CN103749742A - Production method of zanthoxylum oil - Google Patents
Production method of zanthoxylum oil Download PDFInfo
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- CN103749742A CN103749742A CN201310748189.8A CN201310748189A CN103749742A CN 103749742 A CN103749742 A CN 103749742A CN 201310748189 A CN201310748189 A CN 201310748189A CN 103749742 A CN103749742 A CN 103749742A
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- zanthoxylum essential
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Abstract
The invention discloses a production method of zanthoxylum oil. The method comprises the following steps: selecting dried zanthoxylum and vegetable oil; baking and sauting the vegetable oil for 10-60 minutes at 60-100 DEG C, adding the dried zanthoxylum accounting for 6-12wt% of the vegetable oil when cooling the vegetable oil to 50-80 DEG C and maintaining for 2-10 minutes so as to obtain mixed oil; adding the mixed oil obtained in the mixing and sauting manner into an oil presser, maintaining the temperature within 70-100 DEG C and performing initial squeezing so as to obtain the zanthoxylum oil; performing preliminary filtration on the initially-squeezed zanthoxylum oil by using a filter screen so as to filter a majority of impurities; introducing the zanthoxylum oil subjected to the preliminary filtration into a vacuum filter; performing filtration on zanthoxylum oil again under the condition that the oil temperature is maintained within 75 DEG C to 105 DEG C so as to improve the filtration efficiency; adding the zanthoxylum oil subjected to the vacuum filtration into a centrifugal oil filter and performing rotating precipitation and filtration again, thereby obtaining the zanthoxylum oil. The method is high in production efficiency, wide in raw material resource, low in cost and pure in zanthoxylum oil taste.
Description
Technical field
The present invention relates to food processing technology field, relate in particular to a kind of production method of Zanthoxylum essential oil.
Background technology
Chinese prickly ash pericarp is conventional flavoring, and in pricklyash bark, all kinds of volatile flavor content, up to 9%, is not only and is refined the good raw material of making senior flavoring essence, and be standing edible flavouring.The function that Chinese prickly ash has appetizing, invigorating the spleen, builds up health.At present, Chinese prickly ash has been subject to numerous people's favor, has a sudden rise in social status.Existing Zanthoxylum essential oil preparation method has the methods such as fractionation, the poach way of distillation.Fractionation mainly extracts aromatic oil from Chinese pepper with the chemical reagent of ether, benzinum, and the Zanthoxylum essential oil that this method is extracted exists chemical agent residue, and aromatic oil quality is impure, the shortcoming that peculiar smell is heavier.China Patent Publication No. CN101606676 discloses " a kind of production technology of fresh pepper green pepper oil " on December 23rd, 2009, and it obtains fresh Chinese prickley ash extract after having adopted mechanical broken skin, and recycling vegetable oil mixes the method for soaking acquisition Zanthoxylum essential oil.But this method is owing to adopting the wet Chinese prickly ash processing Zanthoxylum essential oil of silver pheasant, thereby be subject to the restriction in the place of production, picking season, be difficult to produce in non-Chinese prickly ash main producing region, non-picking season, have the shortcoming that transport of materials storage cost is high simultaneously.Because wet Chinese prickly ash water content is large, so the Zanthoxylum essential oil water content of producing is also large, acid value is high, cannot guarantee the stability of the quality of fresh zanthoxylum oil.The existing non-Chinese prickly ash place of production, the Zanthoxylum essential oil processing method in non-picking season are all with rape oil, to allocate after the aromatic oil of prior extraction fresh pepper and numb element again, in allocation process, all to add the chemical reagent such as emulsifying agent, stabilizing agent, neither environmental protection, of long duration all can have peculiar smell.
Summary of the invention
The production method of the Zanthoxylum essential oil that a kind of production efficiency is high, raw material sources are wide, cost is low, mouthfeel is pure that the object of the invention is to solve above-mentioned shortcoming and provide.
