Nothing Special   »   [go: up one dir, main page]

CN101869084A - Preparation method for magnetic pearl nucleus - Google Patents

Preparation method for magnetic pearl nucleus Download PDF

Info

Publication number
CN101869084A
CN101869084A CN201010208002A CN201010208002A CN101869084A CN 101869084 A CN101869084 A CN 101869084A CN 201010208002 A CN201010208002 A CN 201010208002A CN 201010208002 A CN201010208002 A CN 201010208002A CN 101869084 A CN101869084 A CN 101869084A
Authority
CN
China
Prior art keywords
magnetic
pearl
preparation
pearl nucleus
nuclear
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201010208002A
Other languages
Chinese (zh)
Inventor
宋文东
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangdong Ocean University
Original Assignee
Guangdong Ocean University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangdong Ocean University filed Critical Guangdong Ocean University
Priority to CN201010208002A priority Critical patent/CN101869084A/en
Publication of CN101869084A publication Critical patent/CN101869084A/en
Pending legal-status Critical Current

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/80Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
    • Y02A40/81Aquaculture, e.g. of fish

Landscapes

  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Magnetic Treatment Devices (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to a preparation method for a magnetic pearl nucleus. An ordinary round pearl nucleus is adopted as the seed nucleus of the pearl nucleus, high polymer is adopted as the film-forming substance of the pearl nucleus, and is added with a magnetic substance and then other auxiliaries, so that magnetic coating is prepared, the coating is uniformly coated on the surface of the seed nucleus, and after drying and solidification under the temperature of 60 DEG C to 70 DEG C, the shiny, round magnetic pearl nucleus with 0.1mm to 1.0mm of coating is formed. The pearl nucleus is safe and non-toxic, and a pearl cultured with the magnetic pearl nucleus is magnetic, and has the effects of promoting the circulation of blood and increasing the oxygen content of blood.

