CN107353664A - A kind of edible packing membrane based on sargassan - Google Patents
A kind of edible packing membrane based on sargassan Download PDFInfo
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- CN107353664A CN107353664A CN201710544865.8A CN201710544865A CN107353664A CN 107353664 A CN107353664 A CN 107353664A CN 201710544865 A CN201710544865 A CN 201710544865A CN 107353664 A CN107353664 A CN 107353664A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L99/00—Compositions of natural macromolecular compounds or of derivatives thereof not provided for in groups C08L89/00 - C08L97/00
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D65/00—Wrappers or flexible covers; Packaging materials of special type or form
- B65D65/38—Packaging materials of special type or form
- B65D65/46—Applications of disintegrable, dissolvable or edible materials
- B65D65/463—Edible packaging materials
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/18—Manufacture of films or sheets
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2399/00—Characterised by the use of natural macromolecular compounds or of derivatives thereof not provided for in groups C08J2301/00 - C08J2307/00 or C08J2389/00 - C08J2397/00
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2405/00—Characterised by the use of polysaccharides or of their derivatives not provided for in groups C08J2401/00 or C08J2403/00
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/06—Biodegradable
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/16—Applications used for films
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
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- General Health & Medical Sciences (AREA)
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- Biochemistry (AREA)
- General Preparation And Processing Of Foods (AREA)
Abstract
The present invention discloses a kind of edible packing membrane based on sargassan, and the composition and parts by weight of packaging film are：The weight ratio of 56 82 parts of flour, 20 38 parts of sargassan, 2 10 parts of sucrose, 0.2 0.3 parts of active peptides, 2 10 parts of vegetables, 5 15 parts of egg, 10 25 parts of chitosan, 2 10 parts of water, sargassan and sucrose is 2 ~ 15:1；The present invention uses the material of people's daily consumption as packaging film raw material, the packaging film of preparation can be used as food, pharmaceutical packing film, with good instant capacity and mechanicalness, packaging film can also allay one's hunger as food, packaging film is used for the free radical that food surface can be removed when fresh vegetables or meat products, delay food oxidization time, be advantageous to extend the freshness date and quality of food.
Description
Technical field
The present invention relates to a kind of edible packing membrane, more particularly to a kind of edible packaging based on sargassan
Film.
Background technology
Polysaccharide membrane is made up with various polysaccharide (such as starch, chitosan, cellulose, sodium alginate, colloid) of primary raw material,
It is that one kind is studied and application is than edible packing membrane earlier, has the characteristics that transparency is good, intensity is high.Polysaccharide film chemistry
Stable, suitable for long-time storage, but water preventing ability is typically poor.Albuminous membranae with vegetable protein (such as soybean protein, zein,
Wheat gluten protein etc.) and animal protein (such as lactalbumin, albumen, fish myofibrillar protein) be raw material, pass through
Disulfide bond and more skin chains crosslinking film forming.Albuminous membranae is easy to digest, being rich in nutrition, good mechanical property, and with excellent oxygen, two
Carbonoxide and grease barrier property, but water preventing ability is poor.Lipid film can by sources be divided into vegetable oil type film, animal adipose membrane and wax
For three kinds of type film due to the low pole of raw material, lipid film has good water preventing ability.But during the independent film forming of lipid material, film uniformity
Poor, mechanical performance and transparency be not high, and easily produces wax taste and bad mouthfeel.At present, generally using lipid material as helping
Agent is used in combination with polysaccharide or protein.Composite membrane is mixed to form by polysaccharide, protein, lipid.By specifically matching combination,
Composite membrane can better profit from the property of various raw materials, composite membrane is had wider feature, meet different food products
The needs of packaging, and also have certain research to composite package film application both at home and abroad.