The production method of a kind of Zanthoxylum essential oil of the present invention, comprises that step is as follows; (1) raw material is selected: select dried flower green pepper, vegetable oil material;
(2) parch: vegetable oil material, at 60-100 ℃ of parch 10-60 minute, when vegetable oil material temperature is down to 50-80 ℃, is added to the dried flower green pepper of vegetable oil material weight 6-12%, keep 2-10 minute, obtain mixing oil plant;
(3) squeezing: add oil plant squeezer by mixing the mixing oil plant of frying after perfume (or spice), maintain the temperature at 70-100 ℃, tentatively squeeze out Zanthoxylum essential oil; (4) initial filter: will tentatively squeeze out Zanthoxylum essential oil and tentatively filter with filter screen, the most of impurity of filtering;
(5) vacuum filtration: by the Zanthoxylum essential oil after initial filter, introduce in vacuum filter and again filter, during oil temperature remain on 75-105 ℃, to improve filter efficiency.(6) centrifugal filtration: the Zanthoxylum essential oil through vacuum filtration is added in centrifugal oil filter and is again rotated precipitation, filtration, obtain Zanthoxylum essential oil.
The production method of above-mentioned a kind of Zanthoxylum essential oil, wherein: for quality better, dried flower green pepper adopts that kind is pure, quality is superior.
The production method of above-mentioned a kind of Zanthoxylum essential oil, wherein: the preferred rapeseed oil of vegetable oil or soybean oil.
The production method of above-mentioned a kind of Zanthoxylum essential oil, wherein: pressing temperature is controlled at 85-95 ℃.
The present invention compared with prior art, has obvious advantage and effect, from above technical scheme: due to directly squeezing after having adopted dried flower green pepper and oil plant to mix, shortened production procedure, improved the daily output, 1 two of complete equipments workman's day can be produced 2 tons of Zanthoxylum essential oils, and production efficiency is high; Adopt dried flower green pepper to mix oil plant and directly squeeze, be not subject to the restriction in geographical position, Chinese prickly ash producing region.Raw material is applied widely: the equal of each Chinese prickly ash kind as domestic and international in clovershrub, pericarpium zanthoxyli schinifolii, rattan green pepper etc. can adopt this processing method.Can effectively reduce costs: the relatively wet Chinese prickly ash transportation of the condition of storage of dried flower green pepper storage cost is lower; Simultaneously can squeeze at any time Zanthoxylum essential oil according to market demand and sell, thereby can reduce the rate of capital employed, and this technique is without expensive device, labour protection measures is less demanding, and labour intensity is little, is beneficial to and reduces costs, time saving and energy saving.Mouthfeel is pure: by the direct cold pressing Pericarpium Zanthoxyli fruit of physical mechanical, make the active ingredient in Chinese prickly ash fully be dissolved into edible vegetable oil, directly obtain containing the high Zanthoxylum essential oil of active ingredient, the technological design of science has retained Chinese prickly ash genuineness and abundant nutritional labeling to greatest extent.
The specific embodiment
embodiment 1:
A production method for Zanthoxylum essential oil, comprises that step is as follows: (1) raw material is selected: select kind is pure, quality is superior dried flower green pepper, vegetable seed;
(2) parch: vegetable seed, 90 ℃ of parch 50 minutes, when vegetable seed temperature is down to 50-60 ℃, is added to the dried flower green pepper of vegetable seed weight 8%, keep 6-8 minute (further to remove the moisture in Chinese prickly ash), obtain mixing oil plant;
(3) squeezing: add oil plant squeezer by mixing the mixing oil plant of frying after perfume (or spice), maintain the temperature at 85-95 ℃, tentatively squeeze out Zanthoxylum essential oil; (4) initial filter: will tentatively squeeze out Zanthoxylum essential oil and tentatively filter with filter screen, the most of impurity of filtering;
(5) vacuum filtration: by the Zanthoxylum essential oil after initial filter, introduce in vacuum filter and again filter, during oil temperature remain on 75-85 ℃, to improve filter efficiency.(6) centrifugal filtration: the Zanthoxylum essential oil through vacuum filtration is added in centrifugal oil filter and is again rotated precipitation, filtration, obtain Zanthoxylum essential oil.
