture, and uniformly stirring to obtain the composition of ester catechin and vitamin C palmitate;
the application method of the prepared composition is that the composition is directly prepared into feed for mixing or added with pigeon sand for use, and the composition can be used for raising breeding pigeons to improve the oxidation resistance and the immune function of a matrix and improve the egg quality.
The invention has the following beneficial effects:
according to the composition of the ester catechin and the vitamin C palmitate for the breeding pigeons, the vitamin C palmitate and the composite self-emulsifying agent form an encapsulation effect, so that the stability and the absorptivity of the catechin can be effectively guaranteed, and on the other hand, the vitamin C palmitate and the ester catechin have high-efficiency synergistic effect, so that the bioavailability of ECGC is remarkably improved, the efficacy of the composition is remarkably superior to that of a conventional catechin and catechin-vitamin C combined additive, and after the additive is continuously applied, the health condition of the breeding pigeons can be remarkably improved, and the production performance is improved. The defects of the prior art are overcome, the instability problem of the conventional catechin is overcome, the biological efficacy of the catechin is obviously improved, and the usage amount is lower, so that the catechin has better biological safety; the raw materials used by the composition are food-grade or feed-grade raw materials, and no other chemical preparation is added, so that the composition can be used as a functional additive for substitute resistance to improve the oxidation resistance and immunity of a pigeon breeding organism and improve the egg quality.
The composition is an ester active substance, and a considerable amount of the active substance is absorbed by lymphatic circulation through a special packaging process and a self-emulsifying technology, so that the first pass effect of the liver is effectively avoided, and the organism has a longer half-life period. The ester catechin and the vitamin C palmitate have special biological synergistic effect, thereby ensuring that the composition has biological efficacy which is obviously superior to that of the conventional catechin.
Detailed Description
The present invention is described in further detail in the following detailed description with reference to specific embodiments, which are intended to be illustrative only and not to be limiting of the scope of the invention, as various equivalent modifications of the invention will become apparent to those skilled in the art after reading the present invention and are intended to be included within the scope of the appended claims.
All the raw materials and reagents of the invention are conventional market raw materials and reagents unless otherwise specified.
Example 1
A composition of ester catechin and vitamin C palmitate for breeding pigeons and preparation thereof are disclosed:
1) mixing 15 parts of vitamin C palmitate and 10 parts of composite self-emulsifying agent, heating to fully melt, keeping the temperature at 105 ℃, adding 30 parts of catechin crude extract containing 50% of EGCG, and continuously stirring for 20min to form ester type catechin composite coating liquid;
the composite self-emulsifying agent is a mixture of propylene glycol and glycerol in a weight ratio of 1: 5;
2) slowly adding the compound coating liquid into 10 parts of cured dispersion powder puffed corn flour subjected to preheating treatment, continuously stirring, fully mixing, cooling to room temperature, adding 35 parts of montmorillonite powder serving as an auxiliary material, uniformly stirring, crushing the finally obtained mixture, sieving by a 60-mesh sieve, and uniformly mixing by a stirrer to obtain the composition of ester catechin and vitamin C palmitate.
Example 2
A composition of ester catechin and vitamin C palmitate for breeding pigeons and preparation thereof are disclosed:
1) mixing 15 parts of vitamin C palmitate and 15 parts of composite self-emulsifying agent, heating to fully melt, keeping the temperature at 110 ℃, adding 20 parts of catechin crude extract containing 50% of EGCG, and continuously stirring for 20min to form ester type catechin composite coating solution;
the composite self-emulsifying agent is a mixture of glycerol, Tween-80 and glyceryl mono-distearate in a weight part ratio of 1:3: 3;
2) slowly adding the compound coating solution into 10 parts of pre-heat-treated solidified dispersed powder (5 parts of corncob powder and bran powder respectively), continuously stirring, cooling to room temperature after fully mixing, adding 40 parts of filling auxiliary materials (20 parts of medical stone powder and kaolin powder respectively), uniformly stirring, crushing the finally obtained mixture, sieving by a 60-mesh sieve, and uniformly mixing by a stirrer to obtain the composition of ester catechin and vitamin C palmitate.
