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Search Results (1,114)

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14 pages, 4355 KiB  
Article
Computational Fluid Dynamics Analysis of Gas Suction in Coaxial Flow Venturi Injector: Impact of Gas–Liquid Interface Structure in Mixing Section
by Yihan Zu, Wenchen Zhong, Enle Xu and Zhenyong Miao
Appl. Sci. 2024, 14(23), 10839; https://doi.org/10.3390/app142310839 - 22 Nov 2024
Viewed by 349
Abstract
The gas–liquid Venturi injector has been widely applied in industrial production due to its advantages of high entrainment and low energy consumption. In this study, Computational Fluid Dynamics (CFD) was employed to investigate the effect of the gas–liquid interface structure within the mixing [...] Read more.
The gas–liquid Venturi injector has been widely applied in industrial production due to its advantages of high entrainment and low energy consumption. In this study, Computational Fluid Dynamics (CFD) was employed to investigate the effect of the gas–liquid interface structure within the mixing section on entrainment behavior by varying the geometry of the mixing section during gas–liquid coaxial flow. The simulation results indicate that along the jet direction, the gas–liquid interface generally transitions from a smooth cylindrical shape to a lobed structure in the mixing section. Surface waves mainly appear in the lobed region. Furthermore, lobed and surface wave structures reduce pressure loss and enhance entrainment. Additionally, the study found that longer mixing sections enhance entrainment under low flow resistance. This study provides valuable insights for achieving high jet entrainment and offers supplementary research on gas–liquid interface structures in jets constrained by solid boundaries. Full article
23 pages, 9176 KiB  
Article
Influence of Boundary Conditions on the Estimation of Thermal Properties in Insulated Building Walls
by Manon Rendu, Jérôme Le Dréau, Patrick Salagnac and Maxime Doya
Buildings 2024, 14(12), 3706; https://doi.org/10.3390/buildings14123706 - 21 Nov 2024
Viewed by 209
Abstract
The objective of this study is to evaluate the ability of inverse techniques to estimate the resistance and the capacity of a highly insulated multilayer wall under real weather conditions. The wall is equipped with temperature sensors inside and on its inner and [...] Read more.
The objective of this study is to evaluate the ability of inverse techniques to estimate the resistance and the capacity of a highly insulated multilayer wall under real weather conditions. The wall is equipped with temperature sensors inside and on its inner and outer surfaces, and the boundary conditions have been measured over a 14-day period. Uncertainties on various parameters of the model are evaluated, including internal and external convective heat transfer coefficients (±20% and ±7 W.m-².K−1 respectively), external long-wave heat transfer coefficient (±0.15 W.m−2.K−1) and solar absorption coefficient (±0.06). A sensitivity analysis demonstrated the high correlation with some parameters defining the thermal performance of the walls (thermal resistance or capacity). A solution is proposed to limit the number of identified parameters, while allowing the identification of the thermal resistance and the thermal capacity of the walls. There are two cases: either the weather conditions are accurately measured (temperature, short- and long-wave radiation) and the thermal characteristics can be assessed, or intrusive sensors are installed, and the thermal characteristics can be evaluated more accurately. Full article
(This article belongs to the Section Building Energy, Physics, Environment, and Systems)
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Figure 1

Figure 1
<p>Locations of sensors in the wall.</p>
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<p>Photos of the experimental setup: (<b>a</b>) outdoor air temperature sensor; (<b>b</b>) radiometers; (<b>c</b>) sonic anemometer; (<b>d</b>) outdoor surface temperature sensors; (<b>e</b>) indoor air temperature sensors with ventilated shield and indoor surface temperature sensors.</p>
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<p>Boundary conditions for the <span class="html-italic">ROLBS case:</span> temperature and solar radiation (<b>a</b>), the related wind rose (<b>b</b>) and wind speed and direction against time (<b>c</b>).</p>
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<p>Boundary conditions for the <span class="html-italic">ROLBS case:</span> temperature and solar radiation (<b>a</b>), the related wind rose (<b>b</b>) and wind speed and direction against time (<b>c</b>).</p>
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<p>Boundary conditions for the <span class="html-italic">typical cloudy day</span> and the <span class="html-italic">typical sunny day</span>.</p>
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<p>Estimation of location of sensor <span class="html-italic">S<sub>2</sub></span> based on the temperature distribution under steady-state conditions.</p>
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<p>Location of boundary conditions and sensors.</p>
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<p>Outdoor convective heat transfer coefficients for different correlations in the <span class="html-italic">ROLBS case</span>.</p>
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<p><span class="html-italic">RC model</span> structure for the <span class="html-italic">6R3C model</span>.</p>
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<p>Validation of the <span class="html-italic">24R21C model</span>.</p>
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<p>Principle of inverse method, adapted from [<a href="#B54-buildings-14-03706" class="html-bibr">54</a>].</p>
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<p>Study of the impact of the variation of heat transfer coefficients during the <span class="html-italic">cloudy day</span> and the <span class="html-italic">sunny day</span>.</p>
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<p>Sensitivity analysis of the parameters estimated during both typical days (<span class="html-italic">BC1</span>).</p>
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<p>Estimation of <span class="html-italic">R</span>- and <span class="html-italic">C</span>-values—data with and without noise—<span class="html-italic">BC1</span>.</p>
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<p>Sensitivity analysis of the parameters to be estimated with free floating conditions (<span class="html-italic">sunny day</span>) and with active heating (1 March 2019) with <span class="html-italic">BC2</span>.</p>
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<p>Estimation of <span class="html-italic">R</span>- and <span class="html-italic">C</span>-values—data with and without noise—<span class="html-italic">BC2</span>.</p>
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<p>Estimation of <span class="html-italic">R</span>- and <span class="html-italic">C</span>-values from measured experimental data and using outside and inside boundary conditions.</p>
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<p>Temperature measured in the wall and estimated by the model and the residuals.</p>
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<p>Procedure for experimental design.</p>
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27 pages, 6162 KiB  
Article
Numerical Study of the Nonlinear Soil–Pile–Structure Interaction Effects on the Lateral Response of Marine Jetties
by Marios Koronides, Constantine Michailides, Panagiotis Stylianidis and Toula Onoufriou
J. Mar. Sci. Eng. 2024, 12(11), 2075; https://doi.org/10.3390/jmse12112075 - 17 Nov 2024
Viewed by 332
Abstract
This study presents three-dimensional finite element analyses of two marine structures subjected to lateral loading to approximate environmental forces (e.g., wind, waves, currents, earthquakes). The first structure is a marine jetty supported by twenty-four piles, representative of an existing structure in Cyprus, while [...] Read more.