embodiment 2:
A production method for Zanthoxylum essential oil, comprises that step is as follows: (1) raw material is selected: select dried flower green pepper, soybean;
(2) parch: soybean, 60 ℃ of parch 60 minutes, when vegetable oil temperature is down to 60-70 ℃, is added to the dried flower green pepper of vegetable oil weight 12%, keep 10 minutes (further to remove the moisture in Chinese prickly ash), obtain mixing oil plant;
(3) squeezing: add oil plant squeezer by mixing the mixing oil plant of frying after perfume (or spice), maintain the temperature at 70-80 ℃, tentatively squeeze out Zanthoxylum essential oil; (4) initial filter: will tentatively squeeze out Zanthoxylum essential oil and tentatively filter with filter screen, the most of impurity of filtering;
(5) vacuum filtration: by the Zanthoxylum essential oil after initial filter, introduce in vacuum filter and again filter, during oil temperature remain on 80-90 ℃, to improve filter efficiency.(6) centrifugal filtration: the Zanthoxylum essential oil through vacuum filtration is added in centrifugal oil filter and is again rotated precipitation, filtration, obtain Zanthoxylum essential oil.
embodiment 3:
A production method for Zanthoxylum essential oil, comprises that step is as follows: (1) raw material is selected: select kind is pure, quality is superior dried flower green pepper, peanut;
(2) parch: peanut, 100 ℃ of parch 10 minutes, when peanut temperature is down to 70-80 ℃, is added to the dried flower green pepper of peanut weight 6%, keep 2 minutes (further to remove the moisture in Chinese prickly ash), obtain mixing oil plant;
(3) squeezing: add oil plant squeezer by mixing the mixing oil plant of frying after perfume (or spice), maintain the temperature at 80-100 ℃, tentatively squeeze out Zanthoxylum essential oil; (4) initial filter: will tentatively squeeze out Zanthoxylum essential oil and tentatively filter with filter screen, the most of impurity of filtering;
(5) vacuum filtration: by the Zanthoxylum essential oil after initial filter, introduce in vacuum filter and again filter, during oil temperature remain on 90-105 ℃, to improve filter efficiency.(6) centrifugal filtration: the Zanthoxylum essential oil through vacuum filtration is added in centrifugal oil filter and is again rotated precipitation, filtration, obtain Zanthoxylum essential oil.
The above, it is only preferred embodiment of the present invention, not the present invention is done to any pro forma restriction, any technical solution of the present invention content that do not depart from, any simple modification, equivalent variations and the modification above embodiment done according to technical spirit of the present invention, all still belong in the scope of technical solution of the present invention.
Claims (4)
1. a production method for Zanthoxylum essential oil, comprises that step is as follows: (1) raw material is selected: select dried flower green pepper, vegetable oil material;
(2) parch: vegetable oil material, at 60-100 ℃ of parch 10-60 minute, when vegetable oil material temperature is down to 50-80 ℃, is added to the dried flower green pepper of vegetable oil material weight 6-12%, keep 2-10 minute, obtain mixing oil plant;
(3) squeezing: add oil plant squeezer by mixing the mixing oil plant of frying after perfume (or spice), maintain the temperature at 70-100 ℃, tentatively squeeze out Zanthoxylum essential oil; (4) initial filter: will tentatively squeeze out Zanthoxylum essential oil and tentatively filter with filter screen, the most of impurity of filtering;
(5) vacuum filtration: by the Zanthoxylum essential oil after initial filter, introduce in vacuum filter and again filter, during oil temperature remain on 75-105 ℃, to improve filter efficiency; (6) centrifugal filtration: the Zanthoxylum essential oil through vacuum filtration is added in centrifugal oil filter and is again rotated precipitation, filtration, obtain Zanthoxylum essential oil.