Description

A kind of preparation method of magnetic pearl nucleus
Technical field
The invention belongs to a kind of preparation method of magnetic pearl nucleus.
Background technology
China's pearl industry is with a long history, and along with progress of science and technology, the breed amount of pearl constantly increases, and crudy also improves thereupon, but sales value does not have proportional rise.Return its reason, remove the performance resources advantage, develop the economy, aspect such as the rich masses comes with some shortcomings, and the more important thing is that new technology development is backward relatively.Nowadays, pearl sector is badly in need of increasing spending on science and technology, and strengthens basic research and application technical research, and the active development new product is with further raising pearl quality and increase pearl added value.
Present characteristic pearl has: noctilucence pearl, attached shell pearl, madanku are few to the research of magnetic pearl.Magnetic action can produce six large effects when human body: stimulate circulation, improve microcirculation; Regulate blood pressure, reduce blood viscosity; Anti-inflammatory, analgesia; Improve body immunity, delay senility; Regulate neural function, eliminate tired; Toxin expelling.
Based on this, in the surface applied of former common pearl nuclear with the cold magnetisable material of safety non-toxic, make pearl nuclear with magnetic, cultivate the pearl that has magnetic with this, when human body is worn, can bring into play it and stimulate circulation, increase the effect of oxygen carrying content in the blood, decorate the effect of cohabiting with health care thereby reach, its price must significantly improve.
Summary of the invention
The preparation method who the purpose of this invention is to provide a kind of magnetic pearl nucleus by preparing a kind of magnetisable coating, is coated in free pearl nuclear surface with it and makes the noctilucence magnetic pearl nucleus, inserts nuclear with it, cultivates the magnetic pearl with health-care efficacy.
For achieving the above object, the present invention adopts following technical scheme:
1, serves as base nuclear with common free pearl nuclear, select for use and contain the common pearl nuclear that calcium carbonate, lucite and organic resin are main component, as shell pearl nuclear, coral pearl nuclear, marble pearl nuclear, giant clam pearl nuclear, oyster pearl inside the body of a freshwater mussel nuclear.
2, select nontoxic radiationless magnetic (γ-Fe for use 2O 3Or Fe 3O 4) as magnetisable material, add film forming matter and auxiliary agent, be mixed with magnetic coating.
Raw material and proportioning that magnetic coating is used are as follows:
Component content w/%
High molecular polymer 50~70
Magnetisable material 20~30
Coalescents 1.0~10
Dispersant 1.0~10
Defoamer 0.1~1.0
The deionized water surplus
Preparation method: after each raw material taken by weighing, deionized water is put earlier in people's agitator, under stirring at low speed, added dispersant and part defoamer and mix, then with magnetic slowly in the vortex of falling people, after adding magnetic, improve mixing speed, add plasticizer, coalescents, stir 20~30min, after being uniformly dispersed, under stirring at low speed, slowly add high molecular polymer and residue defoamer, regulate the pH value and be about 8, can make magnetic coating.
3, the coating of magnetic coating: after magnetic coating is coated on free radical nuclear, in 60~70 ℃ of baking ovens, dry immediately, if dry back coating surface non-uniform light is selected the repeatedly method of spraying, oven dry at once after each spraying continues to dry after the spraying then again.Can obtain the smooth paint film of surfacing.
4, control magnetisable coating thickness is 0.1~1.0mm, can obtain magnetic pearl nucleus.
The prepared pearl nucleus band of the present invention is magnetic, and can stimulate circulation, and increases the oxygen carrying content in the blood, and safety non-toxic after the processing of pearl nuclear activity, is inserted nuclear, can cultivate the magnetic pearl of high high added value.
Embodiment
Embodiment 1
γ-Fe 2O 3The preparation raw material and the proportioning of magnetic pearl nucleus are as follows:
Material composition content w/%
Aqueous epoxy resin emulsion 60
γ--Fe 2O 3Magnetic 25
12 carbon alcohol esters 5
Polyethylene glycol-1,000 6
Dimethicone 0.5
The deionized water surplus
Take by weighing each component according to above formula rate, part prescription is put in the dispersator, add various auxiliary agents, after slowly stirring 20~30min and mixing, again with γ-Fe 2O 3In the vortex that magnetic adding impeller stirs, improve mixing speed, magnetic material is evenly spread in the solution, the PH of regulation system is neutrality or meta-alkalescence.Add aqueous epoxy resin emulsion and all the other auxiliary agents and water then gradually, after stirring 30~40min at a slow speed and being uniformly dispersed, can make γ-Fe 2O 3Magnetic coating.
Selecting background color for use is 200 of the common shell pearl nuclears of white, after the washing oven dry, magnetic coating evenly is coated in free radical nuclear surface after, 60 ℃ of baking and curing make the magnetic pearl nucleus that coating layer thickness is 0.1~1.0mm.
Embodiment 2
Fe 3O 4The preparation raw material and the proportioning of magnetic pearl nucleus are as follows:
Material composition content w/%
Benzene emulsion 60
Fe 3O 4Magnetic 20
12 carbon alcohol esters 6.0
Polyethylene glycol-1,000 8.0
Dimethicone 0.5
The deionized water surplus
Take by weighing each component according to above formula rate, the water of will partly filling a prescription is put in the dispersator, adds various auxiliary agents, slowly stir 20~30min to be mixed evenly after, again with Fe 3O 4In the vortex that magnetic adding impeller stirs, improve mixing speed, magnetic material is evenly spread in the solution, the PH of regulation system is neutrality or meta-alkalescence.Add benzene emulsion and all the other auxiliary agents and water then gradually, after stirring 30~40min at a slow speed and being uniformly dispersed, can make Fe 3O 4Magnetic coating.
Selecting background color for use is 200 of the common shell pearl nuclears of white, after the washing oven dry, magnetic coating evenly is coated in the free nuclear of base surface after, 60 ℃ of baking and curing, making thickness is the F magnetic pearl nucleus of 0.1~1.0mm.
Embodiment 3
The cultivation of magnetic pearl
The cultivation of magnetic pearl is grown cultured pearls to test the Xuwen pearl and has been obtained very good result, the magnetic pearl nucleus that makes according to above-mentioned technical scheme, pteria martensii is carried out manually inserting nuclear, each pearly shellfish is inserted two nuclears, from cultured 2 months pearly shellfish, take out pearl, the core-remaining rate of shellfish reaches 72.6%, and staying check figure is 1.45/shellfish.