This study presents three-dimensional finite element analyses of two marine structures subjected to lateral loading to approximate environmental forces (e.g., wind, waves, currents, earthquakes). The first structure is a marine jetty supported by twenty-four piles, representative of an existing structure in Cyprus, while the second is a simplified four-pile marine structure. Soil–pile interaction is modelled using nonlinear p-y, τ-z, and q-z springs that are distributed along the piles, while steel plasticity is also considered. This study examines the relationship between failure modes, deformation modes, and plastic hinge locations with soil behaviour and soil reaction forces. It also aims at investigating the behaviour of the above structures in lateral loading and quantifying the consequences of unrealistic assumptions such as soil and steel linearity or tension-resistant q-z springs. The results indicate that such assumptions can lead to the wrong prediction of failure modes, plastic hinges, and critical elements while emphasising the crucial role of soil nonlinearity and axial pile–soil behaviour on the structural response. It is demonstrated that the dominant nonlinear sources relevant to this study, whether soil nonlinearity, plastic hinge formation, or a combination of the two, are primarily influenced by the axial capacity of soil–pile foundation systems, particularly their tensile component. Full article
(This article belongs to the Section Ocean Engineering)
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Figure 1

Figure 1
<p>Reference marine structure situated off the coast of Vasiliko, Cyprus: (<b>a</b>) view of the entire jetty, (<b>b</b>) T-junction’s closer view.</p>
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<p>View of the platform deck’s underside, depicting the connections between the piles and the deck. It also includes a schematic representation of the pile positions and their inclination directions, as well as details regarding their cross-sectional area and length.</p>
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<p>Soil stratigraphy and material characterisation below the T-junction.</p>
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<p>Profiles of small-strain Young’s modulus derived using Equations (2) and (3), as proposed by [<a href="#B42-jmse-12-02075" class="html-bibr">42</a>,<a href="#B46-jmse-12-02075" class="html-bibr">46</a>], respectively, with the assumed profile superimposed.</p>
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<p>FE model of the SPSI<sup>jetty</sup> system shown in (<b>a</b>) isoparametric, (<b>b</b>) plan (x-y), (<b>c</b>) x-z side, and (<b>d</b>) y-z side views.</p>
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<p>FE model of the SPSI<sup>8×8</sup> system shown in (<b>a</b>) isoparametric, (<b>b</b>) x-z side, and (<b>c</b>) plan (x-y) views.</p>
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<p>Stress–strain behaviour of steel input in the analyses.</p>
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<p>Impact of steel plasticity and nonlinear behaviour of springs on the force–displacement response of SPSI<sup>8×8</sup> marine structure. The stages of plastic hinge formation are illustrated for analyses involving elastoplastic steel.</p>
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<p>Sum of T, Q and P reactions forces of nonlinear springs acting on the −x and +x piles, computed from analyses involving either elastic or elastoplastic steel.</p>
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<p>Sum of T, Q and P reactions forces of linear springs acting on the −x and +x piles, computed from analyses involving either elastic or elastoplastic steel.</p>
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<p>Sequence of plastic hinge formation (indicated by numbering) in the SPSI<sup>8×8</sup> marine structure, as predicted by analyses involving (<b>a</b>) linear springs, and (<b>b</b>) nonlinear springs. Distribution of plastic strains is plotted at the last converged increment of the analyses.</p>
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<p>Impact of steel plasticity, springs nonlinearity and tension allowance of the pile tip springs on the force–displacement response of the SPSI<sup>jetty</sup>.</p>
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<p>Variation in all reaction forces (T, Q and P) of the springs attached on the centre (C) and rear (R) piles, as shown in <a href="#jmse-12-02075-f005" class="html-fig">Figure 5</a>b, with applied lateral force. The results are produced by EPsteel analyses that use either linear or nonlinear springs (nonlinear q-z springs are tensionless).</p>
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<p>Variation in all reaction forces (T, Q and P) of the springs attached on the centre (C) and rear (R) piles, as shown in <a href="#jmse-12-02075-f005" class="html-fig">Figure 5</a>b, with applied lateral force. The results are produced by EPsteel and nonlinear analyses with either tensionless or tension-resistant q-z.</p>
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<p>Plastic strain accumulation on the piles predicted by the analysis with linear springs, illustrated in (<b>a</b>) plan (x-y) view, and (<b>b</b>) side (x-z) view. The numbering indicates the sequence of hinge formation. The side view includes both initial (green) and deformed (black) structures, with displacements exaggerated by a factor of 5. All results are from the last converged increment of the analysis.</p>
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<p>Plastic strain accumulation on the piles predicted by the analysis with nonlinear springs and tensionless q-z springs, illustrated in (<b>a</b>) plan (x-y) view, and (<b>b</b>) side (x-z) view. The numbering indicates the sequence of hinge formation. The side view includes both initial (green) and deformed (black) structures, with displacements exaggerated by a factor of 5. All results are from the last converged increment of the analysis.</p>
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<p>Plastic strain accumulation on the piles predicted by the analysis with nonlinear springs and tension-resistant q-z springs, illustrated in (<b>a</b>) plan (x-y) view, and (<b>b</b>) side (x-z) view. The numbering indicates the sequence of hinge formation. The side view includes both initial (green) and deformed (black) structures, with displacements exaggerated by a factor of 5. All results are from the last converged increment of the analysis.</p>
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<p>(<b>a</b>) Axial force and (<b>b</b>) bending moments acting on various cross-sections (as shown in <a href="#jmse-12-02075-f015" class="html-fig">Figure 15</a>) plotted against the platform’s horizontal displacement.</p>
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<p>T-z spring curves input in the numerical model for (<b>a</b>) dense sand and (<b>b</b>) Marl layers.</p>
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<p>Q-z spring curves input in the numerical model at pile tips.</p>
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<p>P-y spring curves input in the numerical model for (<b>a</b>) dense sand and (<b>b</b>) Marl layers.</p>
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19 pages, 11375 KiB  
Article
Thermal Protection and Dielectric Properties of Borosilicate Coatings for SiCf/SiC Composites Under High-Temperature Oxidation
by Xiaohui Dong, Lianyi Wang, Ruiying Luo, Guoteng Zhang, Jinsen Wang, Xiaotian Yang, Huiyong Yang and Juntong Huang
Coatings 2024, 14(11), 1456; https://doi.org/10.3390/coatings14111456 - 15 Nov 2024
Viewed by 479
Abstract
Currently, oxidation of SiCf/SiC composites in harsh environments such as high temperatures has become a key challenge for their application in high-temperature structural wave-absorbing materials. In this study, borosilicate glass (BSZ) coatings were prepared using the thermal nitrogen–oxygen process. The evolution [...] Read more.
