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Directed ortho Metalation reaction of aryl O-carbamates on solid support.

Author information

Affiliations

  • 1. Department of Chemistry, Queen's University, Kingston, Ontario, Canada K7L 3N6.
      Authors
    • Milburn C 1
    (1 author)

Organic Letters, 01 Feb 2005, 7(4):629-631
https://doi.org/10.1021/ol0476220 PMID: 15704911 

Abstract 

The first Directed ortho Metalation (DoM) reaction of aryl O-carbamates on polystyrene-divinylbenzene (PS-DVB) resin using a trityl linker is described. Using low temperatures and short metalation times, a range of electrophiles have been introduced to give, after cleavage from support, substituted benzyl alcohols in high purity. [reaction: see text]

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Read article at publisher's site: https://doi.org/10.1021/ol0476220

Read article for free, from open access legal sources, via Unpaywall: http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp05/MQ63340.pdfUnpaywall

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