Claims (6)

1. the preparation method of a magnetic pearl nucleus, it is characterized in that with common free pearl nuclear be base nuclear, high molecular polymer is a filmogen, be aided with suitable magnetisable material, coalescents, dispersant, defoamer, the formulated a kind of magnetic coating of deionized water again, evenly be coated on base nuclear surface with this, oven dry forms.
2. require the preparation method of 1 described a kind of magnetic pearl nucleus according to patent, it is characterized in that: the base selected for use nuclear is to be the common pearl nuclear of main component with calcium carbonate, lucite and organic resin: shell, coral, giant clam, oyster freshwater mussel, marble, surface clean is smooth.
3. require the preparation method of 1 described a kind of magnetic pearl nucleus according to patent, it is characterized in that: raw material that magnetic coating is used and proportioning are:
Material composition content w/%
High molecular polymer 50~70
Magnetisable material 20~30
Coalescents 1.0~10
Dispersant 1.0~10
Defoamer 0.1~1.0
The deionized water surplus
Its process for preparation is: after each raw material is taken by weighing, mix, normal temperature can obtain magnetic coating after stirring 20min down.
4. require the preparation method of 1 described a kind of magnetic pearl nucleus according to patent, it is characterized in that: used high molecular polymer is aqueous epoxy resins, acrylic emulsion or benzene emulsion.
5. require the preparation method of 1 described a kind of magnetic pearl nucleus according to patent, it is characterized in that: used magnetisable material is di-iron trioxide (γ-Fe 2O 3) or four oxidations, three (Fe 3O 4) magnetic.
6. require the preparation method of 1 described a kind of magnetic pearl nucleus according to patent, it is characterized in that magnetic coating evenly is coated on free radical nuclear surface, 60~70 ℃ of baking and curing form light, circular, and coating layer thickness is the magnetic pearl nucleus of 0.1~1.0mm.
CN201010208002A 2010-06-14 2010-06-14 Preparation method for magnetic pearl nucleus Pending CN101869084A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201010208002A CN101869084A (en) 2010-06-14 2010-06-14 Preparation method for magnetic pearl nucleus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201010208002A CN101869084A (en) 2010-06-14 2010-06-14 Preparation method for magnetic pearl nucleus

Publications (1)

Publication Number Publication Date
CN101869084A true CN101869084A (en) 2010-10-27

Family

ID=42994317

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201010208002A Pending CN101869084A (en) 2010-06-14 2010-06-14 Preparation method for magnetic pearl nucleus

Country Status (1)

Country Link
CN (1) CN101869084A (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103299940A (en) * 2013-06-26 2013-09-18 千足珍珠集团股份有限公司 Method for culturing nucleated pearls
CN105284677A (en) * 2015-10-05 2016-02-03 王小凤 Pearl nucleus soak solution capable of breeding large-grained nucleated pearl
CN106106277A (en) * 2016-06-29 2016-11-16 广东海洋大学 A kind of manufacture method of magnetic pearl nucleus
CN107286791A (en) * 2017-08-09 2017-10-24 临海市绿邦水性涂料有限公司 A kind of paint film can be by water paint of magnet adsorption and preparation method thereof
CN108504227A (en) * 2018-03-29 2018-09-07 广州新莱福磁电有限公司 A kind of aqueous magnet board coating and preparation method thereof
CN111171659A (en) * 2020-02-24 2020-05-19 四会市中日化工实业有限公司 Water-based environment-friendly paint for automobile exterior and preparation method thereof
CN116584423A (en) * 2023-05-08 2023-08-15 广东海洋大学 Preparation method of bluish violet pearl nuclei

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS57152837A (en) * 1981-03-18 1982-09-21 Mitsubishi Steel Mfg Breeding of pearl shellfish and magnetic cage for breeding same
JP2004024062A (en) * 2002-06-24 2004-01-29 Matsushita Pearl Co Ltd Pearl breeding method
WO2005012425A1 (en) * 2003-07-31 2005-02-10 Mitsubishi Rayon Co., Ltd. Resin composition for molding material and molded article made therefrom
CN101243777A (en) * 2008-03-13 2008-08-20 苏州市珍妮日用化工有限公司 Noctilucence pearl cultivating method

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS57152837A (en) * 1981-03-18 1982-09-21 Mitsubishi Steel Mfg Breeding of pearl shellfish and magnetic cage for breeding same
JP2004024062A (en) * 2002-06-24 2004-01-29 Matsushita Pearl Co Ltd Pearl breeding method
WO2005012425A1 (en) * 2003-07-31 2005-02-10 Mitsubishi Rayon Co., Ltd. Resin composition for molding material and molded article made therefrom
CN101243777A (en) * 2008-03-13 2008-08-20 苏州市珍妮日用化工有限公司 Noctilucence pearl cultivating method

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103299940A (en) * 2013-06-26 2013-09-18 千足珍珠集团股份有限公司 Method for culturing nucleated pearls
CN103299940B (en) * 2013-06-26 2014-09-03 千足珍珠集团股份有限公司 Method for culturing nucleated pearls
CN105284677A (en) * 2015-10-05 2016-02-03 王小凤 Pearl nucleus soak solution capable of breeding large-grained nucleated pearl
CN106106277A (en) * 2016-06-29 2016-11-16 广东海洋大学 A kind of manufacture method of magnetic pearl nucleus
CN107286791A (en) * 2017-08-09 2017-10-24 临海市绿邦水性涂料有限公司 A kind of paint film can be by water paint of magnet adsorption and preparation method thereof
CN108504227A (en) * 2018-03-29 2018-09-07 广州新莱福磁电有限公司 A kind of aqueous magnet board coating and preparation method thereof
CN111171659A (en) * 2020-02-24 2020-05-19 四会市中日化工实业有限公司 Water-based environment-friendly paint for automobile exterior and preparation method thereof
CN111171659B (en) * 2020-02-24 2024-02-06 四会市中日化工实业有限公司 Water-based environment-friendly paint for automobile exterior and preparation method thereof
CN116584423A (en) * 2023-05-08 2023-08-15 广东海洋大学 Preparation method of bluish violet pearl nuclei
CN116584423B (en) * 2023-05-08 2024-05-10 广东海洋大学 Preparation method of bluish violet pearl nuclei

Similar Documents

Publication Publication Date Title
CN101869084A (en) Preparation method for magnetic pearl nucleus
CN104224685B (en) Facial mask liquid and preparation method thereof
CN105969046A (en) Disease-suppression antibacterial beautiful sealant and preparation technology thereof
WO2016004792A1 (en) Controllable color-changing foundation cream/liquid foundation
KR101020874B1 (en) Capsulation composition of algae spores for promoting attachment and growth of marine organisms
CN101861842A (en) Method for preparing special pearl nuclei for cultivating blister pearls
CN104710717B (en) Macromolecule clay material
CN108300031A (en) A kind of interior wall multi-functional environment-protection texture coating and its preparation process
CN105367000B (en) A kind of liquid diatom ooze wall material and preparation method thereof
CN106893467A (en) A kind of preparation method of fibroin aqueous polyurethane nano composite water-proof leather finishing agent
CN107619076A (en) The formula of the special water purification agent of aquaculture class
CN102732075A (en) Wood putty and preparation method thereof
CN107236431A (en) A kind of nano wall covering
CN107118670A (en) A kind of interior wall environment friendly emulsion paint and preparation method thereof
CN102764726A (en) Beewax spraying method
CN107628778A (en) A kind of preparation technology of multifunctional room interior finish material
CN109206958A (en) A kind of gloss oil and preparation method thereof for discharging anion
CN1204059C (en) Oxygen-supplying body and preparing method thereof
CN104278020A (en) Microbial water purifying agent for weever farming water and preparation method of microbial water purifying agent
CN109354210A (en) A kind of complex microorganism water purification agent and its application
CN103784366B (en) A kind of bamboo charcoal grey black nial polish
CN104446205A (en) Technical clay with solidifiable capacity at room temperature and preparation method of technical clay
CN106726777A (en) A kind of water-based nail polish base bond material and preparation method thereof
KR100257084B1 (en) Manufacturing method of resistance mushroom bath
CN109988475A (en) A kind of skin texture wall film and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20101027