Currently, oxidation of SiCf/SiC composites in harsh environments such as high temperatures has become a key challenge for their application in high-temperature structural wave-absorbing materials. In this study, borosilicate glass (BSZ) coatings were prepared using the thermal nitrogen–oxygen process. The evolution of mechanical and coating microwave dielectric properties of the composites with and without BSZ coatings after oxidation at 1100 °C, 1200 °C, 1300 °C and 1400 °C was investigated. The results showed that the mechanical strength of the BSZ-coated SiCf/SiC specimens remains virtually unchanged, with a remarkable strength retention rate of 94%. The exceptional oxidation resistance of these coatings can be attributed to the formation of self-healing oxides and the reinforcing “pinning” effect of ZrSiO4. With an increase in oxidation temperature, the dielectric properties of the oxidized coatings are determined by the intrinsic properties of the generators and the porosity. Overall, these features highlight the potential of borosilicate coatings in the field of electromagnetic wave-absorbing composites, and the current work establishes a correlation between the oxidized microscopic properties of the coatings and the dielectric properties. Full article
(This article belongs to the Special Issue Applications of Ceramic and Cermet Coatings)
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Figure 1
<p>Coatings preparation process and procedure.</p>
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<p>Three-dimensional morphology of coatings after thermal nitrogen–oxygen treatment processes (<b>a</b>) 800 °C, (<b>b</b>) 1000 °C, (<b>c</b>) 1200 °C, (<b>d</b>) 1300 °C.</p>
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<p>Surface morphology and EDS of coatings at different thermal nitrogen–oxygen treatment temperatures (<b>a</b>) 800 °C, (<b>b</b>,<b>c</b>) 1100 °C, (<b>d</b>–<b>f</b>) 1200 °C, (<b>g</b>–<b>i</b>) 1300 °C.</p>
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<p>Cross-sectional morphology and EDS maps of coatings prepared by nitrogen–oxygen heat treatment at 1200 °C.</p>
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<p>Surface morphology of coated samples after 200 h of oxidation: (<b>a</b>–<b>c</b>) S-Y-1100, (<b>d</b>–<b>f</b>) S-Y-1200, (<b>g</b>–<b>i</b>) S-Y-1300, (<b>j</b>–<b>l</b>) S-Y-1400.</p>
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<p>Cross-section morphology of coated samples after 200 h of oxidation: (<b>a</b>) S-Y-1100, (<b>b</b>) S-Y-1200, (<b>c</b>) S-Y-1300, (<b>d</b>) S-Y-1400.</p>
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<p>XRD patterns of coated samples before and after 200 h of oxidation: (<b>a</b>) before oxidation, (<b>b</b>) after oxidation.</p>
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<p>XPS of coated samples after 200 h of oxidation at different temperatures. (<b>a</b>) Total spectrum (<b>b</b>) O1s fine spectrum, (<b>c</b>) Zr3d fine spectrum, (<b>d</b>) Si2p fine spectrum.</p>
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<p>Weight-change rate curves of coated samples static oxidized at different temperatures for 200 h: (<b>a</b>) SiC-SiC<sub>f</sub>/SiC, (<b>b</b>) BSZ/SiC-SiC<sub>f</sub>/SiC.</p>
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<p>Acoustic emission signal energy-cumulative energy–strain–stress curves for SiC<sub>f</sub>/SiC composites. (<b>a</b>) As prepared (without BSZ), (<b>b</b>) 1300 °C-200 h (without BSZ), (<b>c</b>) as prepared (with BSZ), (<b>d</b>) 1300 °C-200 h (with BSZ).</p>
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<p>Electromagnetic properties of the samples before and after oxidation. (<b>a</b>) real part, (<b>b</b>) imaginary part, (<b>c</b>) loss angle tangent, (<b>d</b>) impedance matching.</p>
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<p>The mechanism of microwave oxidation on the coating after 200 h oxidation at different temperatures. (<b>a</b>) RT, (<b>b</b>) 1100 °C, (<b>c</b>) 1200 °C, (<b>d</b>) 1300 °C, (<b>e</b>) 1400 °C.</p>
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31 pages, 17042 KiB  
Article
An Effective Alternative to the Open Trench Method for Mitigating Ground-Borne Environmental Body Waves: Corrugated Cardboard Boxes Reinforced with Balsa Wood
by Ayşenur Subaşı, Erkan Çelebi, Muhammet Burhan Navdar, Osman Kırtel and Berna İstegün
Appl. Sci. 2024, 14(22), 10544; https://doi.org/10.3390/app142210544 - 15 Nov 2024
Viewed by 388
Abstract
This research develops and evaluates a recyclable corrugated cardboard vibration isolation box reinforced with balsa wood as an alternative to traditional open trench methods for mitigating ground-borne environmental body waves. This study includes designing and testing scaled prototypes, laboratory analyses, prototype fabrication, and [...] Read more.
This research develops and evaluates a recyclable corrugated cardboard vibration isolation box reinforced with balsa wood as an alternative to traditional open trench methods for mitigating ground-borne environmental body waves. This study includes designing and testing scaled prototypes, laboratory analyses, prototype fabrication, and full-scale field experiments. In soft ground conditions, ensuring slope stability during deep excavations is a key engineering challenge for open trenches. For this purpose, scaled prototypes were subjected to laboratory tests to assess the resistance of the wave barrier’s wall surface. Numerical analyses were also conducted to evaluate the strength of the internal lattice structure under various loads. A prototype was fabricated for on-site experiments simulating real-world conditions. Field experiments evaluated the vibration isolation performance of the proposed barrier. Accelerometer sensors were strategically placed to gather data, analyzing ground surface vibrations for free field motions to assess the vibration shielding efficiency of both the open trench method and the corrugated vibration isolation box, with and without Styrofoam infill. This study concludes that the recyclable corrugated vibration isolation box is a viable alternative, offering comparable or improved vibration isolation efficiency in soft soil conditions while promoting environmental sustainability using recyclable materials. Full article
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Figure 1
<p>Double-wave corrugated cardboard [<a href="#B43-applsci-14-10544" class="html-bibr">43</a>,<a href="#B44-applsci-14-10544" class="html-bibr">44</a>].</p>
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<p>Balsa wood [<a href="#B46-applsci-14-10544" class="html-bibr">46</a>,<a href="#B47-applsci-14-10544" class="html-bibr">47</a>].</p>
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<p>Scaled test models of the vibration box.</p>
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<p>Different grid internal frames: (<b>a</b>) Scaled Model-1, (<b>b</b>) Scaled Model-2, (<b>c</b>) Scaled Model-3, (<b>d</b>) Scaled Model-4.</p>
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<p>Determination of the strength of scaled models by 3-point bending tests.</p>
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<p>The variation of top plate midpoint displacement values according to the number of finite elements.</p>
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<p>Analyzing the model of Scaled Model-4 in SAP2000 software.</p>
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<p>Comparison of numerical results with experimental results.</p>
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<p>Placing the samples in the water tank for curing test.</p>
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<p>Framework system of a module of the BCCB Trench prototype.</p>
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<p>Creating the internal grid system.</p>
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<p>A completed module of the BCCB Trench prototype.</p>
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<p>The completion of the BCCB Trench prototype by assembling the modules.</p>
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<p>Waterproofing of the BCCB Trench prototype.</p>
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<p>The site of the wave barrier vibration performance test.</p>
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<p>Soil profile of the test site.</p>
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<p>The dynamic load source and application method.</p>
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<p>The vibration measurement system.</p>
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<p>The vibration measurements under impact loading in the barrier-free condition.</p>
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<p>The filling material: polystyrene foam (Styrofoam).</p>
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<p>Layout of measuring points from a schematic view of the monitoring field test area with BCCB Trench.</p>
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<p>The process of trench excavation and the placement of the BCCB Trench.</p>
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<p>A general overview of the experimental measurements: (<b>a</b>) No Trench, (<b>b</b>) Empty Trench (<b>c</b>) BCCB Trench, and (<b>d</b>) Styrofoam-filled BCCB Trench.</p>
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<p>Comparative acceleration−time responses of a single impact test for each accelerometer.</p>
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<p>Comparative acceleration−time responses of a single impact test for each accelerometer.</p>
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<p>Comparative of normalized acceleration−time responses for each accelerometer.</p>
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<p>Comparative of normalized acceleration−time responses for each accelerometer.</p>
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<p>Comparison of normalized amplitude reduction ratio (ARR) in three components of instruments for (<b>a</b>) PGA, (<b>b</b>) PGV, and (<b>c</b>) PGD values [<a href="#B53-applsci-14-10544" class="html-bibr">53</a>].</p>
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9 pages, 520 KiB  
Review
Sleep Architecture Changes in Diabetes
by Yuanjie Mao
J. Clin. Med. 2024, 13(22), 6851; https://doi.org/10.3390/jcm13226851 - 14 Nov 2024
Viewed by 290
Abstract
Data on the relationship between sleep architecture and diabetes are limited. However, some evidence suggests that slow-wave sleep (SWS) plays a crucial role in maintaining normal glucose homeostasis and influences insulin secretion capacity. Diabetes is often associated with reduced SWS, even in the [...] Read more.