2. the production method of a kind of Zanthoxylum essential oil as claimed in claim 1, wherein: pressing temperature is controlled at 85-95 ℃.
3. the production method of a kind of Zanthoxylum essential oil as claimed in claim 1 or 2, wherein: dried flower green pepper adopts that kind is pure, quality is superior.
4. the production method of a kind of Zanthoxylum essential oil as claimed in claim 3, wherein: plant grease separation rapeseed oil or soybean oil.
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| CN201310748189.8A CN103749742A (en) | 2013-12-31 | 2013-12-31 | Production method of zanthoxylum oil |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104255945A (en) * | 2014-07-14 | 2015-01-07 | 安徽省东至金润油脂有限责任公司 | Pea zanthoxylum oil |
| CN104357210A (en) * | 2014-10-28 | 2015-02-18 | 赵跃军 | Fresh Yaomazi rattan pepper oil pressing process |
| CN105132141A (en) * | 2015-09-22 | 2015-12-09 | 罗春燕 | Method for preparing prickly ash seed oil through mechanical compression |
| CN105670768A (en) * | 2016-01-20 | 2016-06-15 | 和县绿源油脂有限公司 | Aromatic compound bean oil and production process thereof |
| CN105779100A (en) * | 2016-03-09 | 2016-07-20 | 刘帅 | Making method of yellow mustard oil |
| CN106947584A (en) * | 2017-04-21 | 2017-07-14 | 贵州省贵定县古镇香粮油有限公司 | A kind of processing method of rapeseed oil |
| CN109609253A (en) * | 2018-12-10 | 2019-04-12 | 汉源县川博食品有限公司 | A kind of production method of fresh zanthoxylum oil |
| CN109769959A (en) * | 2017-11-13 | 2019-05-21 | 贵州可一绿色食品有限公司 | A kind of processing technology of Zanthoxylum essential oil |
| CN110731392A (en) * | 2019-10-30 | 2020-01-31 | 樊轩 | method for preparing Chinese prickly ash oil |
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2013
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| US20030024029A1 (en) * | 2001-07-20 | 2003-02-06 | Fiorini Jeffrey L. | Removable insert for athletic leg guards |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104255945A (en) * | 2014-07-14 | 2015-01-07 | 安徽省东至金润油脂有限责任公司 | Pea zanthoxylum oil |
| CN104357210A (en) * | 2014-10-28 | 2015-02-18 | 赵跃军 | Fresh Yaomazi rattan pepper oil pressing process |
| CN105132141A (en) * | 2015-09-22 | 2015-12-09 | 罗春燕 | Method for preparing prickly ash seed oil through mechanical compression |
| CN105670768A (en) * | 2016-01-20 | 2016-06-15 | 和县绿源油脂有限公司 | Aromatic compound bean oil and production process thereof |
| CN105779100A (en) * | 2016-03-09 | 2016-07-20 | 刘帅 | Making method of yellow mustard oil |
| CN106947584A (en) * | 2017-04-21 | 2017-07-14 | 贵州省贵定县古镇香粮油有限公司 | A kind of processing method of rapeseed oil |
| CN109769959A (en) * | 2017-11-13 | 2019-05-21 | 贵州可一绿色食品有限公司 | A kind of processing technology of Zanthoxylum essential oil |
| CN109609253A (en) * | 2018-12-10 | 2019-04-12 | 汉源县川博食品有限公司 | A kind of production method of fresh zanthoxylum oil |
| CN110731392A (en) * | 2019-10-30 | 2020-01-31 | 樊轩 | method for preparing Chinese prickly ash oil |
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Application publication date: 20140430 |