CN104432490B - A kind of manaca extract and the application in cigarette - Google Patents
A kind of manaca extract and the application in cigarette Download PDFInfo
- Publication number
- CN104432490B CN104432490B CN201410667945.9A CN201410667945A CN104432490B CN 104432490 B CN104432490 B CN 104432490B CN 201410667945 A CN201410667945 A CN 201410667945A CN 104432490 B CN104432490 B CN 104432490B
- Authority
- CN
- China
- Prior art keywords
- manaca
- cigarette
- extract
- filtrate
- filter
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a kind of manaca extract, it comprises by manaca through peeling crushing and beating, and add 85wt% ~ 95wt% ethanol water of its weight 4 times amount, add hot reflux 2h, filter while hot, filter residue is used for next step, and filtrate retains; In filter residue, add the 30wt% ethanol water of its weight 5 times amount, add hot reflux 2h, after filtering while hot, by filtrate reduced in volume, obtain concentrate A; Filtered with leaving standstill at initial filtrate mixing is placed on 0 DEG C by concentrate A, filtrate reduced in volume obtains weak yellow liquid and is manaca extract.This preparation method is simple and practical, and operation is implemented easily, and gained manaca extract can be sprayed onto on cigarette shreds, and rolls into cigarette, can effectively improve cigarette pleasant impression, improves cigarette sweet moisture feeling, makes flue gas fine and smooth, increases cigarette flavor concentration.
Description
Technical field
The invention belongs to cigarette additive technical field, be specifically related to a kind of preparation method of manaca extract, the invention still further relates to the application of described manaca extract in cigarette simultaneously.
Background technology
Along with developing rapidly of science and technology and improving constantly of health of people consciousness, various natural product joins in cigarette by increasing tobacco enterprise, thus reaches the effect that safety non-toxic improves cigarette quality and mouthfeel harmfully.
Manaca, also known as Sakyamuni, be a kind of tropical fruit (tree), fruit is fresh and sweet, and the snow-white mouthfeel of pulp is careful, and the micro-acid of the fragrant and sweet point of band again, local flavor is excellent.Every 100 grams of manaca pulp contain: moisture is 8.36 grams, soluble solid is 18.0wt% ~ 26.0wt%, and fat is 0.14wt% ~ 0.3wt%, and mineral matter is 0.6wt% ~ 0.7wt%, carbohydrate is 23.9wt%, calcium is 0.2wt%, and phosphorus is 0.04wt%, and iron is 1.0wt%, organic acid is 0.42wt%, total reducing sugar is 15.3wt% ~ 18.3wt%, and vitamin C is 0.265 gram, and protein is 1.55 grams.Manaca contains abundant vitamin C, has hypoglycemic effect, is also best anti-oxidant fruit, can effective delaying skin aging, skin whitening; Manaca fiber content is higher, effectively can promote enterocinesia.Manaca extract effectively can resist 12 kinds of malignant cells simultaneously.
Research for manaca mainly concentrates on the active anticancer aspect of Annona lactone now, and its extract is used for tobacco business, and there is not been reported.Be that development of raw materials develops new high-grade cigarette additive with manaca, the suction quality of cigarette can be improved, expand its application in cigarette, wide market prospects will be had.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of manaca extract and the application in cigarette.
The present invention also aims to described manaca extract joins in the pipe tobacco of production process, can effectively improve cigarette pleasant impression, improves cigarette sweet moisture feeling, makes flue gas fine and smooth, increases cigarette flavor concentration.
Object of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage of the present invention is percetage by weight.
A first aspect of the present invention relates to a kind of preparation method of manaca extract, and it comprises the following steps:
(1) manaca after clean peeling is broken into pulpous state;
(2) in manaca slurry, add 85wt% ~ 95wt% ethanol water of its weight 4 times amount, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, filter residue is used for next step, and filtrate retains for subsequent use;
(3) in the filter residue in step (2), add the 30wt% ethanol water of its weight 5 times amount, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, it is 1.200 ± 0.006g/cm that gained filtrate is evaporated to density at 40 ± 2 DEG C
3, obtain concentrate A;
(4) step (3) gained concentrate A is mixed with step (2) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 0.920 ± 0.006g/cm that filtrate is evaporated to density at 40 DEG C
3, gained weak yellow liquid is cigarette manaca extract.
In the preferred embodiment of a first aspect of the present invention, in step (3), the filter residue in step (2) is repeatedly leached with the 30wt% ethanol water of its weight 5 times amount, and be heated to 90 ± 2 DEG C of backflow 2h, then filter while hot, at 40 ± 2 DEG C, being evaporated to density after the filtrate at every turn obtained being merged is 1.200 ± 0.006g/cm
3, obtain concentrate A.Step (4) is afterwards still identical.