Data on the relationship between sleep architecture and diabetes are limited. However, some evidence suggests that slow-wave sleep (SWS) plays a crucial role in maintaining normal glucose homeostasis and influences insulin secretion capacity. Diabetes is often associated with reduced SWS, even in the absence of sleep-disordered breathing. Notably, selective suppression of SWS—without reducing total sleep time—can lead to significant increases in insulin resistance, decreased glucose tolerance, and a higher risk of diabetes. Given the growing interest in non-pharmacological lifestyle interventions, such as modifying sleep architecture, it is important to understand how sleep patterns differ in individuals with diabetes and whether these alterations impact diabetes risk and glycemic control. This review aims to provide a concise overview of the current findings on sleep architecture changes in people with diabetes. Full article
(This article belongs to the Section Endocrinology & Metabolism)
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<p>Potential main mechanisms of SWS disruption resulting in diabetes. SWS: slow-wave sleep.</p>
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19 pages, 2797 KiB  
Article
Interactions Between Corn Starch and Ethyl Maltol Under Heat-Moisture Treatment and Its Application in Fried Chicken Nuggets
by Meijuan Xu, Tianwen Liu, Xueqin Gao, Yuran Shi, Xiaodong Zhao and Jian Zou
Foods 2024, 13(22), 3629; https://doi.org/10.3390/foods13223629 - 14 Nov 2024
Viewed by 471
Abstract
This study delved into the interaction between corn starch and ethyl maltol during innovative repeated continuous heat-moisture treatment (RCHMT) and its impact on the quality of fried chicken nuggets. The results reveal that the complexation ratio of ethyl maltol is about 31.6%, and [...] Read more.
This study delved into the interaction between corn starch and ethyl maltol during innovative repeated continuous heat-moisture treatment (RCHMT) and its impact on the quality of fried chicken nuggets. The results reveal that the complexation ratio of ethyl maltol is about 31.6%, and the complex creates dense microporous structures. Native starch and complex samples exhibited an A-type crystal structure, while the physical mixture sample showed superposition peaks of starch and ethyl maltol. Additionally, the peak of C-O-H def., CH2 of the complex sample was blue-shifted to the larger wave number, and the hydrogen bond structure was enhanced. Moreover, the complex exhibited a higher resistant starch content and lower hydrolysis rate and amylose content than the physical mixture sample. The starch–ethyl maltol complex has been demonstrated to be a non-inclusion compound. It has been shown to reduce oil absorption and enhance the crispness of fried chicken nuggets, matching that of commercial products. This finding provides a direction for the development of innovative coating powders. Full article
(This article belongs to the Special Issue Advanced Research and Development of Carbohydrate from Foods)
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Graphical abstract

Graphical abstract
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<p>Complexation ratio at different ultrasonic times of the complex sample. Different letters indicate significantly different (<span class="html-italic">p</span> &lt; 0.05).</p>
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<p>SEM pictures of native starch, mixture, and complex samples. (<b>A-1</b>,<b>A-2</b>) Native starch; (<b>B-1</b>,<b>B-2</b>) mixture sample; (<b>C-1</b>,<b>C-2</b>) complex sample; -1, 1000 magnification; -2, 3000 magnification.</p>
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<p>XRD patterns (<b>A</b>), infrared spectrum (<b>B</b>), infrared deconvolution (<b>C</b>), <sup>13</sup>C-NMR spectra (<b>D</b>), locally enlarged image of <sup>13</sup>C-NMR spectra (<b>E</b>), and fitting image in C1 regions of <sup>13</sup>C-NMR spectra (<b>F</b>–<b>H</b>).</p>
Full article ">Figure 3 Cont.
<p>XRD patterns (<b>A</b>), infrared spectrum (<b>B</b>), infrared deconvolution (<b>C</b>), <sup>13</sup>C-NMR spectra (<b>D</b>), locally enlarged image of <sup>13</sup>C-NMR spectra (<b>E</b>), and fitting image in C1 regions of <sup>13</sup>C-NMR spectra (<b>F</b>–<b>H</b>).</p>
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<p>The hydrolysis curves (<b>A</b>), model fit curves, LOS plots (<b>B</b>–<b>D</b>), and correlation diagram (<b>E</b>) of native starch, mixture, and complex samples. E, Correlation analysis was performed using Pearson’s correlation analysis.</p>
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<p>Coating pick-up (<b>A</b>), oil absorption ratio (<b>A</b>), color values (<b>B</b>), texture (<b>C</b>), rose diagram of artificial sensory evaluation (<b>D</b>) of the chicken nuggets prepared using the complex with different addition ratios, and the texture (<b>E</b>) of chicken nuggets fried at different times. In the rose diagram of the artificial sensory evaluation (<b>D</b>), the letters A–F are the samples prepared by the complex with different addition ratios (0%, 3%, 6%, 9%, 12%, and 15%), and the letter G is the commercial sample. The lowercase letters are significantly different (<span class="html-italic">p</span> &lt; 0.05).</p>
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14 pages, 2909 KiB  
Article
Laser-Induced Decomposition and Mechanical Degradation of Carbon Fiber-Reinforced Polymer Subjected to a High-Energy Laser with Continuous Wave Power up to 120 kW
by Sebastian Schäffer, Stefan Reich, Dominic Heunoske, Martin Lueck, Johannes Wolfrum and Jens Osterholz
J. Compos. Sci. 2024, 8(11), 471; https://doi.org/10.3390/jcs8110471 - 13 Nov 2024
Viewed by 428
Abstract
Carbon fiber-reinforced polymer (CFRP), noted for its outstanding properties including high specific strength and superior fatigue resistance, is increasingly employed in aerospace and other demanding applications. This study investigates the interactions between CFRP composites and high-energy lasers (HEL), with continuous wave laser powers [...] Read more.
