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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 239-242Facile Fabrication of Flower-Like LLM-105...

Facile Fabrication of Flower-Like LLM-105 Three-Dimensional Microstructures

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Abstract:

Flower-like LLM-105 three-dimensional microstructures, which consisted of LLM-105 microrods with rectangular cross-sections, were prepared via a smiple template- and surfactant-free recrystallization process using [Bmim]CF₃SO₃ as good solvent and water as poor solvent. A tentative mechanism for the growth of the flower-like LLM-105 three-dimensional microstructures was proposed on the basis of the analysis of X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). Comparing with LLM-105 raw material, the thermal decomposition took place at lower temperature and the weight loss has increased for the flower-like three-dimensional microstructures in the differential scanning calorimetric/thermogravimetric (DSC/TG) measurements.

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Advanced Materials, CEAM 2011

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Periodical:

Advanced Materials Research (Volumes 239-242)

Pages:

2942-2945

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.239-242.2942

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Online since:

May 2011

Authors:

Jin Chen, Li Li Wang, Guang Cheng Yang, Zhi Qiang Qiao, Fu De Nie

Keywords:

3D Microstructure, Flower-Like, LLM-105, Recrystallization

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© 2011 Trans Tech Publications Ltd. All Rights Reserved

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