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BR112016002360A2 - processo para a produção de um material de aerogel - Google Patents

processo para a produção de um material de aerogel

Info

Publication number
BR112016002360A2
BR112016002360A2 BR112016002360A BR112016002360A BR112016002360A2 BR 112016002360 A2 BR112016002360 A2 BR 112016002360A2 BR 112016002360 A BR112016002360 A BR 112016002360A BR 112016002360 A BR112016002360 A BR 112016002360A BR 112016002360 A2 BR112016002360 A2 BR 112016002360A2
Authority
BR
Brazil
Prior art keywords
hydrophobation
airgel material
gel
colloidal solution
producing
Prior art date
Application number
BR112016002360A
Other languages
English (en)
Inventor
Simmen Caroline
Koebel Matthias
Brunner Samuel
Zhao Shanyu
Original Assignee
Empa Eidgenoessische Mat & Forschungsanstalt
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Empa Eidgenoessische Mat & Forschungsanstalt filed Critical Empa Eidgenoessische Mat & Forschungsanstalt
Publication of BR112016002360A2 publication Critical patent/BR112016002360A2/pt

Links

Classifications

    • EFIXED CONSTRUCTIONS
    • E04BUILDING
    • E04BGENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
    • E04B1/00Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
    • E04B1/62Insulation or other protection; Elements or use of specified material therefor
    • E04B1/74Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
    • E04B1/76Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to heat only
    • E04B1/78Heat insulating elements
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/145Preparation of hydroorganosols, organosols or dispersions in an organic medium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/155Preparation of hydroorganogels or organogels
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/157After-treatment of gels
    • C01B33/158Purification; Drying; Dehydrating
    • C01B33/1585Dehydration into aerogels

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Architecture (AREA)
  • Acoustics & Sound (AREA)
  • Electromagnetism (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Silicon Compounds (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Thermal Insulation (AREA)

Abstract

resumo de patente de invenção para: "processo para a produção de um material de aerogel". processo para a produção de um material de aerogel, compreende as seguintes etapas: a) preparação de uma solução coloidal de óxido de silício em uma mistura alcoólica de solventes; b) desencadeamento da gelificação da solução coloidal através da adição de base, resultando um gel e opcionalmente envelhecimento do gel; c) hidrofobação do gel opcionalmente envelhecido; d) remoção da mistura de solventes através de secagem subcrítica, formando-se o material de aerogel. a solução coloidal de óxido de silício formada na etapa a) contém pelo menos um agente de hidrofobação que pode ser ativado cataliticamente com ácido, sendo que a proporção volumétrica do agente de hidrofobação na solução coloidal perfaz de 5 a 60 %. a hidrofobação na etapa c) é iniciada através da libertação ou adição de pelo menos um catalisador de hidrofobação que interage com o agente de hidrofobação.
BR112016002360A 2013-08-02 2014-07-28 processo para a produção de um material de aerogel BR112016002360A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP13179185.7A EP2832690A1 (de) 2013-08-02 2013-08-02 Verfahren zur Herstellung eines Aerogelmaterials
PCT/EP2014/066213 WO2015014813A1 (de) 2013-08-02 2014-07-28 Verfahren zur herstellung eines aerogelmaterials

Publications (1)

Publication Number Publication Date
BR112016002360A2 true BR112016002360A2 (pt) 2017-08-01

Family

ID=48917409

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112016002360A BR112016002360A2 (pt) 2013-08-02 2014-07-28 processo para a produção de um material de aerogel

Country Status (8)

Country Link
US (1) US20160258153A1 (pt)
EP (2) EP2832690A1 (pt)
JP (1) JP6449279B2 (pt)
KR (1) KR101813898B1 (pt)
CN (2) CN105555710A (pt)
AU (1) AU2014298538B2 (pt)
BR (1) BR112016002360A2 (pt)
WO (1) WO2015014813A1 (pt)