Carbon fiber-reinforced polymer (CFRP), noted for its outstanding properties including high specific strength and superior fatigue resistance, is increasingly employed in aerospace and other demanding applications. This study investigates the interactions between CFRP composites and high-energy lasers (HEL), with continuous wave laser powers reaching up to 120 kW. A novel automated sample exchange system, operated by a robotic arm, minimizes human exposure while enabling a sequence of targeted laser tests. High-speed imaging captures the rapid expansion of a plume consisting of hot gases and dust particles during the experiment. The research significantly advances empirical models by systematically examining the relationship between laser power, perforation times, and ablation rates. It demonstrates scalable predictions for the effects of high-energy laser radiation. A detailed examination of the damaged samples, both visually and via micro-focused computed X-ray tomography, offers insights into heat distribution and ablation dynamics, highlighting the anisotropic thermal properties of CFRP. Compression after impact (CAI) tests further assess the residual strength of the irradiated samples, enhancing the understanding of CFRP’s structural integrity post-irradiation. Collectively, these tests improve the knowledge of the thermal and mechanical behavior of CFRP under extreme irradiation conditions. The findings not only contribute to predictive modeling of CFRP’s response to laser irradiation but enhance the scalability of these models to higher laser powers, providing robust tools for predicting material behavior in high-performance settings. Full article
(This article belongs to the Special Issue Carbon Fiber Composites, Volume III)
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<p>Experimental setup includes an automated sample exchange, operated by a robotic arm.</p>
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<p>A gas cloud expands rapidly caused by laser irradiation of a CFRP plate with 120 kW and a beam size of 20 mm. The plate is perforated after 0.4 s.</p>
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<p>Damage zones of irradiated CFRP samples of two tested materials (P = 120 kW, Ø = 20 mm, d = 4 mm). The heat affected zone (HAZ) extends to areas outside the applied laser spot.</p>
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<p>Perforation times as a function of laser power in a double-logarithmic representation for a beam diameter of 20 mm and different sample thicknesses d. In this diagram, a linear decrease of the logarithm of the perforation time with increase of the logarithm of the laser power can be observed, represented by the solid and dashed lines.</p>
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<p>Volume damage as a function of perforation time in a double-logarithmic representation for various laser powers.</p>
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<p>Volume removal rate as a function of laser power. Symbols: <math display="inline"><semantics> <mrow> <msub> <mrow> <mi>r</mi> </mrow> <mrow> <mi>v</mi> <mi>o</mi> <mi>l</mi> </mrow> </msub> </mrow> </semantics></math> determined from experimental data and Equation (4). Lines: linear fit.</p>
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<p>µCT-scan cross-sections of irradiated CFRP samples reveal details of the heat affected zone and the delamination of fibers. The holes created have a conical shape (M18-1/G939, d = 6 mm).</p>
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<p>Residual compressive strength of laser irradiated CFRP samples determined in accordance with the compression after impact procedure.</p>
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19 pages, 4820 KiB  
Article
Fault Section Identification for Hybrid Transmission Lines Considering the Weak-Feed Characteristics of Floating Photovoltaic Power Plant Inverters
by Huiqiang Ye, Lifeng Zhu, Weifeng Xu, Fangzhou Liu, Xinbo Liu, Yi Xu and Qianggang Wang
Energies 2024, 17(22), 5640; https://doi.org/10.3390/en17225640 - 11 Nov 2024
Viewed by 376
Abstract
The overhead line (OHL)–cable hybrid transmission line, which connects floating photovoltaic (PV) power plants, needs to be considered regarding whether to block reclosing operations or not. However, due to the weak-feed characteristics of PV inverters, existing methods are difficult to apply in this [...] Read more.
The overhead line (OHL)–cable hybrid transmission line, which connects floating photovoltaic (PV) power plants, needs to be considered regarding whether to block reclosing operations or not. However, due to the weak-feed characteristics of PV inverters, existing methods are difficult to apply in this scenario. This paper proposes a criterion for fault section identification in the transmission lines of floating PV power plants based on traveling wave power and the zero-sequence impedance angle. Firstly, the fault current characteristics of photovoltaic inverters under dual-vector control are analyzed, and the applicability of the sequence component impedance directional criterion in this scenario is discussed. Then, the transmission, refraction, and reflection processes of traveling waves in OHL–cable hybrid lines are analyzed, and a traveling wave energy criterion is designed to determine the fault section. Finally, based on the scope of application of the zero-sequence impedance angle and traveling wave energy criterion, a fault section identification method for the hybrid lines of floating PV power plants is established. A deployment method for the proposed method, based on feeder terminal units (FTUs) at the connection points between the OHL and cable is proposed. This method identifies fault sections through traveling waves and zero-sequence impedance angles, which are unaffected by PV week feed characteristics, can be applied to all the AC fault types, and do not rely on multi-terminal synchronous sampling. The proposed method is verified on a 1MW PV system built in the PSCAD. Full article
(This article belongs to the Section F3: Power Electronics)
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<p>Diagram of a power grid connected with a water-based PV power plant.</p>
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<p>Control block diagram of positive and negative sequence currents.</p>
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<p>Fault traveling wave refraction and reflection processes.</p>
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<p>Traveling wave mutations of different fault sections.</p>
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<p>Water-based PV power plant with OHL–cable hybrid line.</p>
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<p>Flowchart of fault section judgment.</p>
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<p>Measurement point between the cable and transmission line based on FTUs.</p>
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<p>Structure of the hybrid transmission line model. Voltage and current waveform of the A-phase-to-ground fault.</p>
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<p>Positive sequence resistance angle changes with <span class="html-italic">k</span><sub>λ</sub> and <span class="html-italic">k</span><sub>ρ</sub>.</p>
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<p>Current and voltage waveforms of OHL faults.</p>
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<p>Current and voltage waveforms of cable fault.</p>
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<p>High-frequency characteristics of traveling waves of hybrid line faults.</p>
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<p>The zero sequence resistance angle of a single-phase grounding fault occurs near the zero-crossing point.</p>
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13 pages, 4685 KiB  
Article
High-Performance SAW-Based Microfluidic Actuators Composed of Sputtered Al–Cu IDT Electrodes
by Hwansun Kim, Youngjin Lee, Peddathimula Puneetha, Sung Jin An, Jae-Cheol Park and Siva Pratap Reddy Mallem
Coatings 2024, 14(11), 1420; https://doi.org/10.3390/coatings14111420 - 8 Nov 2024
Viewed by 414
Abstract
To realize highly sensitive SAW devices, novel Al–Cu thin films were developed using a combinatorial sputtering system. The Al–Cu sample library exhibited a wide range of chemical compositions and electrical resistivities, providing valuable insights for selecting optimal materials for SAW devices. Considering the [...] Read more.