Example 3
A composition of ester catechin and vitamin C palmitate for breeding pigeons and preparation thereof are disclosed:
1) mixing 10 parts of vitamin C palmitate and 20 parts of composite self-emulsifying agent, heating to fully melt, keeping the temperature at 100 ℃, adding 25 parts of catechin crude extract containing 50% of EGCG, and continuously stirring for 20min to form ester type catechin composite coating liquid;
the composite self-emulsifying agent is a mixture of propylene glycol, glycerol and polyoxyethylene castor oil in a weight part ratio of 1:1: 18;
2) slowly adding the compound coating solution into 20 parts of pre-heated solidified dispersion powder (10 parts of activated carbon and calcium carbonate respectively), continuously stirring, fully mixing, cooling to room temperature, adding 25 parts of filling auxiliary materials (15 parts of medical stone powder and 10 parts of montmorillonite powder), uniformly stirring, crushing the finally obtained mixture, sieving by a 60-mesh sieve, and uniformly mixing by a stirrer to obtain the composition of ester catechin and vitamin C palmitate.
Example 4
A composition of ester catechin and vitamin C palmitate for breeding pigeons and preparation thereof are disclosed:
1) mixing 20 parts of vitamin C palmitate and 10 parts of composite self-emulsifying agent, heating to fully melt, keeping the temperature at 108 ℃, adding 40 parts of catechin crude extract containing 50% of EGCG, and continuously stirring for 20min to form ester type catechin composite coating liquid;
the composite self-emulsifying agent is a mixture of propylene glycol, glycerol and glyceryl mono-distearate in a weight part ratio of 1:4: 4;
2) slowly adding the compound coating solution into 10 parts of pre-heat-treated solidified dispersing powder (5 parts of bran powder and puffed corn powder respectively), continuously stirring, cooling to room temperature after fully mixing, adding 20 parts of filling auxiliary materials (10 parts of kaolin powder and anhydrous sodium sulphate respectively), uniformly stirring, crushing the finally obtained mixture, sieving by a 60-mesh sieve, and uniformly mixing by a stirrer to obtain the composition of ester catechin and vitamin C palmitate.
The following comparative experiments were carried out on the effect of young pigeon breeders fed with compositions of different catechin formulations:
TABLE 1 composition of different catechin formulations
| Group of | Catechin component | Concentration of use |
| 1# | Catechin formulation of example 1 | 200mg/kg |
| 2# | Catechin formulation of example 2 | 200mg/kg |
| 3# | Catechin crude extract containing 50% EGCG | 200mg/kg |
| 4# | Catechin crude extract containing 50% EGCG | 200mg/kg |
| 5# | Catechin crude extract containing 50% EGCG and vitamin C | 200mg/kg+400mg/kg |
| 6# | Blank group-basic feed | - |
Young pigeon breeders of 7 months old are selected and fed with the composition prepared in table 1 by adding basal feed, and are formally tested for 4 weeks after being pre-fed for 1 week.
The serum and the pigeon egg quality of young pigeons of each group are detected, and the test results are as follows:
TABLE 2 influence of different treatment groups on the antioxidant function of pigeon sera
As can be seen from Table 2, the antioxidant function of the serum of the breeding pigeon can be improved by using the composition provided by the embodiment of the invention for breeding the breeding pigeon.
TABLE 3 influence of different treatment groups on the serum immunoglobulin content of breeding pigeons
As can be seen from Table 3, the composition of the present invention can improve the immune globulin of the serum of the breeding pigeon and improve the body immunity of the breeding pigeon.
TABLE 4 Effect of different treatment groups on the Pigeon protein
As can be seen from Table 3, the composition of the present invention can improve the shell strength, egg white and egg yolk quality of pigeon eggs.
In conclusion, the experimental effect of the catechin and vitamin C compound group is obviously higher than that of the catechin group added with 200mg/kg alone, and some indexes are even close to or higher than that of the catechin group added with 400 mg/kg. The composition of ester catechin and vitamin C palmitate adopted by the invention has better life activity and biological safety, the combination proportion of the composition exerts high biological effect, and the composition is used for breeding pigeon, is helpful for improving the oxidation resistance and immunity of the pigeon matrix and can improve the egg quality.