A second aspect of the present invention relates to the manaca extract prepared by the preparation method of manaca extract described in above-mentioned first aspect.
A third aspect of the present invention relates to the purposes of manaca extract in cigarette according to second aspect.This manaca extract can be applicable to production of cigarettes, does not need to change cigarette original processing technology during application, can directly be added in cigarette shreds by manaca extract.Concrete grammar is: after manaca extract is diluted 4 times of weight with the amount ultra-pure water of cigarette shreds weight 0.3wt%, be sprayed onto on cigarette shreds, prepare cigarette in existing mode in the mode of spraying.
A fourth aspect of the present invention relates to the pipe tobacco comprising described manaca extract.This pipe tobacco can be used for preparation tradition and lights type cigarette or prepare electric heating type cigarette.
The cigarette and the blank cigarette that add manaca extract carry out sensory evaluating smoking, and smoking result shows, manaca extract of the present invention can improve cigarette pleasant impression, improve cigarette sweet moisture feeling, make flue gas fine and smooth, improve cigarette flavor concentration.
Accompanying drawing explanation
Nothing
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, but embodiment is not limited to the technical solution.
Embodiment 1
(1) accurately take the manaca after 2kg peeling, put in juice extractor fragmentation of pulling an oar and obtain manaca slurry.
(2) soaked with the 85wt% ethanol water of its weight 4 times amount by manaca slurry, reflux 2h at temperature 90 DEG C, filters while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(3) the 30wt% ethanol water adding its weight 5 times amount to the filter residue in step (2) leaches, be heated to 90 ± 2 DEG C of backflow 2h, after filtering while hot, repeat this leaching-Jia hot reflux-filtration step several times while hot to filter residue, at 40 ± 2 DEG C, being evaporated to density after merging the filtrate at every turn obtained is 1.200 ± 0.006g/cm
3, obtain concentrate A;
(4) step (3) gained concentrate A is mixed with step (2) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 0.920 ± 0.006g/cm that filtrate is evaporated to density at 40 DEG C
3, obtain weak yellow liquid 398g, be cigarette manaca extract.
Embodiment 2
(1) accurately take the manaca after 2kg peeling, put in juice extractor fragmentation of pulling an oar and obtain manaca slurry.
(2) soaked with the 95wt% ethanol water of its weight 4 times amount by manaca slurry, reflux 2h at temperature 90 DEG C, filters while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(3) the 30wt% ethanol water of its weight 5 times amount is added to the filter residue in step (2), be heated to 90 ± 2 DEG C of backflow 2h, after filtering while hot, repeat this leaching-Jia hot reflux-filtration step several times while hot to filter residue, at 40 ± 2 DEG C, being evaporated to density after merging the filtrate at every turn obtained is 1.200 ± 0.006g/cm
3, obtain concentrate A;
(4) step (3) gained concentrate A is mixed with step (2) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 0.920 ± 0.006g/cm that filtrate is evaporated to density at 40 DEG C
3, obtain weak yellow liquid 411g, be cigarette manaca extract.
Manaca extract in above-described embodiment is used for cloud and mist tobacco leaf formulation, manaca extract is got by the 0.3wt% of cigarette shreds weight, dilute with the ultra-pure water of 4 times of weight, then be sprayed onto on cigarette shreds in the mode of spraying, balance 48h under constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2wt%), roll into Cigarette.The cigarette of gained and blank cigarette transfer to specialty member of smoking carry out sense organ contrast smoke panel test, result is as follows:
Above content is the further description made the present invention in conjunction with concrete preferred embodiment.For general technical staff of the technical field of the invention, the obvious modification made without departing from the inventive concept of the premise, performance or purposes identical, all should be considered as protection scope of the present invention.
Claims (4)
1. a manaca extract, is characterized in that, it is prepared by the method comprised the following steps:
(1) manaca after clean peeling is broken into pulpous state;
(2) in manaca slurry, add 85wt% ~ 95wt% ethanol water of its weight 4 times amount, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, filter residue is used for next step, and filtrate retains for subsequent use;
(3) in the filter residue in step (2), add the 30wt% ethanol water of its weight 5 times amount, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, it is 1.200 ± 0.006g/cm that gained filtrate is evaporated to density at 40 ± 2 DEG C
3, obtain concentrate A;
(4) step (3) gained concentrate A is mixed with step (2) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 0.920 ± 0.006g/cm that filtrate is evaporated to density at 40 DEG C
3, gained weak yellow liquid is cigarette manaca extract.
2. manaca extract according to claim 1, it is characterized in that in step (3), the filter residue in step (2) repeatedly being leached with the 30wt% ethanol water of its weight 5 times amount, and filter while hot after being all heated to 90 ± 2 DEG C of backflow 2h, at 40 ± 2 DEG C, being evaporated to density after the filtrate at every turn obtained being merged is 1.200 ± 0.006g/cm. at every turn
3, obtain concentrate A.