Families Citing this family (39)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106029760B (zh) * 2014-02-26 2020-08-21 日立化成株式会社 气凝胶
CH710694B1 (de) * 2015-02-04 2019-05-15 Rockwool Int Verfahren zur Herstellung eines Aerogels resp. eines Aerogel-Verbundwerkstoffs, sowie Aerogel resp. Aerogel-Verbundwerkstoff erhältlich nach dem Verfahren.
KR101789371B1 (ko) 2015-02-13 2017-10-23 주식회사 엘지화학 실리카 에어로겔 함유 블랑켓의 제조방법 및 이에 따라 제조된 실리카 에어로겔 함유 블랑켓
GB201502613D0 (en) * 2015-02-17 2015-04-01 Univ Newcastle Aerogels
DE102015211812A1 (de) 2015-06-25 2016-12-29 Wacker Chemie Ag Wirtschaftliches Verfahren zur Herstellung von organisch modifizierten Lyo- oder Aerogelen
EP3124443A1 (de) * 2015-07-28 2017-02-01 D. Swarovski KG Kontinuierliches sol-gel verfahren zur herstellung von quarzglas
KR101931569B1 (ko) 2015-11-03 2018-12-21 주식회사 엘지화학 소수성의 산화금속-실리카 복합 에어로겔의 제조방법 및 이로부터 제조된 소수성의 산화금속-실리카 복합 에어로겔
KR101774140B1 (ko) * 2016-01-19 2017-09-01 주식회사 엘지화학 에어로겔 시트의 제조방법 및 장치
KR101953371B1 (ko) * 2016-01-19 2019-02-28 주식회사 엘지화학 에어로겔 시트의 제조방법 및 장치
KR101962207B1 (ko) * 2016-02-17 2019-03-27 주식회사 엘지화학 에어로겔 시트를 포함하는 복합시트 제조방법 및 제조장치
KR101968648B1 (ko) * 2016-02-19 2019-04-12 주식회사 엘지화학 에어로겔 시트의 제조방법 및 장치
KR101962206B1 (ko) 2016-02-19 2019-03-27 주식회사 엘지화학 에어로겔 시트를 포함하는 복합시트 제조방법 및 제조장치
KR20170110993A (ko) 2016-03-24 2017-10-12 주식회사 엘지화학 실리카 에어로겔 제조시스템
FR3050013B1 (fr) * 2016-04-11 2019-08-02 Saint-Gobain Isover Fours et produits d'isolation pour fours
CH712479A1 (de) 2016-05-20 2017-11-30 Flumroc Ag Anlage und Verfahren zur Herstellung eines Aerogel-Verbundwerkstoffs und Aerogel-Verbundwerkstoff.
FR3053263B1 (fr) * 2016-07-04 2018-08-31 Keey Aerogrl Procede continu de fabrication d'un aerogel
PL3490954T3 (pl) 2016-07-29 2020-06-29 Evonik Operations Gmbh Sposób wytwarzania hydrofobowego materiału termoizolacyjnego zawierającego krzemionkę pirogeniczną
EP3281920A1 (de) * 2016-08-12 2018-02-14 D. Swarovski KG Kontinuierliches sol-gel-verfahren zur herstellung von silicathaltigen gläsern oder glaskeramiken
US11279622B2 (en) 2016-09-12 2022-03-22 Lg Chem, Ltd. Method for producing silica aerogel and silica aerogel produced thereby
KR101942474B1 (ko) * 2016-11-18 2019-01-25 주식회사 엘지화학 전가수분해된 알킬 폴리실리케이트의 합성방법
RU2759942C2 (ru) 2017-01-18 2021-11-18 Эвоник Оперейшенс ГмбХ Гранулированный теплоизоляционный материал и способ его получения
CN106955650A (zh) * 2017-04-01 2017-07-18 东华大学 一种三维多孔框架增强纤维气凝胶材料及其制备方法
DE102017209782A1 (de) 2017-06-09 2018-12-13 Evonik Degussa Gmbh Verfahren zur Wärmedämmung eines evakuierbaren Behälters
EP3498671A1 (en) * 2017-12-15 2019-06-19 EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt Superinsulating silica aerogel with high stiffness and density
CN111818994A (zh) * 2018-03-05 2020-10-23 赢创运营有限公司 生产气凝胶材料的方法
EP3597615A1 (en) 2018-07-17 2020-01-22 Evonik Operations GmbH Granular mixed oxide material and thermal insulating composition on its basis
JP7009673B2 (ja) 2018-07-17 2022-01-25 エボニック オペレーションズ ゲーエムベーハー ヒュームドシリカ造粒物に基づく断熱組成物、その製造方法およびその使用
WO2020016036A1 (en) 2018-07-18 2020-01-23 Evonik Operations Gmbh Process for hydrophobizing shaped insulation-material bodies based on silica at ambient pressure
CN111039583B (zh) * 2018-10-11 2022-10-11 卢孟磊 一种低成本快速制备微纳结构气凝胶膨胀珍珠岩的方法
DE102018128410A1 (de) * 2018-11-13 2020-05-14 Fraunhofer Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren zur Herstellung von Aerogelen und mit diesem erhältliche Aerogele
WO2020125956A1 (de) 2018-12-18 2020-06-25 Wacker Chemie Ag Verfahren zur herstellung abgerundeter gelpartikel
FR3094975B1 (fr) * 2019-04-10 2022-11-18 Keey Aerogel Procédé de synthèse d’un aérogel de silice hydrophobique de type « one pot » à partir d’un précurseur de silice
WO2021204815A1 (en) * 2020-04-06 2021-10-14 Empa Eidgenössische Materialprüfungs- Und Forschungsanstalt Silica aerogels
EP3896035A1 (en) * 2020-04-15 2021-10-20 EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt Silica aerogels and silica aerogel blankets
CN113563012B (zh) * 2020-04-29 2022-11-04 台湾气凝胶科技材料开发股份有限公司 御寒、隔热的疏水性气凝胶复合胶状物的制备方法及其相关产物
JP7577757B2 (ja) * 2020-04-30 2024-11-05 エボニック オペレーションズ ゲーエムベーハー アルカリ安定性の上昇したシリカエアロゲル
CH717558A1 (de) 2020-06-22 2021-12-30 Rockwool Int Aerogel-Verbundwerkstoffen, sowie Wärmedämmelement.
EP4177231A1 (de) 2021-11-03 2023-05-10 Evonik Operations GmbH Wärmedämmsysteme mit verbesserter kosteneffizienz
CN117510181B (zh) * 2023-11-07 2024-04-16 武汉中科先进材料科技有限公司 一种超疏水、增强型二氧化硅气凝胶毡及其制备方法