Prior art such as Chinese invention granted patent document, Authorization Notice No.：The A of application publication number CN 101885861, should
A kind of edible package film of disclosure of the invention and its production and use, it includes the flour of 50-85 parts by weight, and 2-10
The sucrose of parts by weight, the vegetables of 2-10 parts by weight, the egg of 5-15 parts by weight, and the water of 2-10 parts by weight, by upper
The raw material mixed grinding of ratio is stated into being film-made after paste material.The edible package film outward appearance similar to plastic sheeting, can 70~
Dissolved in 100 DEG C of water, it is edible, available for packaging for making the inner packaging materials of various food, Some Drugs etc., to human body
Health is harmless, and has certain nutritive value.With instant capacity, heat is instant, meets water changes, and can be kept when heat does not meet water
Good mechanical performance.And its technique is simple, low manufacture cost, but the packaging film is delaying the Food Oxidation degree of cladding
Aspect is not ideal, is unfavorable for guaranteeing the quality, being fresh-keeping for food.
The content of the invention
It is an object of the invention to provide a kind of edible packing membrane based on sargassan, has good instant capacity
And mechanical performance, it is degradable in natural environment, the oxidation of packaged food can be delayed, remove the free radical of food surface, can be carried
The fresh-keeping effect of high food, extends the shelf life.
To achieve the above object, the scheme taken is the present invention：A kind of edible packing membrane based on sargassan,
The composition and parts by weight of packaging film be：Flour 56-82 parts, sargassan 20-38 parts, sucrose 2-10 parts, active peptides 0.2-
0.3 part, vegetables 2-10 parts, egg 5-15 parts, chitosan 10-25 parts, water 2-10 parts, the weight ratio of sargassan and sucrose is
2~15:1；The amino acid sequence of active peptides is：
MKTVRVAAAVALLFAFVWIQESSAQADAQMEEMEGPEDVDIPVELKVEEVVDAMSSYSRAKRGLKCKLRCRL；Vegetables
One or more in being spent for spinach, green vegetables, celery, carrot, tomato, western indigo plant, the present invention use the material of people's daily consumption
Expect that, to pack film raw material, the packaging film of preparation can be used as food, pharmaceutical packing film, have good instant capacity and mechanicalness,
Packaging film can also allay one's hunger as food, and packaging film is used for the free radical that food surface can be removed when fresh vegetables or meat products,
Delay food oxidization time, be advantageous to extend food freshness date and quality, the active peptides added in packaging film have compared with
Strong removing removes free radical, prevents the effect of lipid peroxidation, and rice protein antioxidation tripe has stronger removing DPPH certainly
By base, hydroxyl radicals, active peptides are to Fe2+Acted on certain chelant, delay Food Oxidation, by controlling sargassum
Instant capacity and degradation speed of the weight of polysaccharide and sucrose than that can significantly increase packaging film, advantageously reduce environmental pollution.
The preparation method of edible packing membrane based on sargassan is：
1）The extraction of sargassan：Sargassum powder is taken, adds deionized water, sargassum powder and deionized water in mass ratio
Ratio be 1:20, refluxing extraction, refluxing extraction temperature is 80 ~ 83 DEG C, and extraction time is 7 ~ 9h, and leaching liquor is centrifuged, taken
Clear liquid, sediment add deionized water, refluxing extraction, leaching liquor centrifugation, take supernatant, merge supernatant, revolving, add ethanol,
The alcohol liquor ratio of supernatant and ethanol is 3 ~ 3.5:1, refrigerated overnight, centrifugation, taking precipitate, freeze-drying, obtain sargassan；
2）By weight, take flour to be mixed into pasty state with water, obtain paste, in vegetables plus water is squeezed the juice, and adds sucrose, chitosan
After mixing, sequentially add paste, egg, sargassan, active peptides and be ground into slurry, be put into and make film mechanism film, edibility bag
The thickness for filling film is 0.1mm-0.5mm, and the edible packing membrane prepared by the above method has excellent instant capacity and machinery
Performance, it is degradable in natural environment, the oxidation of packaged food can be delayed, remove the free radical of food surface, food can be improved
Fresh-keeping effect, the sargassan of addition is soluble in water, viscosity is higher, coagulation ability is strong, strengthens the mechanical strength of packaging film,
The content of iodine of packaging film is improved, the mouthfeel of packaging film is greatly improved.
Compared with prior art, beneficial effects of the present invention are：1）The present invention uses the material of people's daily consumption as bag
Film raw material is filled, the packaging film of preparation can be used as food, pharmaceutical packing film, have good instant capacity and mechanicalness, packaging film
It can also be allayed one's hunger as food；2）Packaging film is used for the free radical that food surface can be removed when fresh vegetables or meat products, delays
Food oxidization time, be advantageous to extend the freshness date and quality of food；3）The sargassan that is added in packaging film is soluble in water,
Viscosity is higher, coagulation ability is strong, strengthens the mechanical strength of packaging film, improves the content of iodine of packaging film, also makes the mouthfeel of packaging film
It is greatly improved；4）The raw material of packaging film are simple and easy to get, and cost is cheap, and preparation method is simple, easily realize batch production.
Embodiment
The solution of the present invention is described in further detail by the following examples：
Embodiment 1：
A kind of edible packing membrane based on sargassan, the composition and parts by weight of packaging film are：62 parts of flour, sargassum are more
Sugar 32 parts, 8 parts of sucrose, 0.24 part of active peptides, 7 parts of vegetables, 10 parts of egg, 18 parts of chitosan, 6 parts of water, sargassan with
The weight ratio of sucrose is 4:1；The amino acid sequence of active peptides is：
MKTVRVAAAVALLFAFVWIQESSAQADAQMEEMEGPEDVDIPVELKVEEVVDAMSSYSRAKRGLKCKLRCRL；Vegetables
For spinach, green vegetables, celery, carrot.
A kind of preparation method of the edible packing membrane based on sargassan is：
1）The extraction of sargassan：Sargassum powder is taken, adds deionized water, sargassum powder and deionized water in mass ratio
Ratio be 1:20, refluxing extraction, refluxing extraction temperature is 82 DEG C, extraction time 7.1h, leaching liquor is centrifuged（5000r/
Min, 10min）, supernatant is taken, sediment adds deionized water（1:20）, refluxing extraction, refluxing extraction temperature is 82 DEG C, during extraction
Between be 7.1h, leaching liquor centrifugation（5000r/min, 10min）, supernatant is taken, merges supernatant, 50 DEG C of revolvings are sent to 1/4 volume,
The alcohol liquor ratio of addition ethanol, supernatant and ethanol is 3:1, refrigerated overnight, centrifugation（5000r/min, 10min）, taking precipitate is cold
It is lyophilized dry, obtain sargassan；
2）By weight, take flour to be mixed into pasty state with water, obtain paste, in vegetables plus water is squeezed the juice, and adds sucrose, chitosan
After mixing, paste, egg are sequentially added（The egg white of egg is 2 with yolk ratio:1）, sargassan, active peptides are ground into
Slurry, is put into and makes film mechanism film, the thickness of edible packing membrane is 0.3mm.
Embodiment 2：
A kind of edible packing membrane based on sargassan, the composition of packaging film and preferred weight part are：59 parts of flour, horse hair
20 parts of polysaccharides, 10 parts of sucrose, 0.2 part of active peptides, 6 parts of vegetables, 10 parts of egg, 18 parts of chitosan, 8 parts of water, sargassum is more
The weight ratio of sugar and sucrose is 2:1；The amino acid sequence of active peptides is：
MKTVRVAAAVALLFAFVWIQESSAQADAQMEEMEGPEDVDIPVELKVEEVVDAMSSYSRAKRGLKCKLRCRL；Vegetables
For spinach, celery, tomato, Xi Lanhua.
A kind of preparation method of the edible packing membrane based on sargassan is：
1）The extraction of sargassan：Sargassum powder is taken, adds deionized water, sargassum powder and deionized water in mass ratio
Ratio be 1:20, refluxing extraction, refluxing extraction temperature is 82 DEG C, extraction time 7.1h, leaching liquor is centrifuged（5000r/
Min, 10min）, supernatant is taken, sediment adds deionized water（1:20）, refluxing extraction, refluxing extraction temperature is 81.75 DEG C, is carried
It is 7.91h to take the time, and leaching liquor centrifuges（5000r/min, 10min）, supernatant is taken, merges supernatant, 50 DEG C of revolvings are sent to 1/4
The alcohol liquor ratio of volume, addition ethanol, supernatant and ethanol is 3.19:1, refrigerated overnight, centrifugation（5000r/min, 10min）, take
Sediment, freeze-drying, obtains sargassan；
2）By weight, take flour to be mixed into pasty state with water, obtain paste, in vegetables plus water is squeezed the juice, and adds sucrose, chitosan
After mixing, paste, egg are sequentially added（The egg white of egg is 2 with yolk ratio:1）, sargassan, active peptides are ground into
Slurry, is put into and makes film mechanism film, the thickness of edible packing membrane is 0.2mm.
The performance of edible packing membrane prepared for the checking present invention, inventor is by packaging film manufactured in the present embodiment and city
Conventional packaging film on field（0.2mm）Tested, contrast experiment, test result is as follows：
| Thickness mm | Transparency T%.mm | Solubility mg/h | Vapor transmission coefficient（g·mm）/（m2·d·KP2） | Tensile strength MPa | |
| The packaging film of the present embodiment | 0.2 | 15.62 | 1.91 | 5.27 | 11.71 |
| Market routine packaging film | 0.2 | 14.34 | 1.82 | 5.01 | 10.38 |
Shown by above-mentioned comparative experimental data, the performance of the edible packing membrane of the invention based on sargassan is better than normal
Packaging film is advised, there is good using effect.
Routine operation in the operating procedure of the present invention is well known to those skilled in the art, herein without repeating.
Technical scheme is described in detail embodiment described above, it should be understood that it is described above only
For the specific embodiment of the present invention, it is not intended to limit the invention, all any modifications made in the spirit of the present invention,
Supplement or similar fashion replacement etc., should be included in the scope of the protection.
SEQUENCE LISTING
<110>Pujiang County Ou Li Bioisystech Co., Ltd
<120>A kind of edible packing membrane based on sargassan
<130> 1
<160> 1
<170> PatentIn version 3.5
<210> 1
<211> 72
<212> PRT
<213>It is artificial synthesized
<400> 1
Met Lys Thr Val Arg Val Ala Ala Ala Val Ala Leu Leu Phe Ala Phe
1 5 10 15
Val Trp Ile Gln Glu Ser Ser Ala Gln Ala Asp Ala Gln Met Glu Glu
20 25 30
Met Glu Gly Pro Glu Asp Val Asp Ile Pro Val Glu Leu Lys Val Glu
35 40 45
Glu Val Val Asp Ala Met Ser Ser Tyr Ser Arg Ala Lys Arg Gly Leu
50 55 60
Lys Cys Lys Leu Arg Cys Arg Leu
65 70
Claims (7)
- A kind of 1. edible packing membrane based on sargassan, it is characterised in that：The composition and parts by weight of the packaging film be： Flour 56-82 parts, sargassan 20-38 parts, sucrose 2-10 parts, active peptides 0.2-0.3 parts, vegetables 2-10 parts, egg 5- 15 parts, chitosan 10-25 parts, water 2-10 parts, the weight ratio of the sargassan and sucrose is 2 ~ 15:1.
- A kind of 2. edible packing membrane based on sargassan according to claim 1, it is characterised in that：The activity is more The amino acid sequence of peptide is：MKTVRVAAAVALLFAFVWIQESSAQADAQMEEMEGPEDVDIPVELKVEEVVDAMSSYSRA KRGLKCKLRCRL。
- A kind of 3. edible packing membrane based on sargassan according to claim 1, it is characterised in that：The vegetables One or more in being spent for spinach, green vegetables, celery, carrot, tomato, western indigo plant.