3. the purposes of manaca extract according to claim 1 in cigarette, is characterized in that manaca extract to dilute with the amount ultra-pure water relative to cigarette shreds weight 0.3wt%, is then sprayed onto on cigarette shreds in the mode of spraying.
4. comprise the pipe tobacco of the manaca extract described in claim 1 or 2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410667945.9A CN104432490B (en) | 2014-11-20 | 2014-11-20 | A kind of manaca extract and the application in cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410667945.9A CN104432490B (en) | 2014-11-20 | 2014-11-20 | A kind of manaca extract and the application in cigarette |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104432490A CN104432490A (en) | 2015-03-25 |
| CN104432490B true CN104432490B (en) | 2016-03-09 |
Family
ID=52879836
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410667945.9A Active CN104432490B (en) | 2014-11-20 | 2014-11-20 | A kind of manaca extract and the application in cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104432490B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107201274B (en) * | 2017-06-13 | 2020-06-19 | 武汉黄鹤楼香精香料有限公司 | Method for extracting tobacco flavor by taking tamarind as raw material and application |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2007135976A (en) * | 2005-02-28 | 2009-04-10 | Нара Инститьют оф Сайенс энд Текнолоджи (JP) | METHOD FOR REDUCING THE CONTENT OF ALKALOIDS IN PLAN (OPTIONS), THE ISOLATED NUCLEIC ACID MOLECULE (OPTIONS), GENETICALLY MODIFIED PLANT (OPTIONS) AND THE PRODUCT IS BASED ABOUT THEM. |
| CN101575324B (en) * | 2009-05-15 | 2011-05-25 | 贵州正鑫药业有限公司 | Preparation method for extracting anticancer valid-position medicine SHIKEMOXIN from sweetsop |
| CN102754784B (en) * | 2012-08-08 | 2013-06-19 | 天宁香料（江苏）有限公司 | Method for preparing tamarind fruit extract and application of same in edible essence |
-
2014
- 2014-11-20 CN CN201410667945.9A patent/CN104432490B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN104432490A (en) | 2015-03-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103989244B (en) | A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof | |
| CN102499460B (en) | Extracting method for radix ophiopogonis extract and dark plum extract as well as cigarette containing radix ophiopogonis extract and dark plum extract | |
| CN103783660B (en) | The supercritical extraction method of flavor matter and application thereof in a kind of tobacco leaf fragment | |
| CN106820251A (en) | A kind of herbal tea cigarette | |
| CN106036982B (en) | A kind of preparation method and applications of cigarette bay leaf extract | |
| CN102423124A (en) | Tobacco sheet and preparation method thereof | |
| CN105686065A (en) | Tea tobacco and making method thereof | |
| CN101991182B (en) | Method for producing nontoxic and harmless tobacco leaves from low-grade tea leaves, tea dust and other tea raw materials by paper making method | |
| CN103783651A (en) | Application of supercritically-extracted aquilaria sinensis in tobacco reproduction technology with paper making method | |
| CN103666761A (en) | Carrot extract and application thereof in tobacco flavoring and charging | |
| CN101455442B (en) | Grape extractum and preparation method thereof and use thereof in cigarette performing | |
| CN101637303A (en) | Lemon extract, preparation method thereof and application thereof in cigarette flavoring | |
| CN100593565C (en) | Petroleum extracted sophora flower extractum and its application in perfuming cigarette | |
| CN103330282A (en) | Application of moringa oil in cigarette and cigarette containing moringa oil | |
| CN104432490B (en) | A kind of manaca extract and the application in cigarette | |
| CN101455440A (en) | Mango extractum and preparation method thereof and use thereof in cigarette perfuming | |
| CN105146740A (en) | Preparation method of raisin extract for cigarette and application of raisin extract in cigarette | |
| CN108949347A (en) | Increase the essence and its preparation method and application for heating the new cigarette flue gas moist feeling that do not burn | |
| CN104489916B (en) | The application of red currant extract in cigarette | |
| CN107361398A (en) | A kind of tea extraction in May and preparation method thereof and the application in cigarette | |
| CN104382226B (en) | Preparation method of burley tobacco extract | |
| CN104593150A (en) | Preparation method of mulberry extract and application of mulberry extract in cigarettes | |
| CN102657375B (en) | Method for preparing extract from traditional Chinese medicines and application of extract as tobacco additive | |
| CN104694254A (en) | Red ginseng extract, and preparation method and application thereof | |
| CN104498185A (en) | Carambola extract as well as preparation method and application of carambola extract in cigarettes |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |