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Optimization of biodiesel production process from Jatropha oil using supported heteropolyacid catalyst and assisted by ultrasonic energy

Ali Sabri Badday, Ahmad Zuhairi Abdullah and Keat-Teong Lee

Renewable Energy, 2013, vol. 50, issue C, 427-432

Abstract: Application of ultrasound-assisted biodiesel production process from Jatropha oil catalyzed by activated carbon-supported tungstophosphoric acid catalyst was studied. Influences of ultrasonic energy on different process variables were elucidated. Reaction variables i.e. reaction time (10–50 min), reactants' molar ratio (5:1–25:1), ultrasonic amplitude (30–90% of the maximum sonifier power) and catalyst amount (2.5–4.5 w/w oil) were studied. A mathematical representation for biodiesel yield was successfully generated. A yield of 91% was achieved in just 40 min at a moderate ultrasonic amplitude (∼60%), high molar ratio (25:1) and low reaction temperature (65 °C). Interactions between the variables were also validated statistically. Leaching study revealed that the reaction was predominately heterogeneous in nature.

Keywords: Biodiesel; Jatropha oil; Ultrasonic irradiation; Tungstophosphoric acid catalyst; Optimization; Interaction (search for similar items in EconPapers)
Date: 2013
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Persistent link: https://EconPapers.repec.org/RePEc:eee:renene:v:50:y:2013:i:c:p:427-432

DOI: 10.1016/j.renene.2012.07.013

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