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Synthesis and X-ray Structures of Polymeric Calcium Carboxylates

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Abstract

The reactions of calcium hydroxide with pivalic, 1-naphthoic, and 2-furancarboxylic acids afford the corresponding polymeric calcium carboxylates. Depending on the crystallization conditions, calcium pivalate is isolated as two different coordination polymers: [Ca3(Piv)6(DMF)2]n·0.635nC6H6·0.365nDMF (I) and [Ca(Рiv)(H2O)2.333(DMF)0.666]n·nРiv·0.333H2O (II). The synthesized calcium 1-naphthoate contains coordinated water molecules [Сa(Naph)2(H2O)2]n (III), and calcium furoate [Ca(Fur)2]n (IV) contains no ancillary ligands. The structures of compounds I–IV are determined by X-ray diffraction (XRD) (CIF files CCDC nos. 2342790–2342793, respectively). The structures of compounds I–III are characterized by the 1D polymeric structure, and compound IV is the 3D polymer.

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Funding

This work was supported by the Ministry of Science and Higher Education of the Russian Federation in the framework of the state assignment of the Kurnakov Institute of General and Inorganic Chemistry (Russian Academy of Sciences).

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Moscow, Russia

    A. S. Samulionis, J. K. Voronina, S. N. Melnikov, A. S. Gavronova, D. A. Utepova, N. V. Gogoleva, D. S. Yambulatov, S. A. Nikolaevskii, M. A. Kiskin & I. L. Eremenko

  2. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russia

    A. S. Goloveshkin

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  1. A. S. Samulionis
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  2. J. K. Voronina
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Dedicated to Professor V.P. Fedin in celebration of his 70th birthday

Translated by E. Yablonskaya

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Samulionis, A.S., Voronina, J.K., Melnikov, S.N. et al. Synthesis and X-ray Structures of Polymeric Calcium Carboxylates. Russ J Coord Chem 50, 757–767 (2024). https://doi.org/10.1134/S1070328424601043

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