To realize highly sensitive SAW devices, novel Al–Cu thin films were developed using a combinatorial sputtering system. The Al–Cu sample library exhibited a wide range of chemical compositions and electrical resistivities, providing valuable insights for selecting optimal materials for SAW devices. Considering the significant influence of electrode resistivity and density on acoustic wave propagation, an Al–Cu film with 65 at% Al was selected as the IDT electrode material. The selected Al–Cu film demonstrated a resistivity of 6.0 × 10−5 Ω-cm and a density of 4.4 g/cm3, making it suitable for SAW-based microfluidic actuator applications. XRD analysis revealed that the Al–Cu film consisted of a physical mixture of Al and Cu without the formation of Al–Cu alloy phases. The film exhibited a fine-grained microstructure with an average crystallite size of 7.5 nm and surface roughness of approximately 6 nm. The SAW device fabricated with Al–Cu IDT electrodes exhibited excellent acoustic performance, resonating at 143 MHz without frequency shift and achieving an insertion loss of −13.68 dB and a FWHM of 0.41 dB. In contrast, the Au electrode-based SAW device showed significantly degraded acoustic characteristics. Moreover, the SAW-based microfluidic module equipped with optimized Al–Cu IDT electrodes successfully separated 5 μm polystyrene (PS) particles even at high flow rates, outperforming devices with Au IDT electrodes. This enhanced performance can be attributed to the improved resonance characteristics of the SAW device, which resulted in a stronger acoustic radiation force exerted on the PS particles. Full article
(This article belongs to the Special Issue Thin Films and Nanostructures for Electronics)
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<p>Schematic diagram of combinatorial sputtering to produce Al–Cu thin films with varying and uniform compositions.</p>
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<p>Thickness distribution and cross-section images of Al–Cu thin films [<a href="#B25-coatings-14-01420" class="html-bibr">25</a>].</p>
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<p>Surface and cross-sectional SEM images of Al–Cu thin films with uniform thickness and compositions.</p>
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<p>XRD patterns of Al–Cu thin films with uniform physical and chemical properties.</p>
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<p>AFM topography images of sputter-deposited Al–Cu thin films (S1, S2, S3) with different surface roughness values.</p>
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<p>SAW-IDT pattern design for separating 5 μm PS micro-particles. (<b>a</b>) Distribution of resonant frequency depending on IDT pattern width and (<b>b</b>) relationship between total IDT length and electrode pairs at the reference impedance of 50 Ω.</p>
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<p>Resonant frequency of SAW devices with Al–Cu and Au electrode.</p>
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<p>SAW-based microfluidic actuator module for 5 μm PS particle separation. (<b>a</b>) Picture of SAW-based microfluidic actuator module and (<b>b</b>) separation efficiency of PS particles according to the flow rate of PS suspension with a concentration of 100 μg/L.</p>
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<p>Optical microscope images of PS particles captured at the drain/outlet ports in the SAW actuator module consisting of two different electrodes.</p>
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13 pages, 1769 KiB  
Article
Effect of Controlled Expiratory Pressures on Cerebrovascular Changes During Valsalva Maneuver
by Ju-Yeon Jung, Yeong-Bae Lee and Chang-Ki Kang
Appl. Sci. 2024, 14(22), 10132; https://doi.org/10.3390/app142210132 - 5 Nov 2024
Viewed by 435
Abstract
This study aimed to investigate the effects of Valsalva maneuver (VM) with the controlled expiratory pressures on vascular stiffness of common carotid artery (CCA) and cerebral hemodynamic changes using diagnostic ultrasonography. Twenty-seven healthy participants (mean and standard deviation of age = 22.78 ± [...] Read more.
This study aimed to investigate the effects of Valsalva maneuver (VM) with the controlled expiratory pressures on vascular stiffness of common carotid artery (CCA) and cerebral hemodynamic changes using diagnostic ultrasonography. Twenty-seven healthy participants (mean and standard deviation of age = 22.78 ± 1.89) performed 30 and 40 mmHg VM. The right CCA stiffness index and pulse wave velocity (PWV) were measured before (PRE) and after (POST) VM. The peak systolic velocity (PSV), resistance index (RI), and heart rate (HR) were measured before (PRE) and after (POST1 and POST2 during the first and the second 15 s, respectively) VM. Near-infrared spectroscopy (NIRS) was utilized to measure regional oxygen saturation (rSO2) and oxyhemoglobin (HbO) on the left and right prefrontal cortex. Stiffness index decreased by 1.76 (p < 0.001) from PRE to POST only after 30 mmHg VM. PWV decreased by 0.69 m/s (p < 0.001, 30 mmHg) and 0.34 m/s (p = 0.022, 40 mmHg) in POST. Conversely, PSV increased by 5.36 cm/s (p = 0.031, 30 mmHg) and 4.77 cm/s (p = 0.04, 40 mmHg) in POST2. Increase in RI (p = 0.017) and decrease in HR (p = 0.003) occurred only after the 40 mmHg VM. Right HbO decreased after 30 mmHg VM (p = 0.023) from PRE to POST1, and right rSO2 increased after 40 mmHg VM (p = 0.036) from VM (during) to POST1. Both 30 and 40 mmHg VM showed a significant improvement in PWV and an increase in PSV. However, at 30 mmHg VM, a significant decrease in HbO was observed after VM owing to increased cerebral oxygen exchange, and at 40 mmHg VM, an rSO2 increase was observed after VM owing to high vascular pressure. Additionally, the increased pressure and rSO2 at 40 mmHg may have been caused by increased RI. The results indicated that the 30 mmHg VM was more effective on CCA stiffness than the 40 mmHg VM. Full article
(This article belongs to the Special Issue Current Updates on Ultrasound for Biomedical Applications)
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<p>Flow chart of experimental protocol.</p>
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<p>Ultrasound and near-infrared spectroscopy measurements and a schematic of the Valsalva maneuver system with a participant lying on the bed. Abbreviations: NIRS, near-infrared spectroscopy; US, ultrasound.</p>
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<p>Protocol for biosignal acquisition before and after VM. Abbreviations: BP, blood pressure; NIRS, near-infrared spectroscopy; POST, after VM; PRE, before VM; VM, Valsalva maneuver.</p>
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12 pages, 5249 KiB  
Article
Highly Productive Laser Annealing Manufacturing Method Using Continuous Blue WBC (Wavelength Beam Combining) Technique
by Mitsuoki Hishida, Naohiko Kobata, Kentaro Miyano, Masaki Nobuoka, Tatsuya Okada and Takashi Noguchi
Materials 2024, 17(22), 5399; https://doi.org/10.3390/ma17225399 - 5 Nov 2024
Viewed by 525
Abstract
Blue laser annealing can be used to obtain a high-mobility thin-film transistor (TFT) through a laser annealing (i.e., LTPS: low-temperature Poly-Si) process. However, the laser annealing process’s low productivity (as well as high cost) is an issue because the high output power of [...] Read more.
Blue laser annealing can be used to obtain a high-mobility thin-film transistor (TFT) through a laser annealing (i.e., LTPS: low-temperature Poly-Si) process. However, the laser annealing process’s low productivity (as well as high cost) is an issue because the high output power of blue lasers still needs to be addressed. Therefore, productivity can be improved if blue laser energy is efficiently supplied during the laser annealing process using a continuous wave laser instead of a conventional pulsed excimer laser. We developed a blue laser light source (440 ± 10 nm) using the wavelength beam combining (WBC) method, which can achieve a laser power density of 73.7 kW/cm2. In this semiconductor laser, when the power was increased s by 2.9 times, the laser scanning speed was increased by 5.0 times, achieving twice the productivity of conventional lasers. After laser annealing, the size of the crystal grains varied between 2 and 15 μm, resulting in a crystallization rate of 100% by Raman scattering rsult and low resistivity of 0.04 Ωcm. This increase in production capacity is not an arithmetic increase with increased power but a geometric production progression. Full article
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<p>Schematic illustration of wavelength beam combining [<a href="#B6-materials-17-05399" class="html-bibr">6</a>,<a href="#B10-materials-17-05399" class="html-bibr">10</a>,<a href="#B18-materials-17-05399" class="html-bibr">18</a>].</p>
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<p>Appearance model diagram of equipment with line laser processing [<a href="#B15-materials-17-05399" class="html-bibr">15</a>].</p>
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<p>Beam profile of Condition E [<a href="#B15-materials-17-05399" class="html-bibr">15</a>].</p>
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<p>Evaluation of crystallization/substrate cracking at each power density and scanning speed.</p>
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<p>Top view of the cracked area after laser annealing. (In addition to the annealed p-Si on the surface, approximately 5 μm peeled off from the glass surface, revealing a portion of the glass interior in the lower right of the picture).</p>
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<p>Comparison of EBSD results at two different scan speeds: (<b>a</b>) 500 mm/s; (<b>b</b>) 1000 mm /s.</p>
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<p>Comparison of Raman spectrum shifts at the fastest processing speed with different power densities (conditions A, B, C).</p>
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11 pages, 3623 KiB  
Article
Hybrid Functional ITO/Silver Nanowire Transparent Conductive Electrodes for Enhanced Output Efficiency of Ultraviolet GaN-Based Light-Emitting Diodes
by Munsik Oh, Mun Seok Jeong, Jaehee Cho and Hyunsoo Kim
Materials 2024, 17(21), 5385; https://doi.org/10.3390/ma17215385 - 4 Nov 2024
Viewed by 483
Abstract
We investigated hybrid functional transparent conductive electrodes (HFTCEs) composed of indium-tin-oxide (ITO) and silver nanowires (AgNWs) for the enhancement of output efficiency in GaN-based ultraviolet light-emitting diodes (UVLEDs). The HFTCEs demonstrated an optical transmittance of 69.5% at a wavelength of 380 nm and [...] Read more.