- A kind of 4. edible packing membrane based on sargassan according to claim 1, it is characterised in that：It is described to be based on The preparation method of the edible packing membrane of sargassan is：1）The extraction of sargassan：Take sargassum powder, add deionized water in mass ratio, refluxing extraction, by leaching liquor from The heart, takes supernatant, and sediment adds deionized water, refluxing extraction, leaching liquor centrifugation, takes supernatant, merges supernatant, revolving, add Enter ethanol, refrigerated overnight, centrifugation, taking precipitate, freeze-drying, obtain sargassan；2）By weight, take flour to be mixed into pasty state with water, obtain paste, in vegetables plus water is squeezed the juice, and adds sucrose, chitosan After mixing, sequentially add paste, egg, sargassan, active peptides and be ground into slurry, be put into and make film mechanism film.
- A kind of 5. edible packing membrane based on sargassan according to claim 4, it is characterised in that：The step The ratio of sargassum powder and deionized water is 1 in 1:20, refluxing extraction temperature is 80 ~ 83 DEG C, and extraction time is 7 ~ 9h.
- A kind of 6. edible packing membrane based on sargassan according to claim 4, it is characterised in that：The step The alcohol liquor ratio of supernatant and ethanol in 1 is 3 ~ 3.5:1.
- A kind of 7. edible packing membrane based on sargassan according to claim 1, it is characterised in that：It is described edible The thickness of property packaging film is 0.1mm-0.5mm.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107892819A (en) * | 2017-11-29 | 2018-04-10 | 金华市铁骑士生物科技有限公司 | The preparation method of edible packing membrane based on leucosin |
| CN109181321A (en) * | 2018-09-20 | 2019-01-11 | 吴亚琴 | A kind of preparation method of antibacterial mould-proof-type edible membrane material |
| CN110305371A (en) * | 2019-07-06 | 2019-10-08 | 李光宽 | A kind of sargassan food product packing film and preparation method thereof |
| CN114455204A (en) * | 2022-01-17 | 2022-05-10 | 黑龙江省绿色食品科学研究院 | Preparation method of edible composite blood pressure lowering polypeptide packaging film |
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| CN101906220A (en) * | 2010-07-16 | 2010-12-08 | 山东农业大学 | Starch-based edible film and preparation method thereof |
| CN102303747A (en) * | 2011-05-19 | 2012-01-04 | 郑正炯 | Preparation method for edible and soluble composite film packing material |
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| US4994285A (en) * | 1986-10-22 | 1991-02-19 | Asahi Kasei Kogyo Kabushiki Kaisha | Edible body and process for preparation thereof |
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| CN102303747A (en) * | 2011-05-19 | 2012-01-04 | 郑正炯 | Preparation method for edible and soluble composite film packing material |
| CN104893003A (en) * | 2015-05-25 | 2015-09-09 | 苏州市贝克生物科技有限公司 | Polysaccharide based edible film and preparation method and application thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107892819A (en) * | 2017-11-29 | 2018-04-10 | 金华市铁骑士生物科技有限公司 | The preparation method of edible packing membrane based on leucosin |
| CN109181321A (en) * | 2018-09-20 | 2019-01-11 | 吴亚琴 | A kind of preparation method of antibacterial mould-proof-type edible membrane material |
| CN110305371A (en) * | 2019-07-06 | 2019-10-08 | 李光宽 | A kind of sargassan food product packing film and preparation method thereof |
| CN114455204A (en) * | 2022-01-17 | 2022-05-10 | 黑龙江省绿色食品科学研究院 | Preparation method of edible composite blood pressure lowering polypeptide packaging film |
| CN114455204B (en) * | 2022-01-17 | 2023-09-29 | 黑龙江省绿色食品科学研究院 | Preparation method of composite antihypertensive polypeptide edible packaging film |
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