Claims (9)
1. A composition of ester catechin for breeding pigeons and vitamin C palmitate is characterized in that the components in the composition comprise: catechin crude extract containing EGCG, vitamin C palmitate, composite self-emulsifying agent, solidified dispersion powder and filling auxiliary material.
2. The composition of ester catechin and vitamin C palmitate as defined in claim 1, wherein the composition comprises, by weight, 20-40 parts of crude catechin extract containing EGCG, 10-20 parts of vitamin C palmitate, 10-20 parts of composite self-emulsifying agent, 10-20 parts of solidified dispersion powder and 20-40 parts of filling auxiliary material.
3. The composition of ester catechin and vitamin C palmitate as claimed in claim 1, wherein the crude catechin extract contains 5% of EGCG.
4. The composition of ester catechin and vitamin C palmitate as claimed in claim 1, wherein the composite self-emulsifying agent is a composition of polyhydric alcohol and emulsifying agent, and the polyhydric alcohol comprises one or two of propylene glycol and glycerol;
the emulsifier comprises one or more of glycerol, tween-80, polyoxyethylene castor oil oxide and glyceryl monostearate.
5. The composition of ester catechin and vitamin C palmitate as defined in claim 1, wherein the weight ratio of the polyhydric alcohol to the emulsifier in the composite self-emulsifier is 1: 5-1: 9.
6. The composition of ester catechin and vitamin C palmitate as defined in claim 1, wherein the components of the solidified dispersion powder comprise one or more of activated carbon, calcium carbonate, corncob powder, bran powder and puffed corn flour.
7. The composition of ester catechin and vitamin C palmitate as claimed in claim 1, wherein the filling auxiliary materials comprise one or more of medical stone powder, montmorillonite powder, kaolin powder and anhydrous sodium sulphate.
8. A preparation method of the composition of ester catechin for breeding pigeons and vitamin C palmitate as claimed in any one of claims 1 to 7 is characterized by comprising the following steps:
1) mixing vitamin C palmitate and compound self-emulsifying agent, heating to melt completely, keeping the temperature, adding crude catechin extract containing EGCG, and stirring to obtain compound type catechin inclusion solution;
2) slowly adding the compound coating solution into the preheated solidified dispersion powder, continuously stirring, fully mixing, cooling to room temperature, adding the filling auxiliary materials, uniformly stirring, crushing the finally obtained mixture, and uniformly stirring to obtain the composition of ester catechin and vitamin C palmitate.
9. The method for preparing the composition of ester catechin and vitamin C palmitate for the breeding pigeons according to claim 8, wherein the temperature for the heat preservation in the step 1) is 100-110 ℃.
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Citations (2)
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| CN101277618A (en) * | 2005-09-30 | 2008-10-01 | 帝斯曼知识产权资产管理有限公司 | Novel compositions containing polyphenols |
| CN113142414A (en) * | 2021-02-09 | 2021-07-23 | 仲恺农业工程学院 | Enteric tea polyphenol feed additive and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101277618A (en) * | 2005-09-30 | 2008-10-01 | 帝斯曼知识产权资产管理有限公司 | Novel compositions containing polyphenols |
| CN113142414A (en) * | 2021-02-09 | 2021-07-23 | 仲恺农业工程学院 | Enteric tea polyphenol feed additive and preparation method thereof |
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Inventor after: Fu Jing Inventor after: Huang Yanhua Inventor after: Chen Ailing Inventor after: Ma Tingting Inventor after: Zhong Yajing Inventor after: Fu Zhiqi Inventor after: Tu Chengming Inventor after: Deng Shan Inventor before: Fu Jing Inventor before: Huang Yanhua Inventor before: Chen Ailing Inventor before: Ma Tingting Inventor before: Zhong Yajing Inventor before: Fu Zhiqi Inventor before: Tu Cheng |
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Application publication date: 20220111 |