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2659155B2 (ja) * 1992-02-03 1997-09-30 松下電工株式会社 疎水性エアロゲルの製造方法
EP0585456B1 (en) * 1992-02-18 1997-05-07 Matsushita Electric Works Ltd Process for producing hydrophobic aerogel
US5565142A (en) 1992-04-01 1996-10-15 Deshpande; Ravindra Preparation of high porosity xerogels by chemical surface modification.
AU7655594A (en) 1993-08-31 1995-03-22 Basf Aktiengesellschaft Hydrophobic silicic acid aerogels
DE19631267C1 (de) 1996-08-02 1998-04-30 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen
DE19648798C2 (de) * 1996-11-26 1998-11-19 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen durch Oberflächenmodifikation des wäßrigen Gels (ohne vorherigen Lösungsmitteltausch) und anschließender Trocknung
JP3954842B2 (ja) * 2001-08-02 2007-08-08 株式会社アルバック 疎水性多孔質材料の製造方法
FR2849444B1 (fr) * 2002-12-30 2006-07-28 Rhodia Chimie Sa Procede de preparation d'un suspension de silice dans une matiere silicone eventuellement reticulable
BRPI0506438A (pt) * 2004-01-06 2006-12-26 Aspen Aerogels Inc aerogéis de ormosil contendo polimetacrilato ligado por silìcio
FR2873677B1 (fr) * 2004-07-29 2007-08-17 Armines Ass Pour La Rech Et Le Procede d'elaboration de serogels de silice hydrophobes
JP2007134420A (ja) * 2005-11-09 2007-05-31 Ulvac Japan Ltd 疎水性多孔質シリカ材料による構造物内部の埋め込み方法
US7999026B2 (en) * 2007-02-02 2011-08-16 Nissan Chemical Industries, Ltd. Reactive monomer-dispersed silica sol and production method thereof, and curable composition and cured article thereof
KR100848856B1 (ko) * 2007-03-27 2008-07-29 주식회사 넵 영구적 소수성을 갖는 에어로겔의 제조 방법 및 이로부터제조된 영구적 소수성을 갖는 에어로겔
KR100924781B1 (ko) * 2007-09-19 2009-11-03 주식회사 넵 영구적인 소수성을 갖는 고투광성 입상형 에어로겔제조방법 및 이로부터 제조된 입상형 에어로겔
CN101372337B (zh) * 2008-09-28 2010-12-08 厦门大学 共前驱体法常压干燥制备透明二氧化硅气凝胶的方法
CN101691227B (zh) * 2009-10-13 2011-10-12 厦门大学 二氧化硅气凝胶材料的制备方法
KR101187568B1 (ko) 2010-09-29 2012-10-04 한국에너지기술연구원 실리카 에어로겔 과립의 제조방법
JP5669617B2 (ja) * 2011-02-21 2015-02-12 株式会社トクヤマ エアロゲル及び該エアロゲルを用いた断熱材
FR2981341B1 (fr) 2011-10-14 2018-02-16 Enersens Procede de fabrication de xerogels
CN102951650B (zh) * 2012-08-31 2015-05-20 卢斌 一种快速制备SiO2气凝胶的常压干燥方法
CN105308123B (zh) * 2013-06-10 2019-03-29 日产化学工业株式会社 含有二氧化硅的树脂组合物及其制造方法以及含有二氧化硅的树脂组合物的成型品

Also Published As

Publication number Publication date
KR20160054462A (ko) 2016-05-16
CN114408931A (zh) 2022-04-29
WO2015014813A1 (de) 2015-02-05
JP2016530199A (ja) 2016-09-29
JP6449279B2 (ja) 2019-01-09
CN105555710A (zh) 2016-05-04
EP3027558A1 (de) 2016-06-08
AU2014298538A1 (en) 2016-02-25
EP2832690A1 (de) 2015-02-04
KR101813898B1 (ko) 2018-01-02
AU2014298538B2 (en) 2018-02-22
US20160258153A1 (en) 2016-09-08

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Legal Events

Date Code Title Description
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]
B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: EM VIRTUDE DO ARQUIVAMENTO PUBLICADO NA RPI 2472 DE 22-05-2018 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDO O ARQUIVAMENTO DO PEDIDO DE PATENTE, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.