We investigated hybrid functional transparent conductive electrodes (HFTCEs) composed of indium-tin-oxide (ITO) and silver nanowires (AgNWs) for the enhancement of output efficiency in GaN-based ultraviolet light-emitting diodes (UVLEDs). The HFTCEs demonstrated an optical transmittance of 69.5% at a wavelength of 380 nm and a sheet resistance of 16.4 Ω/sq, while the reference ITO TCE exhibited a transmittance of 76.4% and a sheet resistance of 18.7 Ω/sq. Despite the 8.9% lower optical transmittance, the UVLEDs fabricated with HFTCEs achieved a 25% increase in output efficiency compared to reference UVLEDs. This improvement is attributed to the HFTCE’s twofold longer current spreading length under operating forward voltages, and more significantly, the enhanced out-coupling of localized surface plasmon (LSP) resonance with the trapped wave-guided light modes. Full article
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<p>(<b>a</b>) The schematic diagram of process and (<b>b</b>) SEM top-view images and (<b>c</b>) cross-sectional STEM and EDXS elementary maps of ITO/AgNWs HFTCE.</p>
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<p>(<b>a</b>) The optical specular transmittance spectra of the ITO films (100 nm and 300 nm), AgNWs, and ITO (100 nm)/AgNWs HFTCE. (<b>b</b>) <span class="html-italic">I–V</span> curves of the reference 300 nm thick ITO, AgNWs, and ITO/AgNWs TLM patterns formed on the p-type layer of UVLEDs. The insets show the optical microscopic top-view images and schematic diagrams of TLM patterns for AgNWs and ITO/AgNWs.</p>
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<p>(<b>a</b>) <span class="html-italic">I</span>–<span class="html-italic">V</span> curves, (<b>b</b>) <span class="html-italic">I</span>(d<span class="html-italic">V</span>/d<span class="html-italic">I</span>) verus <span class="html-italic">I</span> plots, (<b>c</b>) <span class="html-italic">J</span>–<span class="html-italic">V</span> curves plotted as a function of mesa length (<span class="html-italic">L</span>), and (<b>d</b>) <span class="html-italic">L</span><sub>s</sub> versus forward voltage plots of HFTCE-UVLEDs and reference UVLEDs. The optical microscopic top views of both UVLEDs are shown in the inset of (<b>a</b>).</p>
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<p>(<b>a</b>) <span class="html-italic">L–I</span> curves and (<b>b</b>) normalized external quantum efficiency versus <span class="html-italic">I</span> plots HFTCE-UVLEDs and reference UVLEDs. The EL images of the UVLEDs taken at an injection current of 10 mA and the EL spectra are shown in the insets of (<b>a</b>,<b>b</b>).</p>
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<p>The EL, magnified OM, and CSEM images of (<b>a</b>) reference UVLED and (<b>b</b>) HFTCE-UVLED taken at 8 mA.</p>
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<p>PL—intensity decay curves of HFTCE-UVLEDs and reference UVLEDs.</p>
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<p>Electric field distributions at the cross-section of HFTCE-UVLEDs and reference UVLEDs, computed for TE and TM mode.</p>
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27 pages, 8833 KiB  
Article
Effects of Connecting Structures in Double-Hulled Water-Filled Cylindrical Shells on Shock Wave Propagation and the Structural Response to Underwater Explosion
by Caiyu Yin, Zhiyang Lei, Zeyu Jin and Zifeng Shi
J. Mar. Sci. Eng. 2024, 12(11), 1949; https://doi.org/10.3390/jmse12111949 - 31 Oct 2024
Viewed by 397
Abstract
In conventional double-hulled submarines, the connecting structures that facilitate the linkage between the two hulls are crucial for load transmission. This paper aims to elucidate the effect of these connecting structures on resistance to shock waves generated by underwater explosions. Firstly, a self-developed [...] Read more.
In conventional double-hulled submarines, the connecting structures that facilitate the linkage between the two hulls are crucial for load transmission. This paper aims to elucidate the effect of these connecting structures on resistance to shock waves generated by underwater explosions. Firstly, a self-developed numerical solver is built for the one-dimensional water-filled elastically connected double-layer plate model. The shock wave propagation characteristics, shock response of structure, water cavitation, and impact loads transmitted through the gap water and the connecting structures are analyzed quantitatively. The results reveal that the majority of the shock impulse is transmitted by the gap water if the equivalent stiffness of the connecting structures is much less than that of the gap water. Then, a three-dimensional model of the double-hulled, water-filled cylindrical shell is constructed in Abaqus/Explicit, utilizing the acoustic-structural coupling methodology. The analysis focuses on the influence of the thickness and density distribution of the connecting structures on the system’s shock response. The results indicate that a densely arranged connecting structure results in a wavy deformation of the outer hull and a notable reduction in both the impact response and strain energy of the inner hull. When the stiffness of the densely arranged connecting structure is comparatively low, the internal energy and plastic energy of the inner hull are decreased by 16.5% and 24.1%, respectively. The findings of this research are useful for assessing shock resistance and for the design of connecting structures within conventional double-hulled submarines. Full article
(This article belongs to the Section Ocean Engineering)
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<p>The schematic of typical double-hulled submarines.</p>
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<p>The model illustration of the water-filled elastically connected double-layer plate, where the inner plate is elastically supported, and the rigidity of the connecting structure is designated as <span class="html-italic">K</span><sub>CON</sub>.</p>
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<p>The schematic of the numerical model of the double-hull water-filled cylindrical shell model.</p>
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<p>The distribution schematic for different connecting structures.</p>
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<p>The finite element mesh schematic of the double-hull water-filled cylindrical shell model.</p>
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<p>The exponential decay shock wave profile, corresponding to an explosive mass of 2000 kg and a detonation distance of 30 m.</p>
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<p>(<b>a</b>) The pressure history applied on the stationary inner hull predicted by the numerical solver. (<b>b</b>) Comparison results of the nondimensional shock impulse acting on the stationary inner plate.</p>
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<p>Comparison between the numerical simulations and the experiment results for the measuring point A2, where the detonation distances are (<b>a</b>) 8.4 m and (<b>b</b>) 4.4 m, respectively.</p>
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<p>(<b>a</b>) The schematic diagram of structural and fluid finite element meshes, and (<b>b</b>) the influences of the mesh sizes of the fluid on the predictions of the wet face pressure history on the outer thin hull and inner pressure hull.</p>
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<p>The temporal and spatial distribution of fluid pressure in external and gap water, where the support spring of <span class="html-italic">K</span><sub>S</sub> is soft and equals to 5 × 10<sup>8</sup> Pa/m, and the stiffness of the connection spring <span class="html-italic">K</span><sub>CON</sub> is (<b>a</b>) 9 × 10<sup>8</sup> Pa/m, (<b>b</b>) 4.5 × 10<sup>9</sup> Pa/m, and (<b>c</b>) 2.25 × 10<sup>10</sup> Pa/m. The area denoted in gray represents the cavitation zone.</p>
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<p>The pressure distribution at various time instants for case 1, where the stiffness of support spring <span class="html-italic">K</span><sub>S</sub> is soft and equals to 5 × 10<sup>8</sup> Pa/m and the connecting spring <span class="html-italic">K</span><sub>CON</sub> is 9 × 10<sup>8</sup> Pa/m.</p>
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<p>The temporal and spatial distribution of fluid pressure in external and gap water, where the support spring of <span class="html-italic">K</span><sub>S</sub> is stiff and equals to 5 × 10<sup>10</sup> Pa/m, and the stiffness of the connecting spring <span class="html-italic">K</span><sub>CON</sub> is 9 × 10<sup>8</sup> Pa/m. The area denoted in gray represents the cavitation zone.</p>
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<p>Time histories of the velocities of the outer and inner plates for the six cases.</p>
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<p>The dynamic pressure on fluid-solid coupling surfaces and force of connection spring <span class="html-italic">K</span><sub>CON</sub>, where the stiffness of the connection spring is (<b>a</b>) 9 × 10<sup>8</sup> Pa/m, (<b>b</b>) 4.5 × 10<sup>9</sup> Pa/m, and (<b>c</b>) 2.25 × 10<sup>10</sup> Pa/m. The stiffness of support spring <span class="html-italic">K</span><sub>S</sub> is soft and equals to 5 × 10<sup>8</sup> Pa/m.</p>
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<p>The dynamic pressure on fluid-solid coupling surfaces and connection force of connection spring <span class="html-italic">K</span><sub>CON</sub>, where the stiffness of the connection spring is (<b>a</b>) 9 × 10<sup>8</sup> Pa/m, (<b>b</b>) 4.5 × 10<sup>9</sup> Pa/m, and (<b>c</b>) 2.25 × 10<sup>10</sup> Pa/m. The stiffness of support spring <span class="html-italic">K</span><sub>S</sub> is stiff and equals to 5 × 10<sup>10</sup> Pa/m.</p>
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<p>Shock wave transmission process in water diagram. The first column represents case No. 0, with no connection structure; the second column corresponds to case No. 2, featuring a connection structure with a thickness of 20 mm and a spacing of 1000 mm.</p>
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<p>The time history of pressure on three different fluid-structure interaction surfaces for cases No. 0, 1, and 2.</p>
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<p>The displacement distribution of structure with different connection structure at the time instant of 1 ms. The amplification coefficient of deformation is 10.</p>
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<p>The displacement response of the outer hull on the side of the explosion source at different time instants for cases No. 0, 2, and 4.</p>
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<p>The displacement response of the inner hull on the side of the explosion source at different time instants for cases No. 0, 2, and 4.</p>
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<p>The velocity response of the outer hull on the side of the explosion source at different time instants for cases No. 0, 2, and 4.</p>
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<p>The velocity response of the inner hull on the side of the explosion source at different time instants.</p>
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<p>The peak velocity results at different locations on the blast-facing surface of the inner hull for cases No. 0, 2, and 4.</p>
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<p>The strain energy results of (<b>a</b>) the outer hull, (<b>b</b>) the inner hull with T-shape stiffeners, and (<b>c</b>) the connecting structures.</p>
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9 pages, 1583 KiB  
Article
The Effect of Silver Nanoparticles on Bond Strength of Calcium Silicate-Based Sealer: An In Vitro Study
by Sundus Bukhary, Sarah Alkahtany and Dalal AlDabeeb
Appl. Sci. 2024, 14(21), 9817; https://doi.org/10.3390/app14219817 - 27 Oct 2024
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Abstract
The aim of this study was to evaluate the bond strength of the calcium silicate-based sealer (CSS) modified with the silver nanoparticles (AgNPs) using the single-cone technique (SC) and the continuous wave condensation (CWC) technique, measured by a universal testing machine. The AgNPs [...] Read more.
The aim of this study was to evaluate the bond strength of the calcium silicate-based sealer (CSS) modified with the silver nanoparticles (AgNPs) using the single-cone technique (SC) and the continuous wave condensation (CWC) technique, measured by a universal testing machine. The AgNPs and the modified sealers were characterized by scanning electron microscopy and transmission electron microscopy. One hundred single-rooted extracted human permanent teeth with a single root canal were cleaned and shaped with a Protaper Next system. The teeth were randomly divided into four groups (n = 25) as follows: Group 1, canals were obturated using the SC technique with TotalFill® BC Sealer. Group 2, canals were obturated using the SC technique with TotalFill® BC Sealer mixed with AgNPs. Group 3, canals were obturated using the CWC technique with TotalFill® HiFlow BC Sealer. Group 4, canals were obturated using the CWC technique with TotalFill® HiFlow BC Sealer mixed with AgNPs. After two weeks, 1 mm-thick dentin slices were cut and exposed to a push-out bond strength test using a universal testing machine. Specimens were examined under a digital microscope to determine the mode of failure. Statistical analysis was performed using ANOVA and Tukey multiple comparison tests (p < 0.05). The nanoparticle characterization revealed a spherical morphology with no obvious aggregations. The results showed that group 4 had the highest dislodgement resistance compared to all groups (p < 0.05). Group 4 was significantly higher in push-out bond strength value than group 1 (p < 0.001) and group 3 (p < 0.003), but not significantly higher than group 2. Cohesive failure was the most prevalent failure mode among all groups. It can be concluded that the incorporation of silver nanoparticles into the calcium silicate-based sealer significantly increased the bond strength. The warm obturation approach demonstrated significantly higher resistance to dislodgment as compared to the single-cone technique. Full article
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Figure 1

Figure 1
<p>(<b>A</b>,<b>B</b>) SEM images of AgNPs illustrating the spherical shape and size range (<math display="inline"><semantics> <mrow> <mo>×</mo> </mrow> </semantics></math>130,000); (<b>C</b>,<b>D</b>) TEM images of AgNPs illustrate the distribution of spherical and semi-identical particles, as well as the absence of particle aggregations (<math display="inline"><semantics> <mrow> <mo>×</mo> </mrow> </semantics></math>300,000); (<b>E</b>,<b>F</b>) TEM images of AgNPs mixed with calcium silicate-based sealer demonstrate the spherical shape of AgNPs, with no obvious aggregation (<math display="inline"><semantics> <mrow> <mo>×</mo> </mrow> </semantics></math>50,000–100,000).</p>
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<p>Images obtained by digital microscopy at 50× magnification for analysis of the mode of failure after push-out test. (<b>A</b>–<b>C</b>) Adhesive mode of failure; no sealer presents on the canal wall. (<b>D</b>–<b>F</b>) Cohesive mode of failure; sealer is located circumferentially on the canal wall. (<b>G</b>–<b>I</b>) Mixed mode of failure; sealer is present partially on the canal wall.</p>
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